1、 D519716 ()STANDARD TEST METHOD FOR DETERMINATION OF FORMALDEHYDE AND OTHER CARBONYL COMPOUNDS IN AIR(ACTIVE SAMPLER METHODOLOGY)2020 ():29.05.2020:3887-20/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Co
2、nshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,W
3、est Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,
4、except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D5197-16 1 D519716 ()1 D5197;,.().1.1.1 (HCHO)().,:,(),2-(),o-,-,-,2,5-.1.2 ,2,4-().1 ASTM D22 D22.05 .1 2016.2016.1991.2009.D5197-091.DOI:10.1520/D5197-16.
5、ASTM D5197-16 2 .-().TO-11A EPA()(.2.2).1.3 ,1(R,R1 (),R ()R1 ().,EPA TO-11A,-.,TO-11A,.10.2.4.10 ppb()1 ppm().,.1.4 .(1-24)(5-60).,.ASTM D5197-16 3 ,(1).2 ,.1.5 3 .1.6 ,1,5/.(8 1,0/)55-105.,(,).1.7 ,(2).,.2 ,.3 Sep-Pak Plus Silica.ASTM D5197-16 4 1.8,.1.9 ,.,.-.1.2.2.1 ASTM:4 D1193 D1356 D3195 D363
6、1 4 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.()2,4-()ASTM D5197-16 5 D3686 (c )E682 2.2 EPA():5 TO-11A EPA-625/R-96/010b,.,1999.3.3.1:3.1.1 ,.D1356 E682.3.2 :3.2.1 .4.4.1 ,0,5 1,5/.,.4.2 5 (EPA),William Jefferson Clinton Bldg.,1200 Pennsylvania Ave.,NW,.,20460,http:/www
7、.epa.gov.ASTM D5197-16 6 .,.,.4C .,10%25C)(9).:-1-0,64 0,46 KI ;-(5);-1.100 ppmv/().(,-),.,37-0,6-M KI.1.,-(3),6.2 ;,6.3 ,6.4 (),;10%75%ASTM D5197-16 9 6.5 ,6.6 ,6.7 -6.8 .6.9 -4C 6.10 ,6.11 6.2.3 (,KI)-.,.,90C .ASTM D5197-16 10 .2.(A)(B)6.2.4 KI .KI -.KI ,-(6).,90C.,/-,(10).6.3 ,(11,12).,-.()-0-1-2
8、-ASTM D5197-16 11 6.4 (75%)(10).,.2-50%20%(3).15C,.6.5,.10.2,-(14-16).,-,-,-.-()-(),2-(-)-()(14).,(,),.,(15).6.6 -,.-.ASTM D5197-16 12 40-60C .-.-0,15 .,.,.6.7 ,.-.,-360,.,.6.8 -,(17).6.9 -,.-.ASTM D5197-16 13 4C,4C (18).6.10 ,.(,-),.,(19).6.11 1 62%24-.,100%,2 (1).,2 .7.7.1 ,0,5-1,50/0,01/.2 3 ,/,/
9、,./0,5 1,5/.3 ,19 1,5/.,.7.2-,;ASTM D5197-16 14 ,:-;-(10 20);-18 (,25-4,6);-,360;-.-.4.4 -.7.3.7.4 (,4-),.7.5,.7.6 (.D3631).7.7 ,().7.8 ,5 2000.7.9,1 50.7.10 ,().7.11 ,1,.7.12 ,1,.ASTM D5197-16 15 7.13,(.7.2)().7.14 .3 7.15 ().7.16 (.D3195),.7.17 .7.18 ,/0,5 1,5/.7.19 ,0 10.7.20 ,(.5).7.21 (),10,-.K
10、I ASTM D5197-16 16 7.22 ,(0,163653).(59)10-,45 ,(.5).4.,-7.23/,.7.24 ,.,.7.25 ,(20125),.-360 ASTM D5197-16 17 .5.7.26 ,15C.7.27 ,9,.7.28 ,.8.8.1 .,10-(a)N2 (b)-ASTM D5197-16 18 ,.6 8.2 ,II D1193.8.3 2,4-(),-.8.4-.8.5 ,60%,1,51.8.6 ,36,5 38%,1,19.8.7,37-%().8.8 ,-().8.9 .8.10 .8.11,().8.12 ,().8.13,(
11、).9.5 ,.,-,-.,.6 ,.,.,.,BDH Ltd.,.,.,Inc.(USPC),.,.ASTM D5197-16 19 9.1 2,4-():,(500 ppm)/(.).9.1.1 ,200 1.9.1.2 1 40-60C.9.1.3 (40C),95%.9.1.4 ,.9.1.5 ,200 ,40-60C ,95%.9.1.6 ,.9.1.4.9.1.7 ,1 3,8-M 100 ,.10.2.4.6 ,.,.ASTM D5197-16 20 .-,.,.,.9.1.8 .9.1.7 0,025/-.,.9.1.9 ,200 ,.,.9.1.7,.10.2.3.9.1.1
12、0 ,25 .20-,.9.1.11 ,25 ,.-.9.1.12 ,.,.ASTM D5197-16 21 9.1.13 -.9.2 -:9.2.1 2-HCl,.-,2-HCl .9.2.2 -(166C)-.,.(,99%).9.2.3-,.9.3 -:9.3.1 -,.9.3.2 .-,.7 100/10 100 .,ASTM D5197-16 22 0,5 20/,.9.3.3 4C .9.4 -:8 .9.4.1 -:9.4.1.1 30 1000-,500 .9.4.1.2 1,0 HCl.9 -,.,.,.,0-10.9.4.1.3 10-20 .9.4.1.4 .9.1.9.
13、4.1.5 0,025/-,.9.4.2 :9.4.2.1 ,10-.5()5(b).ASTM D5197-16 23 9.4.2.2 ,10 .9.4.2.3 .10 ,.9.4.2.4 ,-,7 .9.4.2.5 ,7 .9.4.2.6 ,.9.4.2.7 .9.4.2.8 ,.5(b).-(,.9.4.2.9 9.4.2.15 ).,.9.4.2.9 (,0,642,5 ,-).9.4.2.10 ,.ASTM D5197-16 24 9.4.2.11 300 400/.9.4.2.12 .9.4.2.13 15 ,.9.4.2.14 .9.4.2.15 ,.10.10.1 :10.1.1
14、 ,.15C(.7.26).(.6.2).10.1.2 .(),.11 .,.ASTM D5197-16 25 ,.,.20%.10.1.3 ,.3().0,5 1,5/.(0,005 0,01/).75%-(100 200 HCHO).,.,.12 D3686 ,.10.1.4 ,.2,.,.ASTM D5197-16 26 ,.10.1.5 .,.-,.10.1.6 ,.,.,.10.1.7 .1,0/0,8/.10.1.8 ,.10.1.9 15C,ASTM D5197-16 27 -.10.1.10 .15%,.10.1.11 (),.-.4 C .14.13 ,.10.1.12 :(
15、1):QA-,/;Q1,Q2,.Qn-,;n-.ASTM D5197-16 28 10.1.13 :(2):Vm-,;T2-,;T1-,;T2-T1-,;QA-,/.10.1.14 (Vm),25C 101,3,:(3):Vs-,25C 101,3;Vm-,;PA-,;tA-,C.10.2 :10.2.1 4C .5000 .7 :(7):n-();tr-;W1/2-.12.1.2.2 10%1/.0,5/25%.7%.8.12.1.3 7 ,.E682.-(/)ASTM D5197-16 40 ,10%,.(),.,.,.9.1,.,(),.12.1.4 ,.,.,15-25%,.100%-
16、(1).,().,.,.12.1.5,.ASTM D5197-16 41 13.8 13.1 :.,(),.4.A :0,13 0,18 0,12 0,06(%)46 70 47 44 n 33 33 23 8 B:%(%)89,0(6,02)92,6(13,8)108,7(32,6)114,7(36,1)97,2(3,56)97,8(7,98)100,9(13,2)123,5(10,4)97,5(2,15)102,2(6,93)100,1(6,77)120,0(8,21)n 12 13 12 14 :5,92 7,99 0,522 0,288%12,6 16,54 26,4 19,4 n 31 32 32 17 A -.B 0,5,5 10 ,.13.2 55 105,.,1500 8 ASTM International RR:D22-1024.ASTM :serviceastm.org.ASTM D5197-16 42 (UATP),14 .13.3 45 -()0,85%.13.4 -,10,9%.13.5 16 ,250 -,30 -,13 ,.,.4.1.,-.4.22 -