1、Designation:D726020Standard Practice forOptimization,Calibration,and Validation of InductivelyCoupled Plasma-Atomic Emission Spectrometry(ICP-AES)for Elemental Analysis of Petroleum Products andLubricants1This standard is issued under the fixed designation D7260;the number immediately following the
2、designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope*1.1 This practice covers information
3、 on the calibration andoperational guidance for the multi-element measurements us-ing inductively coupled plasma-atomic emission spectrometry(ICP-AES).1.2 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this st
4、andard to establish appro-priate safety,health,and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision o
5、n Principles for theDevelopment of International Standards,Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade(TBT)Committee.2.Referenced Documents2.1 ASTM Standards:2D4057 Practice for Manual Sampling of Petroleum andPetroleum ProductsD4307 Practice for Pre
6、paration of Liquid Blends for Use asAnalytical StandardsD6299 Practice for Applying Statistical Quality Assuranceand Control Charting Techniques to Evaluate AnalyticalMeasurement System PerformanceD6792 Practice for Quality Management Systems in Petro-leum Products,Liquid Fuels,and Lubricants Testin
7、gLaboratories2.2 ICP-AES Related Standards:C1111 Test Method for Determining Elements in WasteStreams by Inductively Coupled Plasma-Atomic EmissionSpectroscopyC1109 Practice for Analysis of Aqueous Leachates fromNuclear Waste Materials Using Inductively CoupledPlasma-Atomic Emission SpectroscopyD197
8、6 Test Method for Elements in Water by Inductively-Coupled Plasma Atomic Emission SpectroscopyD4951 Test Method for Determination of Additive Elementsin Lubricating Oils by Inductively Coupled PlasmaAtomic Emission SpectrometryD5184 Test Methods for Determination of Aluminum andSilicon in Fuel Oils
9、by Ashing,Fusion,InductivelyCoupled Plasma Atomic Emission Spectrometry,andAtomic Absorption SpectrometryD5185 Test Method for Multielement Determination ofUsed and Unused Lubricating Oils and Base Oils byInductively Coupled Plasma Atomic Emission Spectrom-etry(ICP-AES)D5600 Test Method for Trace Me
10、tals in Petroleum Coke byInductively Coupled Plasma Atomic Emission Spectrom-etry(ICP-AES)D5708 TestMethodsforDeterminationofNickel,Vanadium,and Iron in Crude Oils and Residual Fuels byInductively Coupled Plasma(ICP)Atomic EmissionSpectrometryD6130 Test Method for Determination of Silicon and OtherE
11、lements in Engine Coolant by Inductively CoupledPlasma-Atomic Emission SpectroscopyD6349 Test Method for Determination of Major and MinorElements in Coal,Coke,and Solid Residues from Com-bustion of Coal and Coke by Inductively CoupledPlasmaAtomic Emission SpectrometryD6357 Test Methods for Determina
12、tion of Trace Elements inCoal,Coke,and Combustion Residues from Coal Utiliza-tion Processes by Inductively Coupled Plasma AtomicEmission Spectrometry,Inductively Coupled PlasmaMass Spectrometry,and Graphite Furnace Atomic Ab-sorption Spectro1This practice is under the jurisdiction of ASTM Committee
13、D02 on PetroleumProducts,Liquid Fuels,and Lubricants and is the direct responsibility of Subcom-mittee D02.03 on Elemental Analysis.Current edition approved July 1,2020.Published July 2020.Originally approvedin 2006.Last previous edition approved in 2019 as D7260 19.DOI:10.1520/D7260-20.2For referen
14、ced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe ASTM website.*A Summary of Changes section appears at the end of this standardCopyright AST
15、M International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United StatesThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards
16、,Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade(TBT)Committee.1D7040 Test Method for Determination of Low Levels ofPhosphorus in ILSAC GF 4 and Similar Grade EngineOils by Inductively Coupled Plasma Atomic EmissionSpectrometryD7111 Test Method for Determination of Trace Elements inMiddle Distillate Fuels by Inductively Coupled PlasmaAtomic Emission Spectrometry(ICP-AES)D7303 Test Method for Determination of Metals in Lubri-cating Greases by Inductiv
