1、 D 974-142:139/98 STANDARD TEST METHOD FOR ACID AND BASE NUMBER BY COLOR-INDICATOR TITRATION ():2905-16/ASTM :02.06.2016 2016 -,.9,-49,-1,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM
2、 International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,US
3、A.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM Internationa
4、l or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 974-142 1 D 974-142 :139/98 1 D 974;,.().1 7.6 2015.2 15.1.1 15.1.2 2016.1.*1.1 (.1)2 1 ASTM D02 ,D02.06 .IP .ASTM-IP 1965.1 2014.2015.1948.2012.D974-12.DOI:10.1520/D0974-1402.2,D 11
5、7.ASTM D 974-142 2,.,109.,109,.,109.1 ,.,(),.2 .D 4739.1.2 ,.,.3 ,-,D 664.,D 664;,ASTM D 974-142 3 D 4739,.1.3,.1.4 ,.,.2.2.1 ASTM:3 D 117 ,D 664 D 1193 D 4175 ,D 4739 3.3.1:3.1.1 ,3 ASTM ASTM,www.astm.org serviceastm.org.ASTM ASTM Document Summary.ASTM D 974-142 4 ,.3.1.1.1 -,/-.3.1.2 ,.3.1.2.1 -,-
6、.3.1.3 ,(,),.D 4175 3.2 ,:3.2.1 ,-,.4.4.1 ,ASTM D 974-142 5 ,-(-).,.5.5.1 ,.,.;,.5.2 ,.,.ASTM D 974-142 6 6.6.1 ():50-,0,1 10-,0,05 5-0,02 4 ,0,05 ,.7.7.1 .,4,.,.7.2 ,I,II III D 1193.7.3 ,(0,9%.).().7.4 ,(0,1)9 (-.)4 Reagent Chemicals Society Specifications,American Chemical Society,Washington,DC.,.
7、Annual Standards for Laboratory Chemicals,BDH Ltd,Poole,Dorset,U.K.,and United States Pharmacopeia and National Formulary,U.S.Pharmaceutical Convention,Inc.(USPC),Rockville,MD.ASTM D 974-142 7(HCl,1,19)1000 (2-)(.7.3).,0,0005(.6),8 ()0,1 ,125 ,.,.,.5 ,7.1.6 HCl ,1,00 5,00 .(NaOH)(H2SO4)HCl,.7.5 0,1
8、100 .7.6 -5,6 -,1.-10/0,01/.7.7 ,(0,1)6 ()1 (0,9%)2-5 2006.-Kodak,Baker(Mallinkrodt),Fluka Aldrich 1.Kodak .6 -ASTM International RR:D02-1626.ASTM D 974-142 8.10 15,.2 ()2)(,)5 10.,;(2).,-(Ascarite),(Carbosorb)(Indecarb).7.7.1 ,0,0005.:0,1 0,2 ,1 110 1 40 1 ,2.:(1),(2),6 .,.:=bpVVW100023,204(1)ASTM
9、D 974-142 9:Wp-,204,23-,V-,Vb=,.7.7.2 0,10 50 50 .7 .8 ,.7.8 ,100:1:99.8.8.1 ,8.2,.8.2 (.9)60 5 ,(.10).,1/3,.ASTM D 974-142 10 100-(.9).9 ,8.2,.,.10 ,.9.9.1 .1.100 0,5 ,.-,9.2;/-,10.11 .1.,0,0 3,0 20,0 2,0 0,05 3,0 25,0 2,0 0,2 0,01 25,0 250,0 0,2 0,02 0,001 0,0 25,0 2,0 0,2 0,01 25 250,0 0,2 0,02 0
10、,001 ,20-,.,.ASTM D 974-142 11 9.2 30 (.14).0,1 ,(.12).,(2).(-).-,()0,01 0,05 ().-(.13)15 ,2 0,1 HCl.12 ,0,01 0,05 9.2 9.3.13 ,.14 .15 .,15,.9.3 100 0,5 ,0,1 0,1 .9.3.1 ,.ASTM D 974-142 12 ,.10.10.1 ,-(9.1),9.2,0,1 HCl ,-.10.2 9.3.11.11.1 25 ,0,1 250-100 .500-.50-,.0,1 ,0,1 ,-.,(.15).11.2 250-200 ,.
11、0,1 .-,0,1 HCl ,.ASTM D 974-142 13 ,0,1 ,.12.12.1 ,(QC).QC ,.QC ,.7 QC ,.QC ,.,QC,QC .QC ,.16 QC,QC .7 ASTM MNL 7,Mannual of Presentation of Data Control Chart Analysis,3:Control Charts of individuals,6-,ASTM International,W.Conshohocken,PA,1990.ASTM D 974-142 14 13.13.1 :,/=(A B)M 56,1/W(2):-,(9.2)
12、,-,(9.3),-,W-,.13.2 :13.2.1 :,/=(CM+Dm)56,1/W(3):-,(11.1),-,D-HCl,(11.2),-HCl,W-,.13.2.2 ():,/=(C D)56,1/W(4):-,(11.1),D-,(11.2),-,W-,.13.3 :,/=(+FM)56,1/W(5):ASTM D 974-142 15 E-HCl,(10),-HCl,F-,-,W-,.14.14.1 ,:(D 974)=()(D 974)=()(D 974)=()14.2 :0,02 0,02 0,02 1,0 0,01 1,0 2,0 0,1 15.15.1 ,.,.15.1
13、.1 ,ASTM D 974-142 16 :0,00 0,1 0,03 0,1 0,5 0,05 0,5 1,0 0,08 1,0 2,0 0,12 15.1.2 ,:0,00 0,1 0,04 0,1 0,5 0,08 0,5 2,0 15%17 ,.18 .D 117.19 .,.15.2 ,.ASTM D 974-142 17 16.16.1 ;.()1.p-1.1-:1.1.1 .1.1.2 0,5%.1.1.3 10 1 (.2.7.3).1.1.4 0,1000 250 .(.)100 12.1,20,650 DU (Beckman DU),1 .1.1.5 :1.1.5.1 -
14、11 0,5,r -.2.1.1.1.5.2 0,5 0,01 ,-ASTM D 974-142 18 .1.1.5.3 1,0 0,01 ,.1.1.5.4 r ,.1.1.5.5 50 0,05 26,9 0,1 .2.r -2.1 2.1.1 -D 974 r.2.2 2.2.1 ,:2.2.1.1 r ,-.2.2.1.1.1 r ,pHr 4 pHr 11.pHr -.2.3 2.3.1 (),r.ASTM D 974-142 19 2.4 2.4.1 pHr -.2.5 2.5.1 ,D 664.2.6 2.6.1 .,.4 ,.2.6.2 .2.7 2.7.1 ,(0,2),D
15、664.2.7.2 ,(0,2)D 664.2.7.3 500 5 495 (2-).2.7.4 (pHr=4,0)D 664.10 ASTM D 974-142 20 100 .1.2.7.5 (pHr=11,0)D 664.10 100 .1.2.7.6 (KCl).2.7.7 7.6.2.8 2.8.1 8 D 664.2.9 2.9.1 ,25 2 .-,4,0.2.9.2 ,.,25 2.-,.0,2 11,0,pHr .0,2 11,0,ASTM D 974-142 21 .2.1.-,pHr.2.1 -pHr 2.10 2.10.1 100 (.)0,01 ,pHr 13 14.
16、2.10.2 0,5 0,01 ,pHr 13 14.2.10.3 pHr r.2.1 ,:pH-=11,5 pH-,4,0 pHr pH-ASTM D 974-142 22 -2.10.4 (),.2.11 2.11.1 ,pHr,10 12 pHr.2.12 2.12.1 .2.12.2 ,.D02.06 (D 974-12),.(1 2014.)(1)9.1.ASTM D 974-142 23 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.
