1、 D 7111-15a -(ICP-AES)STANDARD TEST METHOD FOR DETERMINATION OF TRACE ELEMENTS IN MIDDLE DISTILLATE FUELS BY INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROMETRY(ICP-AES)():2877-16/ASTM :06.05.2016 2016 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandar
2、t.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing an
3、d Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Repr
4、oduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 7111-15a 1 D 7111-15a -(ICP-AES)1 D 7111;,.().1.*1.1 ,.1,-(ICP-AES).0,1/2,0/.,.,150C 390C.,1 ASTM D02
5、,D02.03 .1 2015.2015.2005.2015.D7111-15.DOI:10.1520/D7111-15.ASTM D 7111-15a 2 .1.,308,215,396,153 455,403,493,408 393,366 267,716,283,563 228,615,236,375,238,892 324,752 259,939 670,784 220,353,224,688,283,306 279,553 257,610 202,030,204,597,281,616 221,648,341,476 177,495,178,287,185,944,214,914,2
6、13,618 340,458,342,124 214,423 766,490 588,995 251,611 328,068 407,771 283,999,189,991 334,940 310,230 213,857 1.2 .,().1.3 ,.,.1.4,.1.5 ,.ASTM D 7111-15a 3 ,.2.2.1 ASTM:2 D 2880 D 3605 -D 4057 D 4306 D 5185 -(ICP-AES)D 6299 D 6792 D 7260 ,-(ICP-AES)2.2 :2 ASTM,ASTM www.astm.org ASTM serviceastm.org
7、.ASTM.Document Summary ASTM.ASTM D 7111-15a 4 MIL-DTL-16884,3 3.3.1:3.1.1 ,.3.1.2 ().3.1.3 ,(),.3.1.4 ,.3.1.5 ,.3.1.6 ,-.3.1.7 3 300.3.1.8 ,.3.2 ,:3.2.1 ,ICP-3 3 http:/quicksearch.dla.mil http:/.ASTM D 7111-15a 5 .3.2.2 ().4.4.1 .,ICP-AES-.4.2.D 7260 ICP-AES.5.5.1 .,.5.2 D 2880 (,).MIL-DTL-ASTM D 71
8、11-15a 6 16884 .D 3605 -/-.D 3605 .,D 3605.5.3 .().,(,).,.6.6.1 ,.1 2,.1 2 ,.2.,/361,383 1-2 371,029 1-5 6.2 ,.1 2,ASTM D 7111-15a 7 .6.3 ,ICP-,.6.4 D 5185,6.1().7.7.1-ICP-AES-,(.1).190 .7.2 ,.,.7.3 ,.7.4 ,ICP-.Viton.7.5 ,47 0,8 1,0.7.6 ,ASTM D 7111-15a 8 47,.7.7,1000.7.8 ,25 50.7.9,(HDPE),125.7.10
9、,0,0001.8.8.1 .,4.,.8.2 ,-,100/.8.3 ,5000/.8.4,.,12.1,4 ,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.ASTM D 7111-15a 9 .8.5,99,995%.().8.6,99,999%.().8.7 ,10%-.().8.8 (QC),.QC ,18.QC-,QC-QC 12.3.HDPE-.9.9.1 ,.,.10.10.1 ,D 4057.D 4306.HDPE-.ASTM D 7111-15a 10
10、 10.2 .10.3 0,8 1,0 (TFE-,/).,.11.11.1 ICP-.(,),.1 ,-.(,),.,.,.ICP-.,.,ICP-.ASTM D 7111-15a 11 11.2 ,10%-(,),.,.12.12.1 .ICP-,.12.2 :12.2.1 ICP-(,).,.2 ,.12.2.2 ()5000/.,ASTM D 7111-15a 12 50 .50 .12.2.3 50/.(HDPE)(,125,),.(0,001)0,5 5000/50,0.0,001.,16.1.12.3 :12.3.1 2,0/.ICP-(,.),.,(,1,0/).5%.ASTM
11、 D 7111-15a 13 12.3.2 (2,0/)(HDPE)(,125,),.(0,0001)1,0 100/()50,0.0,0001.16.1 (.14).12.3.3 :50-1000 .,12.3.2.12.3.3.1 ,12.2.3,1,0/.12.4 ,(.12.3),.12.5 50 ASTM D 7111-15a 14 1000 .,.,.13.13.1 .1 2,.ICP-,.,.,(.1).13.2 ,(588,995).,ASTM D 7111-15a 15 .1 (,588,995),.,.,.1.(A)(B)14.14.1 .14.2 ,5%ASTM D 71
12、11-15a 16,5%.14.3 ().,.14.4 ICP-,.15 ().e (Rws)e (Ccs),Rws=(Iws Ib)/Iints(1):Iws-e ,Ib-e ,Iints-.ASTM D 7111-15a 17 15.15.1 ICP-:,1000 50,.,.ICP-.15.2 ,.,.ICP-.15.3,14.4 ,:Rf=If/Iints(2):Rf-e ,If-e ,Iintf-.,ICP-ASTM D 7111-15a 18 :Cf=(Rf Ccs)/Rws(3):Cf-(/)e ,Ccs-(/)e ,Rf-e ,Rws-e .15.3.1 3,.(6%),3.,
13、3(Cf),.,.2 ,15.3 .,150C 390C ,.15.4 .5%,.ASTM D 7111-15a 19 16.16.1 :Ccs=(M100/Mcs)C100(4):Ccs-(/)e ,C100-(/)e 100/,M100-()100/,Mcs-()100/.17.17.1 /.,(BDL),(BDL),.18.18.1 (QC)(.8.8).18.1.1 QC QC-,12.3.ASTM D 7111-15a 20 18.1.2 /(QC/QA),.18.1.3 QC/QA,QC/QA-1.19.19.1 .5 (,).(,HDPE-)(,).:19.1.1 ,.3,.5
14、-ASTM International RR:D02-1569.ASTM D 7111-15a 21 19.1.2 ,.4,.()1,0/.5.3.,/B,/0,13-1,77 0,09692 X0,5202 0,11-1,92 0,05896 X0,7520 0,10-1,77 0,0887 X0,7391 0,11-1,73 0,05839 X1,0350 C 0,15-1,60 0,2007(X+0,0001)0,4577 0,11-1,85 0,03470(X+0,6579)0,11-1,71 0,05312 X0,9114 0,10-1,83 0,06941(X 0,02484)0,
15、08-1,73 0,1166 X0,6934 0,10-1,76 0,04820 X0,6570 0,10-1,75 0,04522 X0,9759 0,11-1,74 0,08204 X0,9591 0,10-1,72 0,05274(X+0,3444)C 0,20-1,80 0,1396 X0,522 0,19-1,80 0,1191 X0,3661 C 0,12-1,88 0,1530 X0,9144 C 0,49 1,52 0,2288 X0,7489 0,21-2,03 0,02916(X+1,8414)0,17-1,95 0,07106 X0,3976 0,08-2,02 0,07
16、236 X0,5626 C 0,1557 (X+0,0125)0,6319 C 0,38-1,43 0,1099(X+0,0241)0,2606 0,11-1,73 0,04993 X0,6002 0,10-1,72 0,06637 X0,5841 0,09-1,65 0,05507 X0,7402 A ,.B X ,/.C .-ASTM International RR:D02-1778.ASTM D 7111-15a 22 19.2 -.4.,/B,/0,13-1,77 0,3689 X0,5202 0,11-1,92 0,2353 X0,7520 0,10-1,77 0,3097 X0,7391 0,11-1,73 0,2869 X1,0350 C 0,15-1,60 0,8508(X+0,0001)0,4577 0,11-1,85 0,2495(X 0,09548)0,11-1,71 0,2717 X0,9114 0,10-1,83 0,09703(X+0,4716)0,08-1,73 0,6039 X0,6934 0,10-1,76 0,2200 X0,657 0,10-1,
