1、:D 242504(2009.)-STANDARD TEST METHOD FOR HYDROCARBON TYPES IN MIDDLE DISTILLATES BY MASS SPECTROMETRY ():1522-11/ASTM :11.10.2011 2011 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 1942
2、8,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FGU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,P
3、A 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM In
4、ternational or FGU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 2425-04(2009)1 :D 242504(2009.)-1 D 2425;,.().1.1.1 -,204 343C(400 650F)5 95%,D 86.C12 C16 10 C18.11 ,:,/,(),CnH2n-10(.),CnH2n-14(1 ASTM D02 ,D02.04.0M -.1 2009.2009.1965.2
5、004.D2425-04.DOI:10.1520/D2425-04R09.ASTM D 2425-04(2009)2.),CnH2n-16(.).1 -103 Consolidated Electrodynamics Corp.1.2,(-).1.3 ,.,.,.10.1.2.2.1 ASTM:2 D 86 M D 2549 ,3.3.1 :71()=m/e+71+85.2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 2425-04(2009)3 67(-,)=m/e+67+68+6
6、9+81+82+83+96+97.123()=m/e+123+124+137+138+.249+250.149()=m/e+149+150+163+164+.247+248.91()=m/e+91+92+105+106+.175+176.103(,)=m/e+103+104+117+118+.187+188.115(CnH2n-10,)=m/e+115+116+129+130+.185+186.128()=m/e+128.141()=m/e+141+142+155+156+.239+240.153(nH2n-14,)=m/e+153+154+167+168+.251+252.151(nH2n-
7、16,)=m/e+151+152+165+166+.249+250.177()=m/e+177+178+191+192+.247+248.4.4.1 D 2549 ,-.ASTM D 2425-04(2009)4 ,.,.%.2 D 2549 ,5%232C(450F).5.5.1 ,204 343C(400 650F),.6.6.1 ,.(,0,25%),.7.7.1-.ASTM D 2425-04(2009)5 7.2 ,.(125 325C).7.3 .8.8.1 ,:8.1.1 ,m/e+226 n-.8.1.2 ,m/e+40 292.8.1.3 70-,10 70.3 ,67/71
8、 n-0,26/1.0,2/1 0,30/1.4 ,-103 Consolidated Electrodynamics Corp.,.9.9.1 -.,ASTM D 2425-04(2009)6 .9.2 -C10 C18 ,0,1%.,m/e+69 71 0,1%2 5.10.-10.1 -2 4 (15 30).(!).-m/e+40 292 ,.8.1.1-8.1.3.11.11.1 -,m/e+67 69,71,81 83,85,91,92,96,97,103 106,115 120,128 134,141 148,151 162,165 198,203 212,217 226,231
9、 240,245,246,247 252.:71=71+85(1)67=67+68+69+81+82+83+96+97(2)91=N=0N=6(91+14N)+(92+14N)(3)ASTM D 2425-04(2009)7 103=N=0N=6(103+14N)+(104+14N)(4)115=N=0N=5(115+14N)+(116+14N)(5)141=N=0N=7(141+14N)+(142+14N)(6)153=N=0N=7(153+14N)+(154+14N)(7)151=N=0N=7(151+14N)+(152+14N)(8)177=N=0N=5(177+14N)+(178+14
10、N)(9)11.2 n=10 n=18 :n=m 1(K1)K2(10):n-,n,.m-,m 1-1,P-m,m 1,K1-(.1),K2-n(.1).5 -,-1 .,C9 204C(400F),.ASTM D 2425-04(2009)8 1.m/e ,K1 ,K2 10 134 0.1101 85 11 148 0.1212 63 12 162 0.1323 60 13 176 0.1434 57 14 190 0.1545 54 15 204 0.1656 51 16 218 0.1767 48 17 232 0.1878 45 18 246 0.1989 42 L1 L2 11 1
11、42 0.1201 194 12 156 0.1314 166 13 170 0.1425 150 14 184 0.1536 150 15 198 0.1647 150 16 212 0.1758 150 17 226 0.1871 150 18 240 0.1982 150 11.3 A,:(11)11.4 n 11 n=18 :(12):xn-,n,m-,m 1-1,P-m,m 1,L1-(.1),ASTM D 2425-04(2009)9 L2-n(.1).6 -1 .128 m/e+128.11(142)18(240).11.5 ,:(13)11.6 .(71 67,)(.11.3
12、2).71 67 .,103,115,153 151,.2.,10 11 11 12 12 13 13 15(14,5)14 16(15,5)ASTM D 2425-04(2009)10 ,.(),.11.5.177 C14,C14 177.,3 .4.,()-,-.,.,%,.11.7 -,m/e+67 69,71,81 83,85,91,92,96,97,105,106,119,120,123,124,133,134,137,138,147 152,161 166,175 180,191 194,205 208,219 222,233 236,247 250.:ASTM D 2425-04
13、(2009)11 71=71+85(14)67=67+68+69+81+82+83+96+97(15)123=N=0N=9(123+14N)+(124+14N)(16)149=N=0N=7(149+14N)+(150+14N)(17)91=N=0N=6(91+14N)+(92+14N)(18)11.8 ,(71,69,123 149)(.11.3 2).91 .91 -(.11.3).(.3).5,.(),%,.ASTM D 2425-04(2009)12 3.-.12 13 14.5 15.5 12 13 14.5 15.5 13 14.5 15.5 13 14.5 15.5 :71 100
14、 100 100 100 4 4 6 6 2 1,1 1,5 1 1 2 67 19 21 23 26 100 100 100 100 160 130 150 175 170 150 123 0,1 0,2 1 1 1 3 100 100 100 26 10 20 149 0,2 5 8 100 100 100 91 176 0,4 0,4 0,4 0,4 0,2 3 4 4 5 15 15 20 103 188 1 3 115 186 0,5 1 1 1 1 0,5 128 141 9 9 10 12 2 0,3 0,2 0,1 0,1 0,4 153 1 2 2 2 151 1 5 7 1
15、0 177 2 2 :148 170 192 238 302 347 416 439 220 268 298 220 268 298 66 70 74 81 145 153 165 170 107 137 117 118 150 127 87 92 97 104 180 191 204 209 122 156 134 124 158 135 ()CnH2n-10,()11 12 13 14 10 11 12 13 10 13 10 11 12 13 :71 0,3 0,3 0,4 0,5 0,2 0,4 0,4 1 0,3 1,7 0,5 5,2 1,5 2 67 0,7 0,7 2 3 0,
16、6 1 1 2 0,3 6,0 0,8 1,2 1,5 2 123 0,1 0,1 0,2 0,3 0,1 1 2 0,4 4,8 0,2 0,5 7,8 4 149 1,3 1 1,5 2 0,1 0,2 0,3 0,9 0,1 0,7 0,5 91 176 100 100 100 100 15 18 17 15 0,6 6,2 0,1 0,9 1 1 34A,B 103 188 9 10 10 9 100 100 100 100 1,5 20,3 0,6 0,1 0,1 0,1 115 186 4,4 4,5 5 5 20 28 25 25 100 100 11,4 23 19 18 12A,B 128 0,7 1 1 1 3 5,4 7 15 13 100 0,7 5,6 5,6 141 1,0 2,5 28 100 100 100 153 6,1 8 10 151 4,5 7 7 177 0,6 :450 450 450 450 380 420 420 420 410 372 236 360 380 380 265 242 222 206 280 276 250 227 307