1、 D 7220-12(2017.),STANDARD TEST METHOD FOR SULFUR IN AUTOMOTIVE,HEATING,AND JET FUELS BY MONOCHROMATIC ENERGY DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY 2018 ():07.08.2018:3510-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100
2、 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM Internation
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4、anslations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D7220-12(2017)1 D 7220-12(2017.),1 D7220,.().1.1.1 (EDXRF),2 3/942/.1.1.1 ,1 ASTM D02 ,D02.03 .1 2017.2017.2006.2012.D7220-06.DOI:10
5、.1520/D7220-12R17.ASTM D7220-12(2017)2 ,3/.1.1.2 ,(RFG),/,20 ,/,5 2.1.2 ,.C/H ,.1.3,.1.3.1 /.1.4 ,.,.1.5 ,(TBT).ASTM D7220-12(2017)3 2.2.1 ASTM:2 D4057 D4177 D6299 D6300 E29 3.3.1:3.1.1 ,.,5%.3.1.1.1 EDXRF (=45 5,).().(Pd Ag)(),2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM
6、.ASTM D7220-12(2017)4 .3.2:3.2.1 DBS -,3.2.2 Kcps .3.2.3 EDXRF 3.2.4 PTFE 3.2.5 SDBS -,21,91%3.2.6 SStd ,/,3.2.7 SStock ,/,3.2.8 STK ,4.4.1 K 2,307.,-(.8.4),./.(.,.ASTM D7220-12(2017)5,.).5.5.1 ,2 .180 360.5.2 ,2 .,.5.3 ,6.6.6.1 (),.,-.6.2 M-85 M-100 ,85%100%.,K.,ASTM D7220-12(2017)6 (),.6.3 ,11,.,.
7、,.7.7.1 ,:7.1.1 ,Ag Pd ,.L Ag Pd.,.7.1.2 ,4 .7.1.3 ,175 5,9 Kcps(10000 ).ASTM D7220-12(2017)7 Si.,(,).7.1.4 ,(.8.6).,4,0 (30,4).7.1.5 ,/.8.8.1 3 .,.,.8.2-.3 ,American Chemical Society,Washington,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,Inc.(USPC),Rockville,MD.ASTM D7220-12(2017)8 (.11.1).(-.)1 -,.8.3 ().,.,
8、(),1%.(11.4)(12.1).(.13.1).8.3.1 ,.,.8.4 ()-,0,2/.(,),.,-C/H .8.5 ,ASTM D7220-12(2017)9 ,2 6.,.5 6.,.,.8.6 ,99,9%.8.7 ,.8.8 ,.(.11.5).8.9 ,.2 .,.9.,9.1 D4057 D4177,.9.2 ASTM D7220-12(2017)10 .,.,.,(),.,(,).,.,.,.,.,.,.,.9.3 ,ASTM D7220-12(2017)11 .,(50/).(.9.2).,.(.8.5,8.7,9.2,9.4 9.5).9.4 /,.,9.2.9
9、.5 ,.,.9.6 ,.10.10.1 .,.11.11.1 :11.1.1 -0,1,.1,ASTM D7220-12(2017)12 -.(,PTFE).1/:SStock=DBS SDBS (DBS+)1000(1):SStock-,/,DBS-,SDBS-,21,91%,-.1 ,/-,-,2498 197,72 2,28 11.1.2 -0,1,.2,.(,PTFE).1/:SStd=STK SStock (STK+)(2):SStd-,/,STK-,.ASTM D7220-12(2017)13 2 ,/-,/-,0 100,0 0,0 50 98,0 2,0 5 99,8 0,2
10、 100 96,0 4,0 10 99,6 0,4 250 90,0 10,0 25 98,8 1,2 500 80,0 20,0 50 98,0 2,0 750 70,0 30,0 1000 60,0 40,0 3 ,.2.4 ,.2.11.1.3 .,.,.11.2 ,11 12.11.3 :11.3.1 ,11.3.2 :S=a R+b(3)ASTM D7220-12(2017)14:S-,/,R-,a-,b-,.11.4 ,.A 13.1.11.5 (.8.8).,.b(11.3.2),S .12.12.1 ,.B 13.1.12.2 ,.,.ASTM D7220-12(2017)15
11、 ,.,.12.3 .12.4 K 2,307.,-(.8.4),.5 Pd ,2,86-2,92 2,95-3,04.12.5 ,13.6 .,.,./.13.13.1 ,8.3,:F=A B(4):ASTM D7220-12(2017)16 A-,(.11.4),-,(.12.1).13.2 K .13.2.1 F .13.3 11.14.14.1 ,13.3,.,/,10/,10/,E29.,D7220.15.15.1 ,4,5 D6300.4 (ILS 2006.)-ASTM International RR:D02-1592.ASTM Customer Service service
12、astm.org.5 (ILS 2012.)-ASTM International RR:D02-1736.ASTM Customer Service serviceastm.org.ASTM D7220-12(2017)17 6,(NIST 2770),(NIST 2299)(NIST 1616b)()().7 ILS,(95%),.8 ,.,.15.2 :15.2.1 ,:0,64300,504/(5):X-3 942/,.(.3.)3 ,/,/3 1,1 5 1,4 10 2,1 25 3,3 6 (NIST),100 Bureau Dr.,Stop 1070,Gaithersburg,
13、MD 20899-1070,http:/www.nist.gov.ASTM D7220-12(2017)18 50 4,6 100 6,5 250 10,4 500 14,7 942 20,3 15.2.2 ,:1,11210,504/(6):X-3 942/,.(.4.)4 ,/,/3 1,9 5 2,5 10 3,5 25 5,6 50 8,0 100 11,3 250 18,0 500 25,5 942 35,1 15.3 (NIST 2770),(NIST 2299)(NIST 1616b).,ILS ARV()NIST 95%.5.ASTM D7220-12(2017)19 5 ,N
14、IST ASTM,(RR)NIST SRM,/NIST ,/ASTM ILS ,/(95)?NIST 2770 41,57(0,39)41,8 0,2 NIST 2299 13,6(1,5)12,5-1,1 NIST 1616b 8,4(0,12)8,9 0,5 16.16.1 ;ASTM D7220-12(2017)20 ()X1.X1.1 ().X1.1.1 ,.X1.2 ,.D6299 MNL 7.7 X1.3 .D6299 MNL 7.7 X1.4 ,.,.,.ASTM,.D6299 MNL 7.7 X1.5,7 MNL 7,6,ASTM International,W.Conshoh
15、ocken,PA Conshohocken,PA.ASTM D7220-12(2017)21 ,.,.ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.