1、Designation:D726012Standard Practice forOptimization,Calibration,and Validation of InductivelyCoupled Plasma-Atomic Emission Spectrometry(ICP-AES)for Elemental Analysis of Petroleum Products andLubricants1This standard is issued under the fixed designation D7260;the number immediately following the
2、designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope*1.1 This practice covers information
3、 on the calibration andoperational guidance for the multi-element measurements us-ing inductively coupled plasma-atomic emission spectrometry(ICP-AES).1.2 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this st
4、andard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2.Referenced Documents2.1 ASTM Standards:2D4057 Practice for Manual Sampling of Petroleum andPetroleum ProductsD4307 Practice for Preparation of Liquid Blends for Use
5、asAnalytical StandardsD6299 Practice for Applying Statistical Quality Assuranceand Control Charting Techniques to Evaluate AnalyticalMeasurement System PerformanceD6792 Practice for Quality System in Petroleum Productsand Lubricants Testing Laboratories2.2 ICP-AES Related Standards:C1111 Test Method
6、 for Determining Elements in WasteStreams by Inductively Coupled Plasma-Atomic EmissionSpectroscopyC1109 Practice for Analysis of Aqueous Leachates fromNuclear Waste Materials Using Inductively CoupledPlasma-Atomic Emission SpectroscopyD1976 Test Method for Elements in Water by Inductively-Coupled A
7、rgon Plasma Atomic Emission SpectroscopyD4951 Test Method for Determination of Additive Elementsin Lubricating Oils by Inductively Coupled PlasmaAtomic Emission SpectrometryD5184 Test Methods for Determination of Aluminum andSilicon in Fuel Oils by Ashing,Fusion,InductivelyCoupled Plasma Atomic Emis
8、sion Spectrometry,andAtomic Absorption SpectrometryD5185 Test Method for Determination ofAdditive Elements,Wear Metals,and Contaminants in Used Lubricating Oilsand Determination of Selected Elements in Base Oils byInductively Coupled Plasma Atomic Emission Spectrom-etry(ICP-AES)D5600 Test Method for
9、 Trace Metals in Petroleum Coke byInductively Coupled Plasma Atomic Emission Spectrom-etry(ICP-AES)D5708 TestMethodsforDeterminationofNickel,Vanadium,and Iron in Crude Oils and Residual Fuels byInductively Coupled Plasma(ICP)Atomic EmissionSpectrometryD6130 Test Method for Determination of Silicon a
10、nd OtherElements in Engine Coolant by Inductively CoupledPlasma-Atomic Emission SpectroscopyD6349 Test Method for Determination of Major and MinorElements in Coal,Coke,and Solid Residues from Com-bustion of Coal and Coke by Inductively CoupledPlasmaAtomic Emission SpectrometryD6357 Test Methods for
11、Determination of Trace Elements inCoal,Coke,and Combustion Residues from Coal Utiliza-tion Processes by Inductively Coupled Plasma AtomicEmission Spectrometry,Inductively Coupled PlasmaMass Spectrometry,and Graphite Furnace Atomic AbD7040 Test Method for Determination of Low Levels ofPhosphorus in I
12、LSAC GF 4 and Similar Grade EngineOils by Inductively Coupled Plasma Atomic EmissionSpectrometryD7111 Test Method for Determination of Trace Elements inMiddle Distillate Fuels by Inductively Coupled PlasmaAtomic Emission Spectrometry(ICP-AES)1This practice is under the jurisdiction of ASTM Committee
13、 D02 on PetroleumProducts and Lubricants and is the direct responsibility of Subcommittee D02.03 onElemental Analysis.Current edition approved June 1,2012.Published August 2012.Originallyapproved in 2006.Last previous edition approved in 2006 as D726006.DOI:10.1520/D7260-12.2For referenced ASTM stan
14、dards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe ASTM website.*A Summary of Changes section appears at the end of this standardCopyright ASTM Internation
15、al,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United States1 D7303 Test Method for Determination of Metals in Lubri-cating Greases by Inductively Coupled Plasma AtomicEmission SpectrometryD7691 Test Method for MultielementAnalysis of Crude OilsUsing Inductively Coupled Plasma
16、Atomic EmissionSpectrometry(ICP-AES)E1479 Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers2.3 Other Standards:IP 437 Determination of Additive Elements in Unused Lu-bricating Oils and Additive Packages by InductivelyCoupled Plasma-Atomic Emission SpectrometryISO/TC 17/SC 1 N 883 Guidelines for the Preparation ofStandard Methods of Analysis Using Inductively CoupledPlasma-Atomic Emission Spectrometry and for Use ofICP Spectrometry for the Determinati