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本文(ASTM_D_1491_-_60_1976_rus_scan.pdf)为本站会员(益****师)主动上传,蜗牛文库仅提供信息存储空间,仅对用户上传内容的表现方式做保护处理,对上载内容本身不做任何修改或编辑。 若此文所含内容侵犯了您的版权或隐私,请立即通知蜗牛文库(发送邮件至admin@wnwk.com或直接QQ联系客服),我们立即给予删除!

ASTM_D_1491_-_60_1976_rus_scan.pdf

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11、PacTBop Ia TuTpoBaHn-ToToBAT I I TTpoBaILHoro pacT-Bopa HyTem CMemeH KOMIOHeHTOB B CIenymmMx oLemaX:704 MI e-maHol ycycHo KncIorH(CH_COOH),I34 MI ermpexxIopucroro yre-poxa(CCI4),II6 MI meTaHoa(CH2OH),I8 MI cepHOM KncIoTH(H2 S04)(I+5),I8 mr pacTBopa Byxropucro数 pryTH(HCI2)B me-TaHone(IOO r/muTp)IO MI

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13、eTcA ycToBOCTLCmeCH pacTBopTenL/yrIeBOnOpOn K BOne.B cnyae CIMMKOM OOILmOrOKOInqecTBa yrIeBonopona I CIMKoM IpoOKTeILHOTO THTpOBaHMABOIHHM pacTBopoM OpoMIa-opomaTa,THTpoBaILHaH CMeCL MOKeTHopMa.no peareHTam,He BOeIuM B HepeYeHL AMepKaHCKoroXMTeCKOrO OomeCTBa,CM.heagent Chencica an sten,by.ooeph.vaen

14、.co.,me.Ve yorniteol Staes Pharncacoeia3.Beok ofASTH,23.4.pa3eITcH Ha IBe pa3H.EcI cmech cTaHoBMTca myTHo In pa3-lemerca ha IBe pa3h,aHans opakyT HobTopaT c MeHLuM KOI-ecTBOM oopa3a.6.2.MeTon onpeneeHa KoHua TuTpoBaHng(pmMeaHn 2 3)-CraBaT XmMnecknl crakaH Ha cToiky TTpoBaHMA,ycTaHaBIMBaTcTekIHHH I I

15、aTHoB IekTpoIH,BIuaT MeaIky I HaMHaTTHTpoBaHMe 0,02H pacTBopom OpomMIa-pomaTa.IpOBOIAT OOHTHoeoTeHuomeTpeckoe ThTpoBaHe,chmaa oKa3aha 3IeKTpOIBKy-me cHIH B saBChMoCTH oT KOIHqecTBa THTpoBaHHoro pacTBopa BMLIIIMTpax.KoHe THTpoBaHMA MOKeT OHTL OnpeleIeH OOHTHHMcHocoOoM,IooaBIAT THTpOBaHHHi pacTBop O,I

16、O MI HOpuMAMM.IawTcTaOI3poBaTLca eKTponBMKymel cuIe n cTpoaT rpajMK saBCH-MOCTH cTaOILHO neKTponBymel CHH OT KOecTBa H3pacxoo-BaHHOro TMTpoBaHHoTo pacTBopa B MIIMrpaMMax.ToKa neperOapHMaeTcH 3a KoHe TTpoBaHa.IpMeaHe 2-06mHa pouenypa,3IoeHHaH B.6.2,MokeT OHTL yTOMTeILHo H 3aHMMaTL MHOTO BpeMeHn Ip TH

17、TpoBaHWHcIaoaKTMBHHX oneMHoB,Ha TTo yKa3HBaer pe)eKTpoBKymel cHIpeBumaomi 20-I00 MB/MZH B soHe KOHua THTpoBaHMA.B TX cy-ax yOOHO HOIL3oBaTLca cenyme MeTonKo.HpoOnKaT TuT-poBaHme O,I MI HOpuMAMH c HTepBaIaMH I MMH.3a KOHen THTpOBaHHpMHMaeTCH cHAToe HoKa3aHe eKTpOIByme cI c pelpoM,HeIpeBameM 5-I0 MB/M

18、H.IpmeaHne 3-CTaoILHOCTL KOHua TtpoBaHna up conepkaHM250 mI/kT.(6onee 250 Mr/kr,Iu apyrux npmMecei,BcTynamX BO B3aMO-eicTBue c OpomOm)moxer BH3BaTL ycTolqBui apeip aneKTpoBy-mel cHIN BOIM3n KoHua TuTpoBaHMA.GToT pei nponoKaeTca ameHocle abHoo KoHua ThTpoBaHna Hpn 3omTke TTpoBaHa pMusouTke Opoma.Ip o

19、upeneeHM KoHua TTpoBaHMA,Kora coepa-He TopeHa peBHmaeT 250 Mr/Kr,cKopoCTL BBeleHMA pacTBopaOpOMa-pomaTa He lOIKHa HpeBmaTL 0,5 MI/MMH.C HpOMKeHeMk KoHy TTpoBaHa pereHT BBonaT HopuMaMn no 0,2 0,5 MI MCHmMaor cooTBeTCTByomme noka3aHn 3IC.KoHen TTpoBaHna cunTa-erca locTrhyTHM,Korla beeneHne looaBkn 0,2 MI peareHTa BusHBaeTOTKIOHeHMe He MeHee 0,075 B oT MaKCMMaILHOrO OTKIOHeHIH HOCIe

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