1、 D94-07(2017.)136S1/98,136S2/99 STANDARD TEST METHODS FOR SAPONIFICATION NUMBER OF PETROLEUM PRODUCTS 2017 ():16.11.2017:3318-17/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.AST
2、M International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,U
3、SA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM Internation
4、al or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D94-07(2017)1 D94-07(2017.)136S1/98,136S2/99 1 D94;,.().1.1.1 ,.1 ,D117.,D94,0,1 M KOH 0,1 M HCl.1 ASTM D02 ,D02.06 .1 2017.2017.1921.2007.D94-07(2012)1.DOI:10.1520/D0094-07R17.ASTM D
5、94-07(2017)2 1.1.1 :A (6 13),(14 23).1.2 ,.2 ,.,.,.,D128 IP 284/86.1.3,.1.4 ,.,.6,7,8,10,15,16,17 19.ASTM D94-07(2017)3 1.5 -,(TBT).2.2.1 ASTM:2 D117 ,D128 D1193 D4057 D4177 D6299 D 6792 ,2.2 :3 IP 136 IP 284 3.3.1:2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 ,61 New Ca
6、vendish St.,London,W.I.,England,61 New Cavendish St.,London,WIG 7AR,U.K.,http:/www.energyinst.org.uk.ASTM D94-07(2017)4 3.1.1 ,1 .3.1.1.1 ,.2.3.1.2 (),.4.4.1 ,(),(.),(KOH).4.2 (),().5.5.1 ,.,.,1 ,(.,),ASTM D94-07(2017)5 .5.2 .A 6.6.1 ,250 300,(.3)(.;),.3 ,KOH .(,Nochromix ).6.2 (.,.).7.7.1 .,ASTM D9
7、4-07(2017)6 ,4.,.4 ,.7.2 ,I,II,III IV D1193.7.3 5 95%-(.)(.5)95%-,10%()(.5 6),.5 ,99%-2-(),.,.6 30 (3-1938).5 3A 5%-.7.4 (0,5 M)0,0005 KOH(.7.8 4 ,Washington,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.5 -,1200 Pennsylvania Avenue,NW,Washington,DC 20226.ASTM
8、 D94-07(2017)7.7).7 ,0,1 M KOH HCl 0,5 M(.7,8,10,17 19).7.5 (),.(.4.1.).7.6 ,(.).ASTM(-60/80 )(.).-IP 136.7.7 ,1,0 0,1 100 (.7.3).-(0,1 M)KOH.7.8 KOH(0,5 M)0,5 M KOH ,7.3.24 .7.8.1 ,KOH 0,5 M 0,1 M KOH ()95%-.(.8).8 -,2-(),.7.8.2 KOH ASTM D94-07(2017)8 (.7.9 .8).7.9 0,1 M(C8H5KO4)2,0422 0,0002 ,110C
9、 5C ,100.100 .7.10 ,.(.).7.11,.(.).8.8.1 (.9)():(.10)25 0,03 KOH 25 1 (),.,.().11.50 (ASTM)(.7.6,.12 13)(,),0,5 M(HCl),.ASTM D94-07(2017)9 9 .10 KOH ,30 .11 30 ,10.,2.,.12 50 ,.13 (ASTM)-.8.2 ,.,(.14).,.V2 11.1.14 ,.9.9.1 D4057()D4177(),.ASTM D94-07(2017)10 ,40 80%,20 (.15).15 :,181 400 1 111 180 2
10、71 110 3 31 70 5 16 30 10 0 15 20 10.10.1 0,01 (11.1 W),25 1 (.4.1),25 0,03 KOH(.7.3),(.7).10.2 ,15 25 (.7.10)(.7.11)(.4.1).10.3 30 (.11),50 (ASTM).(,)(.7.6)(.12).10.4 ,(),0,5 M HCl,(.7.3).ASTM D94-07(2017)11 ,.,(.14).,.(V2 11.1).11.11.1 ,A,:A=56,1 M(V1 V2)/W(1):M-,V1-,V2-,W-,56,1-KOH.12.12.1 ,50,0,
11、5 KOH/.12.2 ,50 ,.12.3 0,1 KOH/.12.4 ,D94,.ASTM D94-07(2017)12 13.13.1 ,.1,95%-(.16).16 ,.().1.13.1.1 ,ASTM D94-07(2017)13,.1 .13.1.2 ,.1 .13.2 ,.B 14.14.1 ,250 300,(.3),.14.2 (.6.2).14.3 ,ACS ASTM D94-07(2017)14 (HCl).4 14.4 ,.14.4.1 ,;(AgCl)/(LiCl),KCl.14.5 ,KCl ,(.17).17 ,.,2,5 0,5,(PTFE).14.6 ,2
12、50 300 (.18).18 .,.14.7,.2.14.7.1,.ASTM D94-07(2017)15 ,/.2.14.7.2,10 20,0,05 0,02,.14.7.3 ,.,(.19).19 ,().(),(),D()ASTM D94-07(2017)16 15.15.1 .,4.,.20 ,.15.2 ,I,II,III IV D1193.15.3 95%-(.7.3)(.5)95%-,10%(.7.3 .5 6),.15.4 (0,5 M)0,0005 KOH(.15.7 .7).15.5 (),.(.4.1.).15.6 ,(.),ASTM(-60/80 )(.).-IP
13、136.ASTM D94-07(2017)17 15.7 KOH(0,5 M)0,5 M KOH ,7.3.24 .15.7.1 ,KOH 0,5 0,1 M KOH ()95%-.(.8).15.7.2 KOH (.15.8 .8).15.8 0,1 M(C8H5KO4)2,0422 0,0002 ,110C 5C 1 100.100 .15.9 ,.(.7.10.)15.10 (3,0 M)225,2 KCl 1,0 .15.11,.(.7.11.).15.1).15.12,.15.1.ASTM D94-07(2017)18 16.,16.1 :16.1.1 ,()3,0 M KCl.16
14、.1.2 .,3,0 M KCl .16.1.3 .3,0 M KCl,.16.2 ,10 0,5 M KOH 0,5 M HCl.16.3 :16.3.1 ASTM D94-07(2017)19 (.16.3.3)Nochromix.16.3.2 3,0 M KCl .KCl.16.3.3 ,.,.(,.,).16.3.4 KCl .,.,.16.3.5 KCl .,ASTM D94-07(2017)20:50 38 2-38 ,1.,.,.16.3.6 ,.17.17.1 (.9)():(.10)25 0,03 KOH 25 1 (),.,.()(.8.1 .11).50 ,ASTM.(.
15、7.6)(.12 ASTM D94-07(2017)21 13)(,),0,5 M HCl.17.2 200,10 (.7.6).17.3 .,.,.17.4 0,5 M HCl,2/,.,KOH(VB 21.1),(K2CO3)KOH(.3).17.5 .18.18.1 .,40%80%,20 (.15).19.19.1 0,01 (21.1 ASTM D94-07(2017)22 W),25 1 (.4.1),25 0,03 KOH(.7.3),(.7).19.2 ,15 25 (.7.10)(.7.9)(.4.1).19.3 30 (.8.1 .11),50 ASTM(,)(.7.6)(
16、.12)().19.4 ,(),0,5 M HCl.,(.17).3 .,.19.4.1 .-520.-300,50.ASTM D94-07(2017)23 .3.20.20.1 (QC),.20.2 QC(.ASTM MNL 7).6 20.3 QC ,(.ASTM MNL 7)6.().().20.4 QC 6 ASTM MNL 7,6-.,ASTM International,W.Conshohocken,PA.C D ASTM D94-07(2017)24 ,.QC .QC ,.QC ,.D6792.20.5,QC,.QC ,.20.6 .ASTM MNL 76 D6299.21.21.1 ,A,:(2):56,1-KOH,M-HCl,VB-,VS-,W-,.ASTM D94-07(2017)25 21.2 .,(.3).(VB)(VS).22.22.1 50,0,5 KOH/.22.2 50 ,.22.3 0,1 KOH/.22.4 ,D94,.23.23.1 ,16 7 ,:7 23.1.1 ,2,76 7 -ASTM International RR:D02-1340.A
