1、中EAEPAJbHOE ATEHTCTBONO TEXHYECKOMY PErYJPOBAHIO METPOJOFOCT PHAUOHAJbHbICTAHAAPT56679-POCCMCKO中EAEPAU2015KOMNO3TbI NOMMEPHbIEMeToA onpegeneHn nycToTM3aHne onunanbHoeMocKBaCTaHAapTMHOpM2016FOCTP56679-2015HAUNOHAnbHbI CTAHAAPT POCCCKO EAEPAUKOMNO3TbI nOJMMEPHbIEMeTo onpegeneHA nycToTPolymer composite
2、s.Method for determination of voidsAaTa BBeAeH-2017-01-011 06nacTb npMeHeHCTaHAapt pacnpocTpaHgeTcA ha nonnMepHble KoMno3nTbi n ycTaHaBnnBaet MeTog onpegeneHnAnycroT.HacTo山 cTaHAapt He pacnpocTpaHeTcA Ha nonnMepHble KOMnO3TbI,MaTpnya KoTopbix cropaeTHe nonHOCTbo np CraH.2 HopMaTBHble ccbInKnB HacToA
3、eM cTaHgapte ncnonb3oBaHbi HOpMaTBHble ccbinkn Ha cneAyioune cTaHAapTbi:OCT 6507 MukpoMempb.TexHu4eckue ycnoeuOCT12423-2013(MCO 291:2008)lnacmMaccbi.Ycno6u KoHuuuoHupo6aHuA u ucnbimaHuAo6pa3uoe(npo6)OCT 1513969 nacmMaccbi.Memobi onpedeneHus nnomHocmu(06beMHO Maccbi)OCT P 53228 Becbi HeaemoMamu4ecko2
4、o deicmeuR.Yacmb 1.Memponozu4eckue u mexHu4eckuempeboeaHbimaHu p u M e 4 a H n e-p nonb3oBaHnn HacTOALM cTaHgapToM yenecoo6pa3Ho npoBepNTL AeNcTBe cCLIno4HbIXcTaHapTOB B MHOpMaLOHHon CcTeMe oowero nonb3oBaHA Ha oMManbHoM canTe egepanbHoro areHTcTBano TexHMeckoMy perynnpoBaHio n MeTponorn B ceT VHTep
5、HeT un no exeroAHoMy HpopMaynOHHoMy yKa3aTenioHaoHanbHble cTaHgapTbi,KoTopbin onyonnKoBaH no cocTOHnio Ha 1 HBapg Tekywero roga,n no BbinyckaMexemecHoro nHpopMayoHHoro yxa3aTeng HayOHanLHble cTaHAapTbi 3a Tekyn rog Ecnn 3aMeHeH ccbIno4HbicTaHgapt,Ha KoTopbin AaHa HeAaTnpoBaHHag ccbinKa,To peKoMeHAye
6、TcA cnonL3oBatb AeNcTByowyio Bepcno 3TorocTaHgapTa c y4eToM BCeX BHeceHHbIX B AaHHyO BepcO n3MeHeH.Ecn 3aMeHeH ccbIno4Hbi cTaHAapt,ha KoTopbiAaHa AatpoBaHHa ccbinKa,To peKoMeHAyeTc cnonb3oBaTb BepCMo 3Toro cTaHAapTa c yKa3aHHbIM BbIWe ToAoMyTBepxAeHnA(npHAt).Ecnn nocne yTBepxAeHnA HacToguero cTaHAap
7、Ta B ccbinouHbIN cTaHAapt,ha KoTOpbiN AaHaAaTpoBaHHa ccbinKa,BHeceHo 3MeHeHe,3aTparnBalouee nonoKeHMe,Ha KoTopoe AaHa ccbinKa,TO 3TOnonokeHe pekoMeHAyeTcA npMeHATb 6e3 y4eTa AaHHoro W3MeHeHA.Ecn ccbino4HbiN cTaHAapt OTMeHeH 6e33aMeHbl,To nonoxeHe,B KoTopoM gaHa ccbinKa Ha Hero,peKoMeHAyetca npnMeHAt
8、b B yactn,He 3atparnBaowen 3Tyccbinky.3 CyuHOCTb MeToAaMeTog 3akno4aetcA B onpegeneHnM MaccoBoro cogepaHMA B nonMepHOM KOMnO3MTeapMpyowero HanonHnTeng cMonbi,a Takke nnoTHocT apMnpyowero HanonHnTeng,oTBepAeHHonCMOnbI KOMno3Ta B LenoM.Ha ocHoBe nony4eHHbIX gaHHbIX paccTbIBaoT cogepKaHMe nycTOT BnonMe
9、pHOM KoMno3Te.门p u me 4a Hne-Kak npaBnno,AonycTuMbiM c4nTaetcA Hann4ue nyctot B nonnMepHoM KoMno3ute Ao 1%no Macce.4 06opyAoBaHne4.1 MnKpoMeTp no FOCT 6507 c norpewHOCTbIO 3MepeHA He 6onee 0,01 MM.4.2 Becbi aHannTneckne no FOCT P 53228 c norpewHOCTbi 3MepeHnA He 6onee 0,0001 r.M3AaHne opuanbHoer0CTP
10、56679-20155 nonroToBKa K npoBeneHno NcnbITaHnM5.1 nogroToBka 06pa3uoBO6pa3ubl n onpeneneHna nnoTHOCTM CMOnbI N3roTaBnNBaloT M3 OTBepxneHHON CMonbl,npnMeHeHHON B MccneayeMOM nonnMepHOM KOMno3MTe.ycnoBNA OTBepxkneHNA nonXKHbI COOTBeTCTBOBaTbyCnoBNAM N3rOToBneHNA nonMMepHoro KOMno3NTa.O6pa3ubl ana onpe
11、neneHna nnoTHOCTN CMonbI,apMnpylowero HanonHnTena n nonnMepHoroKOMnO3NTa nonKHbI NMeTb poBHyIO,cnnowHyo noBepXHOCTb.B 3aBNCNMOCTN OT npNMeHeHHoro MeTona onpeneneHna nnoTHOCTn(CM.6.2)K 06pa3uaMnpenbBnOT ononHnTenbHble Tpe6oBaHna:no MeTony A-06pa3ubl AOnxKHbl COoTBeTCTBOBaTb Tpe6oBaHMAM TOCT 15139-69(
12、nyHKTbI 1.2,1.6M3.2.1);no MeToAy 6-COoTBeTCTBOBaTb Tpe60BaHMAM TOCT 15139-69(nyHKTbI 1.2,1.6 n 6.2.1);-no MeToAy B COOTBeTCTBOBaTb Tpe6oBaHMAM TOCT 15139-69(nyHKT 1.6),a Takke MeTbopMy,npn KoTopon BO3MOXKeH TOYHbIN pacyeT oobeMa,M obbeM He MeHee 2 CM5.2 KoHANUNOHNpoBaHnenepea ncnblTaHneM 06pa3ubl KO
13、HAMyMoHupyIoT npn CTaHnapTHon aTMocoepe 23/50 no TOCT 12423He MeHee 40 4.6 npoBeneHne ncnbITaHnn6.1O6山e nonoxeHn:9VcnblTaHna npoBOAAT npn ycnoBMax,yCTaHoBneHHbIX B HopMaTMBHbIX AoKyMeHTax wnM TexHnyecKonAoKyMeHTaunen Ha M3nenne.Ecnn B HMX He yCTaHoBneHbl ycnoBna npoBeneHna ncnblTaHni,To ncnbITaHnanp
14、oBOAAT npn cTaHnapTHoN aTMocoepe 23/50 no OCT 12423.6.2 OnpeneneHne nnoTHOCTn CMonbl n nonnMepHoro KoMno3nTannoTHOCTb onpenenaoT OHNM N3 Tpex cnoco6oB.6.2.1 MeTOn A(MeTon rnapocTaTnyeckoro B3BewnBaHna)nnoTHOCTb 06pa3ya onpenenaoT no rOCT 15139-69(pa3nen 3).6.2.2 MeTon B(MeTon rpanneHTHoN KonoHKn)nno
15、THOCTb o6pa3ua onpenenaoT no rOCT 15139-69(pa3nen 6).6.2.3 MeTon B(MeTon 06Mepa n B3BeunBaHna)6.2.3.1 M3MepaOT nMHeNHble pa3mepbl 06pa3ua MnkpoMeTpoM C TOYHOCTbIO AO 0,01 MMpaccynTblBaloT ero 06beM B Ky6nyecKnx caHTnMeTpax.V3MepeHna Kaxnoro pa3mepa npoBonaT no TopuaM o6pa3ua(HanpnMep,an o6pa3ua nMer
16、oweronpaMoyronbHyio dopMy n wecTb rpaHen 3MepeHne npon3BOAAT B 12 Toukax)n B pacuete ncnonb3yIOTcpenHee 3HayeHne.6.2.3.2 OnpenenoT Maccy 06pa3ya B3BewnBaHneM Ha Becax c TOYHOCTbO Ao 0,0001 r.6.2.3.3 nnoTHOCTb 06pa3ua p,r/CM,BbluncnaOT no copMynemp=(1)raem一Macca o6pa3a,r;v一o6beMo6pa3ua,cM36.3 Onpenen
17、eHne nnoTHOCTn apMnpylowero HanonHnTennnoTHOCTb apMupyiowero HanonHnren onpenenoT no MeTony A(CM.6.2.1)6.4 ConepxkaHne CMonbI B nonnMepHOM KOMno3NTeConepxaHne CMonbl B nonMMepHOM KOMnO3NTe pacCynTblBaOT B COOTBeTCTBMN C npwnoxeHneM A.noTepn npn cxKnraHnn,onpenengeMble 3TMM MeTOAOM,6yayT paBHbl conep
18、xkaHnIo CMonbI B nonnMepHOMKOMnO3NTe7 06pa6oTka pe3ynbTaToB7.1 ConepxaHne nyCTOT B nonnMepHOM KOMno3MTe MoXeT 6bITb paccynTaHo AByMa cnoco6aMn:CnpoMexyTOuHbIM pacueTOM TeopeTnyeckon nnoTHOCTM nonMMepHoro KOMno3MTa(cnoco6 A)n 6e3npoMexKyTouHoro pacueTa TeopeTnueckon nnoTHOCTM nonMMepHoro KoMno3MTa(cnoco6 B).2