1、MEXTOCYAAPCTBEHHbIM COBET No CTAHAAPTM3ALN,METPONor CEPTOKALM(MrC)INTERSTATE COUNCIL FOR STANDARDIZATION,METROLOGY AND CERTIFICATION(ISC)FOCTMEXTOCyAAPCTBEHHbI33577-CTAHAAPT2015yrOb AKTBPOBAHHbICTaHAaptHbIn MeToA onpegeneHA coepxaHngBOAOpacTBOpMbIX BeeCTBM3AaHne on,nanbHoeMocKBaGnCTaHAapTHopM2016FOC
2、T 33577-2015(100,00,5)Mn.O6nnBaot cteHkn Kon6bi octaBweica 4actbio BoAbi.CoeAnHAiot kon6y c KoHAeHcatopoM nnoMewaloT Ha 3nekTpueckylo nnTky.8.4 AoBoAAt Bogy go megneHHoro knneHng c taknm pacyeToM,4To6bi hn oAHa actn4ka yrng He nonanaHa cTeHk Kon6bl.8.5 MeneHHo KnTAt B TeyeHe(900 10)c.8.6 CHnMalot ko
3、n6y c 3nektpuyeckoi nnutkn n 6bicTpo 中unbtpyiot ee coAepxnMoe 4epe3 6yMaKHbiounLtp,npegBaputenbHo cMoyeHhb Bogon tuna l,ucnonb3yemo Ang npoBegeHn ncnbitaHn.loMewa-ot unbtpat B Kon6y Ang unbtpoBahng nog BakyyMom BMectMOctbo 500 Mn,co6nogag ocTopOKHOCtb,yTo6bl He gonyctutb nonagaHng yactuyek yrng B un
4、btpat npu nepennBaHnn.8.7 Oxnaxgalot 中unbtpat go temnepatypbi okpyxaowen cpeAbi.(PH MOHO 3MepTb Ha nopynnnbTpaTa).8.8 门pokannBaiot npu TeMnepatype(1505)C cTeknAHHyio unn pappopoByio eMKoctb An Bbinap-BaHng go noctoHHon Maccbi(0,1 Mr).EMKoctb Ang BbinapnBaHng oxnaxgaiot go TeMnepatypbi okpyxalo-wen c
5、peAbin xpaHAt B3KcnKaTope Mexgy B3BewnBaHnAM.B3BenBaoT cyxyo eMKocTb Ang BbinapBaHn cTo4HOCTb go 0,1 r n 3ancbBaloT pe3ynbTat.8.9 cnonb3yA nunetky,nepeHocAt 50 Mn anuKBoTbi 中unLTpata Bo B3BeweHHyo cTeKngHHyio nnn 中ap-opoByo eMKocTb An BbinapBaHg.8.10 BbinapnBaioT unLtpat gocyxa B cywnnbHom wkay unu
6、Ha napoBon 6aHe go tex nop,noka xng-KOctb He cnaputcA.M36eraiot kung4eHng,4to6bi npeAotBpatntb notepo octatka.8.11 Cywat octatok npu(150 5)C B Te4eHne He MeHee 14,go nocToAHHO Maccbi(0,1 Mr).EMKOCTbAn BbinapBaHn c ocTaTKoM oxnaxAaioTAo TeMnepatypbi oKpyxaouwen cpeAbin xpaHAT B 3KcnKaTope Mex-Ay B3Be
7、WnBaHnAMn.B3BewnBaoT eMKOcTb Ang BbinapnBaHn cocTaTKOM CTO4HOCtbio go 0,1 rn3anncbiBaoTpe3ynbTaT.8.12 Ecnu octatok MeHee 10 Mr,noBtopgiot npouegypy.Ao6aBngioT HOByo anuKBoTy(8.9)B eMKOCTbAn BbinapuBaHg,coAepawyo ocTaTok oT npebiywen annkBoTbi.8.13 poBogt no ABa onpegeneHug Ha kaxgou uccneAyemou npo6
8、e yrng.9 06pa6oTKa pe3ynbTaToB9.1 06wu pacyet BoAopactBopuMbIx BeectB,%,npoBoAAt no 中opmyneBogopacTBOpnMble BewecTBa=(B-A)(D)(100)/(C)(E),(1)rge B-Macca eMKoct An BbinapBaHA c ocTaTKoM,r;A-Macca eMKocT Ang BbinapuBaHg,r;D-06bem BoAbi,cnonb3yeMon Ang 3KcTpakun,Mn;C-Macca yrng,r;E-o6beM cnonb3yeMon an
9、nKBoTbl,Mn.9.1.1 HanpMep,BogopacTBopMble BewecTBa,3KcTparpoBaHHble 3 oHonpoobl yrn np Bbinap-BaHn 50 Mn annKBoTbl,%,paccynTbiBalot cneAyiownM 06pa3om:BoAOpacTBOpnMble BewecTBa=(RW/CW)200,rge RW-Macca cyxoro ocTatka;CW-Macca cyxoro yrng.10 poToKon cnbITaH10.1 poToon cnbiTaH AoneH cogepaTb:10.1.1 cTo4
10、Hk nonyeHA;10.1.2 Tun n o603Ha4eHne aKTBpoBaHHoro yrng;10.1.3 HanMeHoBaHne nocTaBnka;10.1.4 o603Ha4eHne knacca nocTaBnKa(ToproBo Mapkn);10.1.5 HoMep nocTaBngeMon napT;10.1.6 MaccoByo gonio Bnarn no ASTM D 2867;10.1.7 cogepaHe BogopacTBOpMbIX BeeCTB;10.1.8 gaty npoBegeHn cnbiTaH;10.1.9 amunio nognuct na6opaHta,oTopbi npoBen cnbiTaHne;10.1.10 aMnnio n nognncb pyKoBonteng,ogo6pnBwero pe3ynbtatbi cnbitaHnA.3