1、:D 384907(2011.)STANDARD TEST METHOD FOR CARBON BLACK MORPHOLOGICAL CHARACTERIZATION OF CARBON BLACK USING ELECTRON MICROSCOPY ():2054-13/ASTM :16.07.2013 2013 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru (ASTM International)100 rr Harbor Drive,W
2、est Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor D
3、rive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any
4、Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 3849-07(2011):D 384907(2011.)1 D 3849;,.().1.1.1 .(),().1.2,.1.3 1 ASTM D24 D24.81 .1 2011.2012.1980.2007.D 3849-07.DOI:10.1520/D3849-07R11.1ASTM D
5、3849-07(2011),.,.2.2.1 ASTM:2 D 6556 3.3.1:3.1.1:3.1.1.1 ,;.;.3.1.1.2 ;.;.3.1.1.3 ,3-20 (25 150 103 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.2ASTM D 3849-07(2011).).,.3.1.1.4 ,.-,.3.1.2 ,:3.1.2.1 (A).3.1.2.2 (P).3.1.2.3 (V).3.1.3 :3.1.3.1 ,.OFF ON,ON.,.3.1.3.2 ,.ON OF
6、F,OFF.,.3ASTM D 3849-07(2011)3.1.3.3 ,-,.3.1.3.4 ,.4.4.1 ,.,.(),.().()().4.2 ,.5.5.1 ,1,0 .,4ASTM D 3849-07(2011),.60 120.(),.5.2 ,()(TM),640 480 ,./,.5.3 .5.4 ,.1,3 (1 105 .).5.5 ,.5.6 ,30%.5ASTM D 3849-07(2011)5.7 ,0,5.5.8 ,800-900C ,.5.9,150 1000C .5.10 ,3,1.5.11 .5.12 ,25 75.5.13 ,75 10,4 3,0,5-
7、,.5.14 (),225,1.5.15 ,.5.16 ,40 3,.5.17 ,3,111.5.18 ,.5.19 ,3,200 300.A1.5.20 ,1 2.5.21,.5.22,V-2 12,5 .5.23 .5.24 ,.5.25 ,98 15 .5.26,(15000 20000/)6ASTM D 3849-07(2011)75 10.5.27,2000 3.6.6.1,.6.2 (THF),.6.3 1,2-,.6.4,.6.5 ,15/95.6.6 ().6.7 ().7.7.1 ():7.1.1 8 10 ,1 3 (THF).1 ,.N100 N200 ,.7.1.2 ;
8、.,.7.1.3 3-5.7ASTM D 3849-07(2011).10 1 .1 N-220 7.1.4 ,1 3 .,.7.1.5 .,.N700-N900 .8ASTM D 3849-07(2011),.1 3.,1 3 .2 .7.1.6 ().12.1 .,30%.7.1.7 TM,(),.(550C),.7.1.8 (SBR)N-220 and N-774 .1 2.7.2 ():7.2.1 5 10 30-3 20 3 ().9ASTM D 3849-07(2011)3 ,.N100 N200 ,.7.2.2 ,.7.2.3 2,5 40-50 10.4 ,.10 1 .2 N
9、-774 7.2.4 (2 4 3)20 3 .10ASTM D 3849-07(2011)7.2.5 .,.N700 N900 .7.2.6 ,.20 3.7.2.5.5 .7.2.7 ,().12.1 .(35%,).7.2.8 .(,.),.7.2.6 .7.2.7.11ASTM D 3849-07(2011)7.3 ,:7.3.1 (1 3).7.3.2 5 10 ,.,.7.3.3 ,.-;.,5%,.,.7.3.4 .,1 3 (THF).7.3.5 .7.1.2 7.1.8.7.4 ():7.4.1 ,;,.12ASTM D 3849-07(2011)7.4.2 :7.4.2.1
10、 Farrel Tecno Lab Polymill 110P .7.4.2.2 ,76C,-66C,.7.4.2.3 0,2 20/.7.4.2.4 :()N100-N300(25%-)37,5 82,5 30,0 N500-N900(40%-)60,0 66,0 24,0 7.4.2.5 ,.7.4.2.6 ,2.7.4.2.7 ,.25%-10C ,20C 40%-.7.4.2.8 ,.7.4.2.9 ,(),10.10 13ASTM D 3849-07(2011),1-.7.4.2.10 ,.7.4.2.11 5-.,1-.7.4.2.12 ,.7.4.2.13 .7.4.2.11 5
11、-20.7.4.2.14 .7.4.3 25 ,1 3 ().7.4.4 ,.7.1()7.2().8.8.1 .8.2 .,.,14ASTM D 3849-07(2011),(,).,2K 2K .()(/)14 21 1,5 2,0 22 26 2,0 2,5 27 37 2,5 3,0 38 49 3,0 4,0 50 62 4,0 5,0 63 100 5,0 6,0 101 199 6,0 12,0 200 400 12,0 20,0 8.2.1 -,EMSA,STSA.(.D 6556.)8.2.2 ,.8.3 ,2160/.8.4 /2/().9.9.1 ,.9.2 .9.3 1
12、5ASTM D 3849-07(2011),.,.9.4 .,.,2000.9.5 :9.5.1 ,.9.5.2 ,.9.5.3 ,.,(1 1-2.),.,.,.8.2,16ASTM D 3849-07(2011),50.,.9.5.4 (,),.,./.9.6 ,.,.9.7 ,(A)(P).10.10.1 :10.1.1 :3 A=(2),P=().10.1.2 :D=-()=(4 A/)1/2,=13,092(P2/A)0.92(,0.4,=0,4),3 ,2.17ASTM D 3849-07(2011)dp=()=/,VA=(3)=(8/3)A2/P,VP=(3)=dp3/6,n=V
13、A/VP.10.2 :10.2.1 :nt=n ,m=()=(n*dp)/nt,sd=()=n(dp m)2/nt l)1/2,wm=()=(n*dp4)/(n*dp3),hi=wm/m,dsm=()=(n*dp3)/(n*dp2),EMSA=(2/)=6000/(*dsm)(:=1,8/3;),Nt=,M=()=D/Nt,SD=()=(D M)2/(Nt 1)1/2,WM=()=D4/D3,HI=WM/M.11.11.1 :11.1.1 (,),18ASTM D 3849-07(2011)11.1.2 ,11.1.3 ,m(),11.1.4 ,wm(),11.1.5 ,hi,11.1.6 ,
14、EMSA(2/).11.2 :11.2.1 (),11.2.2 ,11.2.3 ,m(),11.2.4 ,WM(),11.2.5 ,HI.12.12.1;.()A1.A1.1 .,.0,25%-1,2-.19ASTM D 3849-07(2011)(1 2).A1.2 .().40 .A1.3 ,180.,.3 4.A1.4 ,.,1,3 .,.100 .,.A1.5 10.,.20ASTM D 3849-07(2011)21 ,.,20 (150 103 .).1500.,().13 20 (100 150 103 .)3.ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).ASTM(www.astm.org/COPYRIGHT/).