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ASTM_D_3157_-_05_2015.pdf

1、Designation:D315705(Reapproved 2015)Standard Test Method forRubber from Natural SourcesColor1This standard is issued under the fixed designation D3157;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number

2、 in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope1.1 This test method covers a method of classifying thecolor of raw rubber according to a standard color scale.1.2 The values stated in SI units are

3、to be regarded as thestandard.The values given in parentheses are for informationonly.1.3 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and

4、determine the applica-bility of regulatory limitations prior to use.2.Referenced Documents2.1 ASTM Standards:2D926 Test Method for Rubber PropertyPlasticity andRecovery(Parallel Plate Method)D1485 Practice for Rubber from Natural SourcesSampling and Sample PreparationD3182 Practice for RubberMateria

5、ls,Equipment,and Pro-cedures for Mixing Standard Compounds and PreparingStandard Vulcanized SheetsD3767 Practice for RubberMeasurement of Dimensions3.Summary of Test Method3.1 The raw rubber is prepared in the form of a molded diskof specified thickness,and the color of this disk is comparedand matc

6、hed as closely as possible with that of colored glassdisks referred to as standard glasses.The standard glasses usedare calibrated according to the intensity of their amber color.Occasionally the color of the rubber cannot be matched due tothe presence of strong yellow,green,or gray tints.Colormatch

7、ing is carried out under diffuse daylight illuminationagainst a matt white background,preferably by use of acomparator that suitably locates and shrouds the test specimenand standard glass.The standard glasses used are calibratedaccording to the intensity of their color to provide a color indexscale

8、 in which higher index values correspond to deeper color.4.Significance and Use4.1 Color of material rubber is of importance in compoundswhere product color is determined by the color of the rawrubber.5.Apparatus5.1 Laboratory Mill,as described in Practice D3182.5.2 Hydraulic Press,capable of giving

9、 a molding pressureof not less than 3.5 MPa(500 psi)over the platen surface andplaten temperatures of 150 6 3C(302 6 5F).5.3 Mold,stainless steel or aluminum,1.60 6 0.05 mm(0.063 6 0.002 in.)thick having holes approximately 14 mm(0.55 in.)in diameter in accordance with Fig.1.5.4 Mold Plates,two,of s

10、imilar material,1.60 6 0.05 mm(0.063 6 0.002 in.)in thickness.5.5 Comparator or Standard Glass Disks3Standard col-ored glasses with color index scale:1 to 5 in half-integral stepsand 5 to 16 in integral steps.5.6 Test Specimen Cutting Die,as described in Test MethodD926.5.7 Thickness Gage,capable of

11、 measuring the test specimento the nearest 0.02 mm(0.001 in.)in accordance with PracticeD3767,Procedure A1.5.8 Polyester or Cellulose Film,transparent of 0.025-mm(0.001-in.)thickness.6.Sampling6.1 Sampling shall be carried out in accordance with TestMethods D1485.1This test method is under the juris

12、diction of ASTM Committee D11 on Rubberand is the direct responsibility of Subcommittee D11.22 on Natural Rubber.Current edition approved Aug.1,2015.Published September 2015.Originallyapproved in 1973.Last previous edition approved in 2010 as D3157 05(2010)1.DOI:10.1520/D3157-05R15.2For referenced A

13、STM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe ASTM website.3Lovibond Comparator disks 4/19A for 1 to 5 units and 4/19B for 5 to 16 unitshave b

14、een found to be satisfactory.The sole source of supply of the LovibondComparator disks known to the committee at this time is Wilkens Anderson Co.(WACO),4525 W.Division Street,Chicago,Illinois 60651,.Ifyou are aware of alternative suppliers,please provide this information to ASTMInternational Headqu

15、arters.Your comments will receive careful consideration at ameeting of the responsible technical committee,1which you may attend.Copyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United States1 7.Test Specimen and Sample7.1 Homogenize the piece to be test

16、ed in accordance withTest Methods D1485,omitting the weighing procedure unlessthat is required for other tests.7.2 Take a test portion of about 30 g from the homogenizedpiece and pass not more than three times(doubling the sheetbetween passes)between the mill rolls at room temperaturewith the nip adjusted so that the final sheet thickness is 1.6 to1.8 mm(0.06 to 0.07 in.).Immediately double the sheet,whichshould be uniform in texture and free of holes,and press thetwo halves lightly together by

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