1、中EAEPAbHOE ATEHTCTBOnO TEXHMYECKOMY PEryMPOBAHO M METPONOHAUOHAnbHbIFOCT PCTAHAAPT57040POCCMCKOW2016中EAEPATA3bl yEBOAOPOAHbIE CKKEHHbIEOnpegeneHne ocTatkaM3AaHne opnnanbHoeMocKBaGnCTaHAapTHopM2016f0CTP57040-2016npeancnoBne1 nOOTOBNEH enepanbHblM rocynapcTBeHHbIM yHMTapHblM npeanpnaTneM Bcepoccnncknn
2、HayuHo-nccnenoBatenbCKnn WHCTNTyT CTaHAapTn3aunn Cblpba,MaTepnanoB n BewecTB(Tyn&BHVMCMT)Ha oCHOBe Co6cTBeHHoro nepeBona Ha pyccKnN 93blK aHrno93blYHON BepcnN cTaHnapta,yka3aHHoro BnyHKTe 42 BHECEH enepanbHblM areHTCTBOM no TexHNyecKoMy perynupoBaHnio n MeTponornn(PoccTaH-napT)3 yTBEPKAEH MBBEDEH B
3、DENCTBVE Npnka3oM enepanbHoro areHTCTBa no TexHwueckoMy pery-nupoBaHnlo M MeTponorn oT 5 ceHTa6pa 2016r.No 1041-CT4 HacToauni CTaHnapT nneHTw4eH cTaHnapTy ACTM2158-11&CTaHnapTHbIn MeTon onpeneneHnaoCTaTKOB B cKnxeHHblx yrneBogopoHbix ra3axASTM D 2158-11 Standard test method for residues inliquefied
4、petroleum(LP)gases,IDT.HaNMeHoBaHne HacTogwero cTaHnapta N3MeHeHO OTHOCNTenbHO HaNMeHoBaHNa yKa3aHHoro cTaHnap-Ta ana npnBeneHna B CooTBeTCTBNe crOCT P 1.5-2012(nyHKT 3.5).npn npNMeHeHWn HacToawero cTaHnapta pekoMeHnyeTca wcnonb3oBaTb BMecTo ccbInoyHbIX CTaHnap-TOB ACTM COOTBeTCTBylowNe WM HauNoHanb
5、Hble N MexkrocynapcTBeHHble cTaHnapTbl,cBeneHnA O KOTopbIXnpnBeneHbl B nononHNTenbHOM npnnoxkeHNN A5 BBENEH BNEPBbIEnpaeuna npuMeHeHua Hacmoawe2o cmaHdapma ycmaHoeneHbl 8 cmambe 26 edepanbHo2o 3aKoHaOcmaHoapmu3auuue Poccuuckou edepauuux.MHcbopMauua o6 u3MeHeHuax K HacmoaweMy cmaHoapmynyonukyemca 6 e
6、xkeaodHOM(no cocmogHulo Ha 1 AHBapa mekywe2o 2oda)UHobopMauuoHHOM yka3ameneHauuOHanbHble cmaHdapmbl,ao中uuuanbHblu mekcm u.3 MeHeHuu u nonpaBok-B exkeMecsYHOM UH中op-MauuoHHOM yka3amene HauuoHanbHble cmaHdapmbl.B cnyuae nepecMompa(3aMeHbl)unu omMeHbIHacmoawe2o cmaHdapma coomeemcmeylowee yeedoMneHue by
7、dem onyonukoeaHo e onuxauweM BbinyckeexkeMeca4Ho20 UHobopMauuoHHo20 yka3amena HauuoHanbHble cmaHdapmbl.CoomeemcmeyiowaUHobopMauus,yeedoMneHue u mekcmbl pa3Mewaromca makke 6 UHobopMauuoHHou cucmeMe obwe2ononb306aHus-Ha oobuuuanbHOM caume edepanbHo2o a2eHmcmea no mexHuyeckoMy peaynupoeaHulo uMemponoau
8、u e cemu MHmepHem(www.gost.ru)CTaHnapTNH中opM,2016HacToawNn CTaHnapT He MoxKeT 6bITb nonHOCTblo wnn yacTNYHO BocnpoN3BeneH,TMpaxknpoBaH n pac-npocTpaHeH B KayecTBe oowuManbHoro 3naHNA 6e3 pa3peweHna enepanbHoro areHTCTBa no TexHNyecKo-My perynnpoBaHnio N MeTponornnFOCT P 57040-2016CoAepxaHne1 06nacTb
9、 npMeHeHA.2 HopMaTBHble ccbIK.3 TepMHb onpegeneHg.4 CyuHOCTb MeToAa.25 Ha3HaeHe n npuMeHeHe26 oMexn.27 Annapatypa.28 PeaKTBbl MaTepanbl59 OnacHble aKTopbl.510 ogroToBka annapaTypbi511 poBeeHne cnbiTaH612 poToon cnbiTaH.713 pe3OHHOCTb CMeweHne.7门punoxeHne X1(cnpaBo4Hoe)BbiuncneHne 3Ha4eHu noka3atene
10、R n O.8门pnnoxeHne AA(cpaBo4Hoe)CBegeHng o cooTBeTcTBnN ccbINo4HbIX cTaHAaptoB ACTM HanoHanbHbIMM MekrocyAapcTBeHHbIM cTaHAapTaM.9FOCTP 57040-2016HALMOHANbHbIM CTAHAAPT POCCMCKO EAEPAMA3bI yEBOAOPOAHbIE CEHHbIEOnpeAeneHe ocTaTkaLiquefied petroleum gases.Determination of residueAaTa BBeAeH-2017-07-011
11、 06nactb npnMeHeHng1.1 HacTowncTaHAaptycTaHaBnnBaeTonpegeneHneocTatka(nocTopOHHNX BewecTB),npncyTcTBy-lou(nx B cxnxeHHbix yrneBoAopoAHbix ra3ax(LPG),BbiBeTpnBaiownxc npu TeMnepatype Bbiwe 38 C.NocTo-pOHHMe BeLLecTBa MoryT 6bITb pactBOpeHbi B CKnxeHHoM yrneBogopoAHoM ra3e,HO B HeKoTopbix cnyagxa3bl M
12、oryT pa3genTbc.1.2 CxnxeHHble yrneBogopoAHble ra3bi,cogepxawue HekoTopbie npotuBoo6negeHnTeNbHble npcag-Kn,Moryt gaBatb own6o4hble pe3ynbtatbi npn ncnbitaHnn no HactoweMy cTaHAapty.1.3 YyBcTBntenbHoctb Metoga no HactoqeMy cTaHgapty He no3Bonget oeHNTb ynCtoTy n otcyt-CTBne BbicoKoKnnnx 3arp3HAiownX
13、BewecTB B LPG,BnnAownX Ha 3kcnnyataunio obopygoBaHng n cTon-MOCTb TexHM4eckoro o6cnyxnBaHng.B TaKoM cny4ae cnonb3yioT 6onee 4yBcTBnTenbHbI MeToA,obecne4nBaow o6HapyxeHne 6onee Hn3koro cogepxaHn pacTBopeHHbIX 3arp3HAOX BeecTB.1.4 lpeAocTepexeHne-PTyTb ABngeTcA onacHbIM MaTepnanoM,nopaxalownM ueHTpanb
14、HyoHepBHyo cucTeMy,nokn n neyeHb.PTyTb nu ee napbi onachbi An3opoBba n Bbi3biBaoT Koppo3nio Matep-anoB.CnegyeT co6niogaTb ocTopokHocTb npu pa6oTe cpTyTbio unpogyKTaMn,cogepxaunM pTyTb.lacnopt6e3onacHoctu(MSDS)u nogpo6Hag gononHnTenbhaA nHpopMalnA no 3aw(nte okpyxaiowe cpeAbi npuBe-geHa Ha canTe:www.
15、epa.gov/mercury/faq.htm.CnegyeT MeTb B BAy,4To npogaxa pTyTn/nn pTyTbcogep-Kawx npoAykToB MOeT 6bITb 3anpeweHa 3aKoHOM.1.5 3Ha4eHng,npnBegeHHbie B eAnHnyax CM,paccMaTpnBaoT kaK cTaHAapTHble.3Ha4eHnA B cko6kaxnpBeAeHbl Tonbko Ang HopMaun.1.6 B HacToAueM cTaHgapte He npeAycMoTpeHo paccMoTpeHMe Bcex Bo
16、npocoB o6ecne4eHnA 6e3onac-HOCTM,cBA3aHHbIX c ero npnMeHeHeM.lonb3oBaTenb HacToero cTaHgapTa HeceT OTBeTCTBeHHOCTb 3aycTaHoBneHne cooTBeTcTByioux npaBn no TexHnKe be3onacHocT noxpaHe 3AopoBb,a Takke onpegengeTLenecoo6pa3Hoctb puMeHeHng 3akoHogatenbHbix orpaHneH nepeg ero cnonb3oBaHeM.2 HopMaTBHble c
17、cbInKB HacToAweM cTaHAapte ncnonb3oBaHbi ccbinkn Ha cnegylowne cTaHAaptbl:2.1 CTaHAapTbI ACTM1):ASTMD 96,Test method for water and sediment in crude oil by centrifuge method(field procedure)ACTMA 96,MeTog onpegeneHng Bogi n ocagka B Hetn LeHTpnpyrnpoBaHnem(noneBo MeToA)(OTMeHeH B2000)2)ASTM D 1796,T
18、est method for water and sediment in fuel oils by the centrifuge method(laboratoryprocedure)ACTMA 1796,OnpegeneHne BoALi n ocagka B Ma3yTe ueHTpn中yrnpoBaHnem(na6opatopHaMeToAMKa)1)YTo4HNTb cCHIIKn Ha cTaHgapTbi ACTM MoxHo Ha caite ACTM www.astm.org nn B cnyx6e nogepxkn knneH-ToB ACTM:serviceastm.org
19、.B nHpopMaunoHHoM ToMe exerogHoro copHnKa cTaHgapToB(Annual Book of ASTMStandards)cneyer o6pau,aTbc K cBoAke cTaHAapToB exeroAHoro c6opHnKa cTaHgapToB Ha cTpaHne caviTa.ASTM D1796,Test method for water and sediment in fuel oils by the centrifuge method(laboratory procedure)(ACTM A 1796,Onpe-AeneHne
20、BoAbi n ocaAka B Ma3yTe yeHTpn中yrnpoBaHnem(na6opaTopHa MeToAnKa).2)C nocneAHe ucTopnueckon Bepcne craHgapta MOxHO 03HaKoMTbCA ha cavite www.astm.org.M3AaHne opnunanbHoeFOCTP57040-2016ASTM D 1835,Specification for liquefied petroleum(LP)gases ACTM A 1835,Cneunnkauna Ha cxn-KeHHble yrneBoopoAHble ra3b
21、lASTME1,Specification for ASTM liquid-in-glass thermometers(ACTMAE 1 CneunnKaynA Ha cTeknAH-Hble MAKoCTHble TepMOMeTpbl)2.2 AoKyMeHT MHCTTyTa 3HepreTKn:IP MeTogbi ncnbitaHn.pnnokeHne A.CneyupnkaynA.CTaHgapTHble TepMoMeTpbi IP(IP Testmethods-Appendix A.Specifications-IP standard thermometers)1)3 TepM
22、Hbi n onpegeneHgB HactoAu(em cTaHAapte npnMeHeHbI cnegyiowne TepMHbI c cOoTBeTCTByiouMn onpeAeneHnAMn:3.1 OnpegeneHu tepMnHoB,xapaktepHbix Ang Hactowero ctaHAapta3.1.1 Bn3yanbHoe Ha6niogeHne MacngHoro ngTHa(oil stain observation):O6LeM pacTBopa ocTaTka,npu KoTopoM MacngHoe ngtho n konbyo coxpaHgeTcA
23、 Ha 中unbTpoBanbHo 6yMare np ycTaHoBneHHbIXycnoBgx B TeeHne 2 MH.3.1.2 octatok(residue):Octato4hbi Matepnan,n3MepgeMbi c to4Hoctbo go 0,05 mn,Bbiknnaownnpu TeMnepatype Bbiwe 38 C,nony4aeMbiinpn ncnapeHn 100 Mno6pa3ya B ycnoBgx HacTogwero MeToga.3.1.3 pacTBop ocrarka(solvent-residue mixture):PacTBop,n
24、onyuaeMbi npn AoBeAeHnn ocTatka BLeHTpu中yxHon npo6npke nocne BbiBeTpnBaHng o6pa3ua pactBopuTenem go o6beMa 10 Mn B ycnoBnAxHacToguero MeToga.4 CyHOCTb MeToAa4.1 BbigepxnBaiot 100 mn npo6bi cxneHHoro HetAHoro ra3a B LeHTpyxHo npo6npke BMect-MOCTbio 100 Mn.M3MepgioT n pernctpupyot 06beM ocTatKa B npo6
25、npke nocne HarpeBaHng go teMnepatypbi38C.4.2 An pactBopeHnA octatka B ueHtp中yxHyio npo6npky go6aBngioT pactBoputent go nonyeHnA10 Mn pacTBopa.He6onbwo n3MepeHHb 06bem pactBopa octatKa B ycTaHOBneHHoM nopAAke noMeaoTha punbtpoBanbhyio 6ymary.Pernctpupyiot Bhewhn BnA 中unbtpoBanbho 6yMarn,ha kotopyio 6
26、bin hahe-CeH M3MepeHHb o6beM pacTBopa ocTaTKa.5 Ha3Ha4eHne n npnMeHeHne5.1 KoHTponb 3a cogepxaHneM ocTatKa(o6g3aTenLHoe Tpe6oBaHne ACTMA1835)nMeeT BaHOe 3Ha-4eHe npu ucnonb3oBaHnn LPG.OcTatkn B cucTeMax noga4n xnAKoctn Moryt npnBectn K HexenaTenbHoMyoTcToo,a B cucteMax oTBoga napoB ocTatKn Moryt nep
27、eHocutbcA n 3arp3HAtb perynnpylowee o6opyAoBa-He.HaKonnBwnecA octatKn MoryT Bbi3biBatb Koppo3nio n 3arpA3HATb cnegyiowN npogykT.Boga,oco6eHHOueno4Hag,Moket npnBect kotka3y perynupyowero o6opygoBaHng n koppo3nn MeTannoB.6 loMexn6.1 TBepqble npnMecn,takne kak pxaB4nHa,okannHa nn rp3b,aBngiotc nomexamn
28、 ng hactoq(eroMeToga,nockonbky HacTown MeToA He npeAycMaTpnBaet onpegeneHne TBepAbiX HepacTBOpnMbiX 3arpA3-HeH.7 Annaparypa7.1 LeHTpyHa npo6npKapagynpoBaHha LeHTpu中yxHag npo6npka BMecTnMOctbio 100 Mn,pa3Mepbi KoTopo npnBegeHbi HapucyHke 1.lepBbie 0,5 Mn npo6npkn gonKHbi MeTb eHy geneHn0,05 Mn.Oco6eH
29、Ho BaxHa opMa KoHnKanpo6upkn.KoHycHoctb npo6npkn gonxHha 6bitb paBHoMephon,a gohbiwko gonxho 6bitb 3akpyrneHHbiM,KaKnoka3aHo Ha pcyHke 1.po6npka gonkHa 6bITb 3roToBneHa n3 TaTenbHO oToXKeHHoTo TepMocTonkoroctekna.pegenbHo gonyctuMag norpewHoctb rpagynpoBkn,ocHoBaHHag Ha onpegeneHnn obbeMa BoAbi,Hecogepxawe Bo3gyxa np 20 C,npuBegeHa s Ta6nnue 1.NloApo6Hble Tpe6oBaHnA K LeHTp中yXHbIMnpo6npKam npBeeHbI B ACTM A 96 n ACTMA 1796.1 MoxHo nony4nm a Energy Institute,61 New Cavendish St.,London,WIG 7AR,U.K.www.energyinstpubs.org.uk.2