1、 ()API RP 13K-2011 RECOMMENDED PRACTICE FOR CHEMICAL ANALYSIS OF BARITE :.-.:64-.:3 :09.09.2011 :09.09.2011 (API).,.API ,.,API This Standard has been translated by Kazakhstan Institute for Standardization and Certification with the permission of the American Petroleum Institute(API).This translated
2、version shall not replace nor supersede the English language version which remains the official version.API shall not be responsible for any errors,discrepancies or misinterpretations arising from this translation.No additional translation or reproduction may be made of the Standards without the pri
3、or written consent of API.Copyright American Petroleum Institute API,.,.API,API -,;,.API,API ,.API ,.,-,.API .,.API .,API,.API ,API.Copyright American Petroleum Institute API -,.,.,.,.API API.,1220 L Street,NW,20005.,.,API,.API,(202)682-8000.API API,1220 L Street,NW,20005.API,1220 L Street,NW,20005,
4、standardsapi.org.Copyright American Petroleum Institute ,API.,.,.,-,().(OHSA),29 1910.1001;,40 61.140 61.156;(763.160-170).,.,Copyright American Petroleum Institute iv 1 12 13 24,3 5 5 5.1 55.2 55.3 66 6 6.1 6 6.2 66.3 76.4 86.5.8 6.6.9 6.7 97 117.1 117.2 11 7.3 127.4.137.5.137.6.14 7.7 14 8,.,15 8.
5、1 158.2 15 8.3 15 8.4 158.5 169.,.,16 9.1 169.2 169.3 179.4 17 9.5 18 10 1810.1 1810.2 1910.3 19 10.4.2010.5.2010.6.20Copyright American Petroleum Institute 10.7.2110.8.21 10.9.21 11 2211.1 2211.2 2211.3 22 11.4 23 12 2312.1 2312.2 2312.3 24 12.4.24 12.5.2412.6.2412.7.25 13 25 13.1 2513.2 2513.3 251
6、3.4.26 13.5.26 13.6.2613.7.27 13.8.2714 ,-2714.1 2714.2 27 14.3 27 14.4 2714.5 2815 2915.1 29 15.2 29 15.3 2915.4.3015.5.30 15.6 30 16 3116.1 3116.2 .3116.3 31 16.4 31 17 3217.1 3217.2 32Copyright American Petroleum Institute 17.3 3217.4.33 17.5.33 17.6.3317.7.3317.8.34 18 34 18.1 3418.2 .3418.3.351
7、8.4.35 18.5 3519 3519.1 35 19.2 36 19.3 3619.4 3719.5 3820 38 20.1 38 20.2 3920.3 3920.4 4020.5 41 21 ()41 21.1 4121.2 4121.3 4221.4 42 21.5 42 22-4322.1 4322.2 4422.3 44 22.4.45 22.5.4722.6 4723 47 ()48 ()50 1 SrSO4 BaSO4 11 1,22 ,40 Copyright American Petroleum Institute 1 1.1 .,.1.2 1 ,;,.1.3 ,.,
8、.1.4 ,.,.2 .().API 13-1,API 13I-2009,API (),15,ISO 10416:20081,.29 ()2,1910.1001 _ 1 ,1 ch.de la Voie-Creuse,Case postal 56,CH-1211,Geneva 20,Switzerland,www.iso.org 2 ,20402 Copyright American Petroleum Institute 40 (),61.140 61.156 51 (),3738-3759(29 1986)1.,()BaSO4,4.50 2.5-3.5 SrSO4 3.97 3.5 BaC
9、O3 4.30 3.5 BaSi2O3 -CaCO3 2.72 3 ,CaMg(CO3)2 2.87 3.54-4 MgCO3 3.0 4 CaSO42H2O 2.3 2 CaF2 3.0 4 Fe2O3 5.2 5.5 Fe2O3nH2O 3.3-4.0 5.5 Fe3O4 5.16-5.17 5.5-6.5 FeCO3 3.7-3.9 3.5-4.0 FeS2 5.0 6-6.5 Fe1-xS 4.6 4 /CuFeS2 4.2 4 PbS 7.5 2.5 ZnS 3.9 3.5-4.0 FeTiO3 4.7 5.5 SiO2,2.65 7.0 (NaK)AlSi3O8,2.6 6.0 K
10、Al2(OH)2AlSi3O10 2.85 2.5 Al2Si2O5(OH)4 2.6 2.0 (Al,Mg)(OH)2Si4O10(Na,Ca)x4H2O 2-3 1-20 3 .3.1 :,3.2 :,Copyright American Petroleum Institute 4,.()(),-,-,-()cBaSO4,%,cCaCO3,%,cCaOH2,%(),cCl -,/cO3 -,/cO3,%-,cement,%,celement1,%,celement2,%,cFe ,/cFe,%,cFeO3,%,cFeO3,%,cHCl-soluble CA,%,.8 cHO3,%-,/cm
11、etal ion,%,/-,/Pb ,/cPbO3,%,P4 ,/S ,/S4 ,/Sr,%,6.6 SrSO4,%,cwater-soluble CA,%,.11 Zn ,/ZnO3,%,fAl2O3 fO3 ,.2,5 8101811 fS 2fSiO2 k ,.1 lST ,Copyright American Petroleum Institute ,m ,m1 ,m1 ,m2 ,m3 ,m4 ,m5 ,n1 ,nm n2 ,nm n3 ,nm n4 ,nm R ,/RIC ,/RM ,/RPO4 ,/V ,VAgNO3 ,VHCl 0,1N HCl,VM 0,2N H2SO4,VP
12、0,2N H2SO4,/5 5.1 5.1.1 .,.5.1.2 ,.,.,(.).5.2 5.2.1 ,.5.2.2 ,(Copyright American Petroleum Institute ),(1%).5.2.3 ,(/).5.2.4 ;.5.3 5.3.1 (BaSO4)(Na2CO3),.5.3.2 (SrSO4)-(Na2CO3),()().5.3.3 (SiO2)(Al2O3)(NAOH),.5.3.4 (NA)()(HCl)/(HF/H2SO4/HNO3),.Na K,HCl,Na K,HF/H2SO4/HNO3.Na K,Na K .5.3.5 (Ca),(Mg)(F
13、e)-(HCl)/(HF/H2SO4/HNO3),.Ca,Mg Fe,HCl,HF/H2SO4/HNO3;Ca,Mg Fe,:(CaF2),(),(Mg )(FeS2).5.3.6 (Fe)(HNO3)/(HCl/HNO3),.5.3.7 (Cu),(Mn),(Pb)(Zn)-(HCl),.5.3.8 (FeCO3)()/(NaOH),.5.3.9 (CO3-2)().5.3.10 (S-);1N HCl 1N H2SO4,H2S .Copyright American Petroleum Institute 5.3.11 ,.5.3.12 ()1000(1832F),.5.3.13 (),/
14、HCl.6 6.1 (BaSO4)(SrSO4)(Na2CO3),(HCl)(Ba),(Sr)-.6.2 6.2.1 6.2.2 (CAS#497-19-8),Na2CO3,.6.2.3 (0,2%),1 Na2CO3,500 .6.2.4 (1:4)(CAS#7647-01-0),20 HCl,80-.6.2.5 (1:19)(CAS#7664-93-9),5 H2SO4,95-.6.2.6 (1%),5 H2SO4,495-.6.2.7 ,5,10 15 (/)Sr 1%HCl.6.2.8 (CAS#1336-21-6),NH4OH,.6.2.9 (CAS#547-58-0),0,1 ,1
15、00 .6.3 6.3.1 .6.3.2,149.6.3.3 ,.6.3.4,0,001.6.3.5 ,.6.3.6 ,25.Copyright American Petroleum Institute 6.3.7 ,25 (10)50 (20).6.3.8 ,1000+20(1832+72F).6.3.9 (),250,400 600.6.3.10 ,-250 -600.6.3.11 .6.3.12,65.6.3.13 ,11,0 -403,11,0 -541 .6.3.14 (TC),250.6.3.15 ,1(12,33 35).6.3.16 6.3.17 ,10.6.3.18 (TD)
16、,.6.4 ,100%.6.5.6.5.1 1,0 .:.,.0,8,.6.5.2 25-,6 Na2CO3.2 Na2CO3.6.5.3 1 1000(1832F).:.6.5.4 ,.:._ 3 40 541 ,.API 13K API .:5%,6.5.9.5%,.6.5.8,.Copyright American Petroleum Institute 6.5.5 .250-,150 .,.:.6.5.6 .6.5.7 40 ,.(12)0,2%Na2CO3.6.5.8 .6.5.8.1 6N HCl,250-.,.,.:,250-.10 400-.6.5.8.2 NH4OH ,NH3.6.5.8.3 541 ,600-.6.5.8.4 6N HCl,250-.6.5.8.5 NH4OH 600-6.5.8.3.6.5.8.6 400.6N HCl.1 6N HCl.,BaSO4,6.5.13-6.5.16.6.5.9 (Ba,Sr,Cr)HCl(20%),600-.,.:,250-,.10 600-.6.5.10 6N HCl .:,.6.5.11 .6.5.12 400 ,
