1、:D7169-16 ,STANDARD TEST METHOD FOR BOILING POINT DISTRIBUTION OF SAMPLES WITH RESIDUES SUCH AS CRUDE OILS AND ATMOSPHERIC AND VACUUM RESIDUES BY HIGH TEMPERATURE GAS CHROMATOGRAPHY 2017 ():25.12.2017:3348-17/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstanda
2、rt.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing a
3、nd Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Rep
4、roduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D7169-16 1 :D7169-16 ,1 D7169;,.().1.*1.1 .().1.2 ,1 ASTM D02 ,D02.04.0H .15 2016.2016.2005.2011.D7169-
5、11.DOI:10.1520/D7169-16.ASTM D7169-16 2 720C,n-C100.1.3 ,C4-C8,.,C4-C8.,.(GC),D7900(.X1).1.4 ,.,.1.5 ,.1.6,-,ASTM D7169-16 3.,.1.7 ,.,.8.2.2.1 ASTM:2 D2887 D2892 (15 )D4057 D6352 174C 700C D7500 100C 735C D7900 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D7169-16 4
6、E594 -,E1510 3.3.1 ,:3.1.1%,.3.1.2 ,(/).3.1.3 (FBP),99,5%,(,100%).3.1.4 (FEt),.3.1.5 (FET),.3.1.6 (IBP),0,5%.3.1.7 (QF),.3.1.7.1 ,(QI),ASTM D7169-16 5.3.1.8 (QI)CS2,.3.1.8.1 ,-,.3.1.9 (R)%,.3.1.9.1%.3.1.10 (RF),%.3.1.10.1 (ASTD),(MSTD)(MSLSTD),.,5010.3.1.11 (ASMP)(),.3.1.12 (),;,.3.1.12.1 ,0,1.,0,05
7、.3.1.13 (SET),-ASTM D7169-16 6,.3.1.14%(RC).3.1.14.1%(ASMP),(RF),(MSMP)(MSLSMP),.3.1.15%(Rt)%,100%.3.1.15.1%,99,6%101,2%,%(Rt)99,6%;100%.3.2:3.2.1 ASMP 3.2.2 ASTD 3.2.3 MSL ,3.2.4 MSLSTD ,3.2.5 MSMP ,3.2.6 MSTD ,.4.4.1 ,ASTM D7169-16 7 ,.-,.,.5010 ,D6352 D7500,.,.5.5.1 ,.%.,.ASTM D7169-16 8 6.6.1 ,.
8、1.:6.1.1-(FID)-,5C 10C ,0,018 (0,45),.FID 0,005/(.E594)106.6.1.2 50C ,.,.-.,.6.2 -,-.,.6.3 ,ASTM D7169-16 9 ,.10,0,1.,.6.4 ,.,(0,1 0,2).5 10 23 26.6.5 -,1%.-.7.7.1 100%0,5 0,09 0,17.7.2 ASTM D7169-16 10 435C.1.20C 0 15C/425C-435C 10 C 50C 15C/425C 5 0,53 0,09-0,15 PDMS 20/-D FID 435C ,:40/450/(N2,He
9、)15/0,2 0,5 1,0 2,0%()10 40 50 A,.,.D .7.3 100.,C100 .7.4 50 52 .1,8 4,0.1 13.1.7.5 n-C5 ASTM D7169-16 11 ,CS2,20C.n-C5 .,.7.6 .C12 C24.0,8 1,2.2 13.2.7.7 -20/.8.8.1 (CS2),99+%.().CS2 .CS2 /.,CS2,.8.2 Polywax 655 Polywax 1000 .-22,.8.4.1 8.4.3,(C5-C100).ASTM D7169-16 12 8.3 :8.3.1 99%.8.4 -.Polywax(
10、P655 P1000),C5-C20,Polywax.,.,8.4.1-8.4.3,-(.8.3),Polywax 655 1000.8.4.1 20 CS2 50.8.4.2 ,8.3,.500 20.500 20 .4C Polywax 655 .-;-.ASTM D7169-16 13 8.4.3 25 Polywax 655 ,8.4.1.10 ,8.4.2.-(200),(15 20)20 ,.CS2(.8.1).8.4.4 2,8.4.3,2 .,4C.1 Polywax Baker Petrolite Corp.(Barnsdall,OK).-,.-Polywax 655 Pol
11、ywax 1000 ,.8.5 -.,.8.5.1 ,:ASTM D7169-16 14 8.5.2 100 0,1 50.CS2 .,.,3.8.5.3 3.8.5.4 ,8.5.2,2.0,1 0,2.8.6 5010 ,5010,.,D7500.8.7 :8.7.1,99,999%.().10/3.8.7.2,99,999%.().10/3.ASTM D7169-16 15.8.7.3,99,999%.().10/3.FID .8.7.4,99,999%.().-5/3.10/3.9.9.1 ,.1.9.2 ,.,D2887 E1510.9.3 ,5C 10C .9.4 :9.4.1 ,
12、C2,C3 C4,C5,-20C C5 C6 CS2.ASTM D7169-16 16 C5 1-4,n-C5.9.4.2 ,IBP ,100C,35C 40C.,.,9.4.1.,20C.10.10.1 .,D4057.,(10).10.2,60C.,(CS2).10.3 0,2 0,25 0,1.10 CS2.0,1.10.3 4C.ASTM D7169-16 17 .10.4 ,.,.11.11.1 0,2 0,25 5010 0,1.10 CS2 0,1.,4C.12./12.1 ,.1.12.2 10,0,1.,.,.,5 10 .12.3 .,.ASTM D7169-16 18 1
13、3.13.1 ,8.4.0,1 0,2 :R=2(t2 t1)/(1,699)(W2+W1)(1):R-,t2-()n-C50,t1-()n-C52,W1-()n-C50 ,W2-()n-C52 .13.1.1 ,1,8 4,0.13.2 ,.8.4,C12-C24,s .C7-C100 s 0,8 2,0.s=(a+b)/2a(2):s-,a-,10%,b-,10%,.,ASTM D7169-16 19 0,8 2,0.13.3 ,8.5,0,1 0,2 Fi :(3):Mi-,20-,Ai-,Ac20-,Pi-(%),8.5.3,Pc20-(%).13.3.1 Fi 0,9 1,10.Fi
14、 ,.14.14.1 ,.14.2 14.6.-,-ASTM D7169-16 20.14.2 .(.15.3),.1.1.5010 ,QC.14.3 ,8.4,.1.2.C5,CS2,C6 C7,C6 C7.C100.14.4 5010,8.5 ,.,20C,.1.3.,4 ,2%.14.5 ,ASTM D7169-16 21 10.3,.QC .14.6 CS2 .,.15.15.1 .,5010.15.2 ,.,13.2.C5-C7 ,.1.2.15.3 ,.1.4 30API,.1.5 ASTM D7169-16 22,.15.3.1,QC .QC ,.15.4 ,.,.,-,.1.6
15、.,.,10%.(,4 5).15.4.1 ,.1.7.15.4.2 .ASTM D7169-16 23,3%.15.5 5010,D6352.5010,.2.,(.16.1.7).2.5010,%BP.C 95,5%Cl,C.F 95,5%Cl,F IBP 428 9 801 16 5 477 3 891 5 10 493 3 918 5 15 502 3 936 5 20 510 3 950 6 25 518 4 963 6 30 524 4 975 7 35 531 4 987 7 40 537 4 998 8 45 543 4 1008 8 50 548 4 1019 8 55 554
16、 4 1030 8 60 560 4 1040 8 65 566 4 1051 8 70 572 4 1062 8 75 578 5 1073 9 80 585 4 1086 8 85 593 4 1099 7 90 602 4 1116 8 95 616 4 1140 7 FBP 655 18 1213 32 A D6352.16.2 .ASTM D7169-16 24 ,16.1.2.3 5010 ,16.1.4.16.1 :16.1.1 5010(),.16.1.2 5010.,.16.1.3 ,16.1.2.16.1.4 ,5010 5010.16.1.5 5010 ,FEt,D6352,ASTM D7169-16 25 .16.1.6 5010 .,.ASTD.16.1.7 5010 5010 D6352 .,.2,.,-.,;,.16.2 :16.2.1 ,5 ,.,3,12.2.16.2.2 ,16.1.2.ASTM D7169-16 26 16.2.3 ,16.1.3.16.3 ,16.1.4.16.4 FID,CS2 .,CS2.,1,930,.,.,CS2.,D28