1、OCT 33905-2016npeAncnoBneLenn,ocHoBHble npnhyunbi n ocHoBHo nopagok npoBegeHng pa6ot no MexrocyAapctBeHHO cTaH-AapTn3aunn ycTaHoBneHbi B OCT 1.0-2015 MexrocyAapcTBeHHaA ccTeMa cTaHAapTn3aunn.OcHOBHblenonokeHnA n OCT 1.2-2015 MexrocyAapcTBeHHaA ccTeMa cTaHAapTn3aunn.CTaHAapTbi Mexrocy-AapcTBeHHble,np
2、aBnna n pekomeHAaunn no MexrocyAapcTBeHHo cTaHgapTn3aunn.paBnna pa3pa6oTkn,nHATA,HOBneHA OTMeHbICBeAeHA o cTaHAapTe1 NOAFOTOBNEH OTKpbiTbiM aKynoHepHbIM o6weCTBoM Bcepoccnckni Hay4Ho-nccnegoBatenb-cKu nHcTutyt no nepepa6otke Hetu(OAO BHM HI)Ha ocHoBe co6cTBeHHoTo nepeBoga Ha pycckni3bK aHo3b4Ho Bepc
3、 cTaHapTa,yka3aHHoro B nyHkTe 52 BHECEH MexrocyAapcTBeHHbIM TeXHn4ecKnM KOMnTeToM no cTaHAapTn3aynn MTK 31 HeTAHbleTonnBa cMa3o4Hble MaTepanbl3 NIPMHAT MexrocyAapcTBeHHbIM CoBeToM no cTaHAaptn3aunn,Metponornn n ceptn中nKaunn(npoToon oT 22 Ho6p 2016 r.N 93-)3a npHATe nporonocoBann:KpaTKoe HanMeHoBaHne
4、 cTpaHbIKoA cTpaHbICokpaueHHoe HanMeHoBaHe HauMoHanbHoro opraHano MK(MCO 3166)004-97no MK(MCO 3166)004-97no cTaHapTM3auMApMeHMAAMMH3KOHOMMKM Pecny6nK ApMeHBenapycbBYToccTaHAapT Pecny6nnKn enapycbpy3GEpy3cTaHAapTKpr3MKGKbiprbi3cTaHAapTPoCCMARUPoccTaHAapTTaAKCTaHTaAKnKcTaHAapTy36eKncTaH品y3cTaHAapT4 pu
5、ka3oM egepanbHoro areHTctBa no texHn4eckoMy perynnpoBaHnio n Metponornn of 4 anpeng2017 r.Ne 259-cT MexrocyAapctBeHHbi cTaHAapt FOCT 33905-2016 BBeAeH B AectBne B KayectBeHa,oHanbHoro cTaHAapTa Pocccko egepaunn c 1 on 2018 r.5 Hactown ctaHgapt AeHtn4eh ctaHAapty ASTM D 3231-13 CtaHAapthbi MetoA onpe
6、geneHnApocpopa B 6eH3nHe(Standard test method for phosphorus in gasoline,IDT).CTaHAapT pa3pa6oTaH noAKoMTeTOM D02.03 neMeHTHbI aHan3 TeXH4ecKoro KOMTeTaASTM D02 HeTenpoAyKTbI cMa304Hble MaTepanbI.HanMeHoBaHne HacToquero cTaHAapTa 3MeHeHO OTHOcnTenbHO HanMeHoBaHng yKa3aHHoro cTaH-Aapta ASTM An npuBeA
7、eHnA B cooTBeTctBne cOCT 1.5(noApa3gen 3.6).ipu npnMeHeHnn HacTowero ctaHAapta pekoMeHAyeTcA ucnonb3oBaTb BMecTo cCbIno4HbIX cTaH-AapToB ASTM cOoTBeTcTByloune M MexrocyAapcTBeHHble cTaHAapTbl,cBeAeHnA o KoTopbix npnBegeHbIB AononHTenbHoM npnoeH AA6 BBEAEH BNEPBbIEMHpopMauu o6 u3MeHeHuAx k HacmoeMy c
8、maHdapmy ny6nukyemc e exe2odHoM uHpopMauuoH-HoM yKa3amene HauuoHanLHbe cmaHdapmbi,a meKcm u3MeHeHuu u nonpaok-eekeMecHOM uHop-MaquOHHOM yka3amene HauuoHanLHbe cmaHdapmbi.B cnyuae nepecMompa(3aMeHbi)unu omMeHbIHacmowe2o cmaHdapma coomeemcmeyiouwee yeedoMneHue 6ydem ony6nukoeaHo e exeMecA4HOMuHpopMauO
9、HHOM yKa3amene HauuoHanLHbie cmaHOapmb.Coomeemcmeyloa uHpopMayu,yee-doMneHue u mekcmbI pa3Meuwalomc makke e uHpopMauOHHou cucmeMe obwe2o nonL3oaHu Ha ou-quanbHoM cauime PedepanLHo2o a2eHmcmea no mexHu4eckoMy pezynupoeaHuio u Memponozuu e cemuMHmepHem(www.gost.ru)CTaH,AapTnHopM,2017B Poccnicko Pegepa
10、ynn hacton ctaHAapt he Moket 6bitb nohoctbio unn yactnyho Bocnpon3Be-AeH,TupaxnpoBaH n pacnpocTpaHeH B ka4ectBe opnuanbHoro 3gaHng 6e3 pa3peweHng OeAepanbHoroareHTcTBa no TexHneckoMy perynpoBaHo n MeTponorn0CT33905-20166.3 PacTBop MonnonaTa aMMOHNA(npenynpexkneHne-npn ropeHwn MokeT BblnenATb AOBNTbI
11、N ra3.Pa3npaxkaeT koxky n rna3aBpeneH Ana 3nopoBba npn nonanaHwn BHyTpb.)(npeaynpexneHne-B AononHeHne K ApyrnM npeAocTo-poxKHOCTAM npl nobaBneHNn KOHueHTpnpoBaHHoN cepHoN KNCnOTbI K Bone cnenyeT Ncnonb3oBaTb Macky nnMua,pe3WHOBble nepyaTkn n pe3WHoBbin dapTyk).B nabopaTopHbln cTakaH noMewaoT 500 CM3
12、 BonbI pa3-MewaloT B 6aHe c xono Hon Bonon,3aTeM npn HenpepblBHOM nepeMewnBaHnn MeaneHHo no6aBnaoT 225 CM3KOHueHTpMpoBaHHon cepHon KNcnoTbl(H2SO,C OTHOCNTenbHon nnoTHOCTbIO 1,84);nna N3MepeHNa 06beMOBKNAKOCTeN wcnonb3yOT rpanyupoBaHHble MepHble UNnNHApbl.3aTeM oxnaxknaloT pacTBop no TeMnepatypbloKpy
13、kalowen cpenbln no6aBnaoT 20r TeTparnapaTa Monn6naTa aMMoHna(NH)Mo,O24H2O.nepeMewn-BaloT Ao nonHoro pacTBopeHna nepeHOCaT B MepHyio Kon6y BMeCTNMOCTblo 1000 CM3.LoBoAaT pacTBopO MeTKN BODON.6.4 PacTBop cynboara rnApa3nHaPacTBopAoT 1,5 r cynboaTa rmapa3MHa(N,Ha HSO)(npeAynpexneHne-KaHueporeH)B 1 AM3B
14、OAbl,13MepeHHon rpanynpoBaHHbIM uNnNHApOM.(npepynpexneHne-PacTBop He cTa6nneH.Ero cneay-eT xpaHNTb nnoTHo 3akynopeHHbIM,B 3awnweHHOM OT Bo3neNCTBNA CBeTa MecTe.)CpoK xpaHeHna pacTBO-pa-He bonee Tpex Henenb.6.5 PeaKTNB MonnonaT-rMApa3NHB MepHyio Kon6y BMecTMMOCTbIO 100 CM3 noMewaloT npn6nn3nTenbHo 50
15、 CM3 BoAbl,3aTeM nnneTKonBHOCAT 25 CM3 pacTBopa MonnonaTa aMMOHNA,nobaBnAiOT nwneTKoN 10 cM3 pacTBopa N,H.HSO WAOBODATBO ON o MeTKN.n p MM e y a H M e 3-naHHbin peaKTnB roTOBAT HenocpencTBeHHo nepen ncnonb3oBaHneM,nockonbky OHHecTa6nneH n gonxeH 6blTb ncnonb3oBaH B TeueHwe 44.Ha kaxknoe onpeneneHne(
16、BKnoua xonocToM onblT)wcnonb3yIOT50cMpeakTnBa.6.6 CTaHAapTHbIN NCXoAHbIN pacTBop docdopa(1,00 Mr P/CM3)CywaT 34 B cywnnbHOM ukadpy npn TeMnepaType oT 105 C Ao 110 C(OT 221 F Ao 230 F)npn6nw3n-TenbHo 5r AnrnapodocdaTa kanna(KH,PO).B MepHyio Kon6y BMecTNMOCTbto 1000 CM3 noMewaloT 150 CM3N3MepeHHon rpa
17、nynpoBaHHbIM uNNNHApoM pa36aBneHHon cepHon KncnoTbl(6.8),BHOCAT(4,393 0,002)rcyxoro KH2PO n nepeMewnBaloT o pacTBopeHNa.AOBOAAT o MeTKn BoAon.6.7 CTaHnapTHbIN pacTBop docdpopa(10,0 MKr P/CM3)nepeHoCaT nwneTkoN 10 CM3 wCXoAHoro cTaHAapTHoro pacTBopa coccpopa B MepHylo Kon6y BMecTn-MOCTbIO 1000 CM3M A
18、OBOAAT Ao MeTKN BOAON.6.8 Pa36aBneHHaa cepHaa kncnoTa(1 yacTb H2SO 10 yacTen BOAbI)(npenynpexneHne KoHueHTpnpoBaHHaa cepHaa KncnoTa Bbl3blBaeT cepbe3Hble oxKorN.CnnbHbINoKncnNTenb.)(npeAynpexneHne-B AononHeHne K ApyrnM npenocTopoxHOCTaM npn no6aBneHnn KOH-LeHTpMpoBaHHon cepHon KMcnoTbl K Bone cnenye
19、T wcnonb3oBaTb Macky nna nMua,pe3wHoBble nepyaTknpe3WHOBbin dapTyK.)B nabopaTopHbin cTakaH,conepxawnn 1 AM3 BoAbl n pa3MeweHHbln B 6aHe c xonogHonBonoN,c noMowblo rpanynpoBaHHoro unnNHapa MenneHHo,npn HenpepblBHoM nepeMewnBaHnn,no6aBnAOT100 CM3 H2SO(OTHOCMTenbHaa nnoTHOCTb-1,84).6.9 OKcnA UNHKa(npeA
20、ynpexneHne-CM.6.8.)(npeAynpexneHne-Bbicoka HacbinHaa nnoTHOCTb oKcnna UNHKaMoxeT npnBecTn K pacnbineHwlo.nnoTHOCTb npw6nn3nTenbHo 0,5 r/CM3 6bina np3HaHa yAoBneTBopnTenb-HoM.）6.10 06pa3ubI KoHTpona KayecTBa(QC)O6pa3ubl QC npeanoyTnTenbHo DonKHbl 6blTb npeAcTaBnTenbHblMN CTa6wnbHblMN o6pa3uaMn OAHorOWnN HeckonbKnx aHanv3npyeMblX KNAKNX HecTenponyKToB.O6pa3ubl QC MoryT 6bITb wcnonb3oBaHblnpoBepKn OCToBepHocTM pe3ynbTaToB npouenypbl wcnblTaHna(CM.pa3nen 11).7O6 op npo67.1 OT6op npo6-no ASTMD 4057.7.2 Vcnonb3yIOT Ta6nnuy 1 Ana Bbl6opa o6beMa o6pa3ua.3