1、MEXTOCYAAPCTBEHHbIM COBET No CTAHAAPTM3ALN,METPONor CEPTOKALM(MrC)INTERSTATE COUNCIL FOR STANDARDIZATION,METROLOGY AND CERTIFICATION(ISC)FOCTMETOCYAAPCTBEHHbI33583-CTAHAAPT2015yrOb AKTBPOBAHHbINPAHYJIPOBAHHbIMCTaHAapTHbIn MeToA onpegeneH nbineo6pa3oBaHnAnp CTpaHM3AaHne onnanbHoeMocKBaGnCTaHAapTHopM2
2、016FOCT 33583-2015ME KTOC YA APC TBEHHbIMC TAHAAPTyOb AKTMBMPOBAHHbIM PAHYMPOBAHHbIMCTaHAaptHLI MetoA onpeAeneHA nLineo6pa3oBaHnA npn nctupaHnnGranular activated carbon.Standard method for determination of dusting attritionAaTa BBeAeHn-2017-04-011 06nacTb npMeHeHA1.1 Hactogwn cTaHAapt ycTaHaBnnBaet
3、npouegypy oueHkn conpoTuBneHnA(cTokoctu)rpaHynupo-BaHHbIX aKTBnpoBaHHbix yrne k nbineo6pa3oBaHnio np ncTpaHn.B HacToeM cTaHAapTe Ko3中nun-eHt nbineoopa3oBaHng npu nctupaHnn,DA,onpegengeTcA Kak Macca(unn paccynTaHHbI o6beM)nbInn BeqnHnLy BpeMeHn,co6paHHo ha npeABapnTenbHO B3BeweHHOM 中NLtpe,no otHoweHn
4、io K Macce eAHbIyrng,noMeweHHon B ycTaHoBneHHoe(onpegeneHHoe)Bn6panOHHoe ycTpoicTBo Ha onpegeneHHoe BpeMA.Take MokeT 6bITL onpegeneHo nepBoHa4anbHoe cogepxaHe nbinn B npo6e.An HacTouero cnbiTaHngrpaHynupoBaHhbi aktuBupoBaHhbi yronb gonkeH cogepxatb He MeHee 90%4actny,pa3Mep koTopbix 6onb-we 80 Mew(0
5、,18 MM)(cM.ASTM D 2867).1.2 EAnHbi n3MepeHng,npuBeAeHHble B cncTeMe CN,cunTalotcA ctaHAapTHbIM.EAnHNLbi N3Mepe-hu(AoMbi n 中ytbi),yka3ahhble B cko6kax,npuBegeHbi Ang nHopmaynn.1.3 B HacToAueM cTaHgapte He npeAycMoTpeHo paccMOTpeHe Bcex BonpocoB o6ecne4eHnA 6e3onac-HOCTM,cBA3aHHbIX c ero cnonb3oBaHeM.
6、onb3oBaTenb cTaHgapTa HeceT OTBeTCTBeHHOCtb 3a o6ecne4e-HMe cooTBeTCTByHOWMX Mep 6e3onacHocT n oxpaHbI 3AopoBbA u onpegenget yenecoo6pa3HOcTbnpMeHeHn 3aoHoaTenbHbx orpaH4eH nepeg ero cnonb3oBaHeM.2 HopMaTBHble ccbInKnAng npuMeHeHng Hactoguero ctaHgapta Heo6xoguMbi chegyiouwne ccbino4Hble gokyMeHtbi.
7、An Hega-TpoBaHHbIX ccbInoK npMeHoT nocneHee n3gaHe ccbino4Horo gokyMeHTa(Bknio4ag Bce ero n3MeHeHng).2.1 CTaHAapTbI ASTM1)ASTM D 2854 Test Method for Apparent Density of Activated Carbon(MeTog onpegeneHn HacbInHoinnoTHOCT aKTBpoBaHHoro yrng)ASTM D 2867 Test Methods for Moisture in Activated Carbon(M
8、eTogbi onpegeneHn Bnarn B aKTBnpo-BaHHOM yrne)ASTME 11 Specification for Woven Wire Test Sieve Cloth and Test Sieves(CTaHgapTHa cneunpnKaunaHa npoBono4Hy cToTKaHb cnbITaTenbHble cTa)ASTM E 300 Practice for Sampling Industrial Chemicals(paKTuKa or6opa npo6 npoMbIWneHHbIX XnMM-yecknx npoAykToB)1)YTO4H
9、NTb CCbUKn Ha cTaHgapTbi ASTM MOHO Ha cavite ASTM:www.astm.org nnu B cny6e noggepxkn KnneH-ToB ASTM:serviceastm.org.B nHpopMaunoHHoM ToMe exerogHoro c6opHnKa cTaHgapToB(Annual Book of ASTMStandards)cnegyer o6pauaTbc K cBogke cTaHgapToB exerogHoro c6opHnKa cTaHgapToB Ha cTpaHnue caviTa.M3aHne onunanb
10、Hoe0CT33583-20153 CywHocTb MeToAa3.1 OnpeneneHHbln o6beM onpeneneHHoN Maccbl rpaHynnpoBaHHoro aKTNBNpoBaHHoro yrna noMewa-HOT B npobonepatenb,KoTopbin nonBepraoT BNopauln c nocTOAHHbIM yckopeHneM(g)B TeueHve onpeneneH-Horo BpeMeHn.IbInb nepeHOCNTCA Bo3nyWHbIM noTOKOM,npoXonAwM yepe3 Bn6pnpylowlylo n
11、poby,n 3aTeMcKannNBaeTCa Ha npenBapnTenbHo B3BeweHHOM nnbTpe.KonwyecTBo nbinn,co6paHHoe 3a wecTb neCATN-MNHyTHbIX WHTepBanoB,onpenengeTca B3BewNBaHneM Ha aHanNTNyecKMX Becax.4 3HayeHne n npnMeHeHne4.1 AKTNBNpoBaHHbIN yronb MoxkeT MexaHnyeckn pa3pywaTbca non Bo3neNCTBneM Tpex cwn:ynapa,apooneHna N WC
12、TMpaHNa.N3 3TWX Tpex Bo3neNCTBNN,NCTNpaHne wnw a6pa3na ABnAOTCA Hanbonee yacToNnpNyNHONo6pa3oBaHna nblnN BnpakTnyeckon 3kcnnyaTauln.Ony6nNkoBaHHble MeTonbl NcnblTaHnn no onpe-eneHWio npoYHOCTNaKTNBNpoBaHHbix yrnen naloT pe3ynbTaTbl,KOTopble,B o6weM,Henb39 wcnonb3oBaTbHa npaKTnke.HanpnMep,npn onpenen
13、eHwn npoyHOCTN c Ncnonb3BaHneM MeTannnyecknx wapNKoB w nono-HOB Ha npoby Bo3neNcTByIOT Bce Tpn chnbl pa3nM4HbIM o6pa3oM,4To o6ycnoBneHo pa3MepoM,dopMon NnnoTHOCTblo yacTNU.VcnblTaHne Ha WcTMpaHne c noMowblo MarHNTHON Mewankn npenycMaTpnBaeT WCTnpa-HMe npo6bl no pa3Mepa yacTNu MeHee 12 Mew.Pe3ynbTaTb
14、l Takoro wcnblTaHna cNnbHo 3aBNCAT OT reoMeTpNyacTNU.B oTnNyNe oT nepeyncneHHbIX MeTonoB NcnblTaHwn,npouenypa wcnblTaHwN,ycTaHoBneHHaa HacTog-WNM CTaHnapToM,no3BonaeT N3MepNTb neNcTBNe cNnbl TpeHNA,BO3HWKalowen Mexkny BN6pnpyiowNMN MMenneHHO ABnraOwNMNCA yacTnuaMN Bo BpeMa NcnblTaHna,N Mano 3aBNCNT
15、OT pa3Mepa,opMbl n nnoTHOC-TN 4aCTNU5 O6opynoBaHne n Tpe6oBaHna K HeMy5.1 Bn6paunoHHa ycTaHoBKa2),cnoco6Has o6ecneyNTb RMS(cpeAHekBanpaTnyHoe 3HayeHne)ycko-peHne 40 M/c2(4g).5.2 VcnblTaTenbHaa ayenka(KaMepa),CM.pwcyHOK 1,N3roToBneHHaa N3 anoMNHnA wnM Apyroro 3neK-TponpoBonawero MeTanna.5.3 nbe3o3neK
16、TpnuecknN akcenepoMeTp3)cnoco6HbIN N3MepNTb RMS yckopeHne,BblopaHHoe nonb30-BaTeneM.nonxonawa ycTaHoBKa n 3HayeHna 40 M/c2(4g)noka3aHa Ha pncyHKax 1 n 2.5.4 npeo6pa3oBaTenb cnrHana4),na B3anMonencTBna akcenepoMeTpa c MnnnnBonbTMeTpoM AC,cnoco6HbIn npoN3BOANTb BbIXO Hoe nMHeNHoe HanpaxkeHne OT 0 no 1
17、 B,nponopunoHanbhoe yckopeHno.5.5 BonbTMeTp5)nepeMeHHoro ToKa OT 0 Ao 1 B.5.6 AMnepMeTp nepeMeHHoro Toka oT Oo 1000 MA c norpewHoCTblo N3MepeHna no 1 MA.5.7 PerynupyeMbin TpaHcdpopMaTop oT 0 Ao 120 B.5.8 TanMep oT 0 no 120 MMH.5.9 Pe3WHoBaa Bn6pon3onAuNoHHaa npoknanka.PekoMeHnyeTca Ncnonb3oBaTb npok
18、nanky N3 Heonpe-HOBoN pe3MHbI TBep oCTblo 45 ycn.en.5.10 PacxonoMep c perynnpylowM knanaHoM,cnoco6HbIN KOHTponnpoBaTb TOK Bo3Ayxa npn cKopoc-TN,BblopaHHon nonb3oBaTeneM HacTogwero cTaHnapTa.noToK npNMepHo 7 n/MNH CYWTaHOT nonxonAWNM npMNcnonb3oBaHnn o6opynoBaHna,noka3aHHoro Ha pncyHKax 1 W 2.5.11 nn
19、bTp nna ynaBnnBaHna yacTnu,nonxonawero pa3Mepa Ang coeAnHeHna c ncnblTaTenbHonAyeNkon(KaMepon),cnoco6Hbin ynaBnnBaTb yronbHyio nbinb.wnbTpbl N3 CTeknoBonoKHa CuNTalOTca nonxo-WNMN.Takke 3pobeKTNBHbIMN B Ncnonb3oBaHnN ABNAHOTCA NnbTpbl ynaBnnBaHna TBepnblx yacTNU,npe Ha3HayeHHble n 3aWNTbl opraHoB bi
20、xaHNA npn okpacke pacnbineHneM wnN npyrx onacHOCTAX,BO3HN-KarowNx npl pacnbineHNN.5.12 TpagyupoBaHHbin unnNHap BMeCTNMOCTbIo 100 Mn.5.13 AHanTMyeckne Becbl c norpewHoCTblO N3MepeHNA no 0,1 Mr.2)HanpnMep MOXHo ncnonb30BaTb Bn6paunoHHyo ycTaHoBKy KoMnaHnn Buffalo Dental Manufacturing Co.,(Underhill Bl
21、vd.,Syosset,NY 11791),Mogenb Ne 1,40 BT npn 115 B,60 Tu,a Takoke BM6pocTanKnBaTenb,Mogenb SyntronM J-1A,30 BT npn 115 B,60 Tu,wnm nx aHanor.3)HanpnMep MOXHo ncnonb3oBaTb akcenepoMeTp KoMnaHnn Endevco,Mogenb Ne 2251,nnn aHanoryHbin.4)HanpnMep MOXHo ncnonb30BaTb npeo6pa3oBaTenb CnrHana KoMnaHnn Endevc
22、o,MoAenb Ne 4416,pa6oTaownnnoapo MynTMeT Keithley 179 oM Keithley Instruments(AurorRd.,Cleveland,OH 44139).2OCT 33583-2015CTABalowa wnnba(4)Tpe6.10,32 UNF 5 Lq.(yHnupoBaHHa MenKa pe3b6a)Tanka 6apawek(4)Tpe6.10,32 UNFO-o6pa3Hoe ynnoTHnTenbHoe Konbuo(4)Tpe6.(6,4 MM)WecTrpaHHa ranka(8)Tpe6.10,32 UNFpKp
23、bBaoa nnacTHa(cM.pcyHoK 3)Pe3MHoBa npoknaAKa(CM.npMe4aHe 1)McnbTaTenbHa 4eka(cM.pcyHoK 3)Pe3MHoBa npoknaka(cM.npMe4aHe 1)MeTannneckoe cTo(cM.npMe4aHMe 2)Pe3HoBa npoknaKa(cM.npMe4aHe 1)Pa3enTenbHa ce(CM.pcyHoK 3)TepnoHoBa npoknaka(cM.npnMeaHne 1)中nbTPTenoHoBa npoknaka(cM.npMe4aHne 1)eppoppoBaHHa nnac
24、TnHa(cM.npMe4aHe 3)Pe3HoBa nponaKa(cM.npMe4aHe 1)BbTHa CeKM(CM.PCyHOK 3)BuHt c nnocko unHApuecko ronoBko(2)Tpe6oBane8,32 UNC Lq.CTonopHa wa6a(2)Tpe6oBaHe An 8 6onToBWecTrpaHHa ranka(2)Tpe6oBaHne 8,32 UNCBepXHAA KpeneHa nnTa B6paOHHO ycTaHOBKn(CM.pMcyHoK 3)WbpeBo naroBb coeHTenAn NPT-(1)门pume4aHue 1-
25、BHytpeHHn qnametp-2 3/4 goiMa(69,9 MM),Hapyxhbi Anametp-3 AoMa(76,2 MM),TonwHa 1/16 AoMa(1,6 MM).门puMe4aHne 2-poBono4HaA tKaHb 250 MKM 3 HepxaBeowen cTann AuaMeTpoM 3 AonMa(76,2 MM)no ASTM E 11.门puMe4aHne 3-lnactnHa c nponycKHLIM ce4eHneM 37%,n3roToBneHHaR n3 24 HepKaBelowencrann,Anamerpom 0,45 qoMa(11,4 MM),c orBepcrugmn 0,066 oiMa(1,68 MM)B yeHTpe,kBaApaTHaRceTka AaMeTpoM 3 AoMa(76,2 MM).PcyHoK 1-cnbiTaTenbHa 4eka An oTceBa nin6 logroToBka npo6bi,06pa3ybi n 06pa3ybi An cnbitahn6.1 OT6npalot npo6bi rpaHynnpoBaHHoro aKTnBnpoBaHHoro yrng B cooTBeTcTBnn c ASTM E 300(CM.Taloke 8.1).3