1、 542372010 -542372010II,2012,2019 ,-1 -(),-42 179 3 -23 2010.1036-4 -ASTM D 63492008 -,-(ASTM D 63492008 Standard test method for determination of major and minor elements in coal,coke,and solid residues from combustion of coal and coke by inductively coupled plasma Atomic emission spectrometry,MOD)
2、,-5 6.C 2019.26 29 2015.162-.-(1 ),.().,-(www.gost.ru)542372010III1 .12 .13 .24.35 .46.57 .68 .79 .710 .811 .912 .1013 .1014.1115 .11 542372010IV ASTM D 63492008,-,:-;-10538;-7 ,12 ,15 ;-ASTM D 63492008 6 5 6-;-6 ,ICP-,3,5 6 ASTM D 63492008;-7 ,-7.10,7.11,10.3.3,11.2.2 ASTM D 63492008;-,-;(4,5),;-10
3、 ,;-11022 750 (815 0).ASTM D 63492008(10.1),-.-2 3,.1 -Solid mineral fuels.Determination of chemical compositionof ash by method of atomic emission spectrometry with inductively coupled plasma 542372010 201207011 1.1 ,(),-.,.-:.,10538.-10538.2 :5725-62002 ()-.6.(5725-6:1994,IDT)51568 .(3310-1:1990,M
4、OD)517601).52501 .(3696:1987,MOD)529172).(11722:1999,5068-2:2007,MOD)1770(104283,478880).-,.3118.4461.6563 .1)337562016.2)335032015.5423720102 6709 .9656.10484.-.10538 .10742 ,.10929.110221).(1171:1997,MOD)11303 .11305.11306 .13867 .23083 ,.241042).25336 .,27313 .-(1170:1977,MOD)27589.(687:1974,IDT)
5、-,1 ,-.,.,-,().,.,.3 .,-.-,.-(ICP-AES).1 ,-.2,1.-2 .-,.1 ,11022,-,-.2 .-,ICP-,-,.1)556612013.2)532282008.532282008.54237201033 .1 ,ICP-AES,212,412;288,16;251,611396,152;256,80;308,215;309,271259,940;271,44;238,204317,93;315,887;364,44;422,67279,553;279,08;285,21;277,983337,280;350,50;334,941178,287;
6、214,900766,491;769,896588,995;589,592182,04257,610;294,92;293,31;293,93455,403;493,41;233,53421,55 2 (/3),-100/3,AlCaFeMgMnTi308,2150,21455,103317,9330,010,010,040,03259,940-0,12279,0790,020,130,250,07257,6100,0050,0020,002288,148588,9950,08 ,-,:Al,Ca,Fe=1000/3,Mn=200/3,Mg=100/3.4 ,.13867.4.1 2-5250
7、1.6709 .52501 2-51760.4.2 (Hl),20=1,19/3 3118.4.3 ,1:1.4.4 -(HF),20=1,17/3 10484.4.5 (HNO3),20=1,42/3 4461.4.6 ,5:95.50 3 (.4.5)(.4.1)1 3.4.7 -70:30.(.4.2)-(.4.4).4.8 ,.(.4.5)(.4.2)-(.4.1).4.9 (H3BO3)9656.4.10 ,1,5%.,54237201044.11 10929,30%.4.12 :,Li2B4O7 5H2O,(LiBO2)1:4.4.13 (LiI 3H2O),.4.14 1000/
8、3.,99,999%.(.5.1).,ICP-AES.(.7.1).4.15 ,(Sc),(Y),(In).-1000/3.,99,999%.(.5.1).4.15.1 (III),Sc2O3,.4.15.2 1000/3.1,534 (.4.15.1)(.4.8),-.50 3 (.4.1),100 3 (.4.3).1 3,(.4.1).,.4.16 ()-.-.,.4.16.1 ,-.4.16.2 .,.-.4.16.3 .,.4.16.4 .,.5 5.1 2-24104 -0,1.5.2 ,-700 1000.1.-11022.5.3 1000 1200.5.4 35 85 3 65
9、63.5.5 .5.6 ,51760,.5.7 ,250 3,100 130 ,.,.,54237201055.8 .(,-.)1770 25336.5.9 75 51568.6 6.1-(ICP)-.-.,-.,-.,.,.,-.6.2 -.,-,.,.,.-.,.-.6.3 ,.,.:;-,-.,6.2.,-,-,.,.,-.,.,.-.-,(.4.15).()5423720106 361,383.6.4 .7 7.1 1000/3(.4.14)0,1 100/3 (.7.2).7.2 (4,0 0,05)(.4.12),-0,1,1000 3,(.5.5).500 3 (.4.6)-.,
10、-.30 .1000 3.(.4.1).-,.7.3 (.7.2).-,.-(.11).7.4 100 3 -(.4.14).1 3 (.4.15).(.7.2),.7.5 7.5.1 ,(.7.3)(.7.4),.3 -,:-;-;-(1/10).3 10/3 20/3 180/3 230/3 -15/3200/3 -30/3400/3 -1,5/320/3 54237201077.5.2 :(,).8 8.1 ,10742,23083 11303.-,-,.1,-.-52917,27589 11305 11022 11306.8.2 110 115.,.-75 51568.,.9 9.1
11、(.8.1).,-.6.-(.5.2),11022 .2 (815 10).,2.,75.(815 10)1,.2,-(815 10).:(815 10),-,.9.2 ,8.2,-,.2.,-,1 500,2 (815 10).-(815 10).75.(815 10)1,-.2,(815 10).:(815 10),()5423720108,-.10 10.1 10.1.1 :-;-,.,.-,-.10.1.2 ,-,.,.,-.10.1.3 -(.4.6),(.4.1).-.,.(.4.6),(.4.1).10.1.4 0,1.10.2 (0,1 0,001),9.1 9.2,(.5.4
12、).(0,4 0,005)(.4.12).-.-(.4.13)(0,1).-1000 1200 (.5.3).-1000 1200 7 .(.4.1),250 400 3.50 3 (.4.6).(.5.5).,30.(.4.1).100 3.1 3 (.4.15)(.4.1).-1000/3 4/3.1 .-,.2 ,.-,.542372010910.3 (0,1 0,001),9.1 9.2,(.5.7)250 3 .130 ,-,.-.,1 3 22(.4.11).,-.,13.5,0 3 HCl HF(.4.7)2,0 3 HNO3(.4.5).100 130 2.-93,0 31,5
13、%-(.4.10).1.,-,.,.HCl:HF(70:30)(.4.7)-,(HCl HNO3)(.4.8).-HCl:HF HNO3 HF.11 11.1 ICP-.11.2 ,ICP-,(-),:-(,);-,;-6 (,-),10;-;-3 ().11.3 -,.,.11.4 ICP-.11.4.1 (.4.16.3)(.7.3).10%.,.5423720101011.4.2 10,(.4.16.4)(.7.3).10%.,-,.11.5 ,.,-.11.6 -ICP-,-.12 ,-,-.12.1 ,40.,-.12.2 .12.3 ()-.-,(.14).-(.4),5.2 57
14、25-62012.12.4 -(.4.16.2),.,-,5725-6.12.5 (.4.16.1).-,5725-6.12.6 -,%.-,SO3,5%.-5%,.,.13 13.1 ,%,A=CVDm100,(1),/3(/3);V ,10,V3(3);D ;m ,.5423720101113.2 d,%,ddA=A100,(2),%;d ,%.d13.2 27313.14 -4.-r R.14.1 r ,-,-,4.14.2 R ,-,4.4 -(r)(R)SiO22,04%73,73%0,13+0,09 2,00+0,10Al2O31,04%29,54%0,17+0,060,86+0,
15、07Fe2O30,39%47,94%0,130,23MgO0,40%7,29%0,02+0,080,11+0,11CaO1,04%44,03%0,110,25TiO20,06%1,47%0,02+0,070,05+0,12K2O0,09%2,53%0,06+0,110,14+0,30P2O50,10%1,34%0,01+0,180,11+0,31 Na2O0,17%7,44%0,06+0,090,10+0,17MnO2198%834 ppm0,160,42BaO266%950 ppm0,07190BaO0,13%3,00%0,170,30SrO285%10460 ppm33+0,076 73+0,164 SO30,14%10,0%0,03+0,060,08+0,06 ,.,.15 :););););)-,.),542372010.,.30.09.2019.25.11.2019.60 841/8.1,86.-.1,58.,115419,.,11.www.jurisizdat.ru y-bookmail.ru ,117418,-,.31,.2.www.gostinfo.ru infogostinfo.ru 662.6:543.812:006.354 75.160.10:;-;-