1、 D 7582-15 STANDARD TEST METHODS FOR PROXIMATE ANALYSIS OF COAL AND COKE BY MACRO THERMOGRAVIMETRIC ANALYSIS 2017 ():17.03.2017:3110-17/ASTM -,.9,-49,-1,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA
2、 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohoc
3、ken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for AS
4、TM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 7582-15 1 D 7582-15 1 D 7582;,.().1.1.1 ,D 2013 D 346.1.2 ,.1.3 D 3173,D 3174 D 3175 .1.4,.1 ASTM D05 ,D05.21 .15 2015.2015.2009.2012.D 7582-12.DOI:10.1520/D7582-15.AS
5、TM D 7582-15 2 1.5 ,.,.2.2.1 ASTM:2 D 121,D 346 D 2013 D 3173 D 3174 D 3175 D 3176 D 3180 D 3302 D 5016 -E 691 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 7582-15 3 3.3.1 ,.D 121.4.4.1 ,.1.,.,.,.950 7.4.2 ,.4.3 .ASTM D 7582-15 4 .4.4 ,.4.5 ,.,.,(),.3 4.6 .,(),D 31
6、73,D 3174 D 3175.,.,3 Riley J.T.,Yanes E.G,Marsh M.,Lawrenz D.,Eichenbaum L.,ASTM,Testing and Evaluation,2010,38(4).458-466.ASTM D 7582-15 5 ,.D 3173,D 3174 D 3175.16.2 ,.3 5.5.1 ,D 3180.5.2 D 3302 ,D 3180 .5.3 ,(.1).1 ,.,.,.5.4 (1),(2)D 3176,(3),ASTM D 7582-15 6 ,(4),.5.5 (1),(2),(3).5.6 ,100 ,.5.7
7、 ,.6.6.1 -,.7.7.1 (MacroTGA),.MacroTGA-,.,ASTM D 7582-15 7 .30 45/950.,.,.0,1.,.MacroTGA-,.7.2 ,.,.8.8.1 (99,5%),(99,5%),1,9/(-10).8.2 (99,5%)(99,5%).8.3 (99,5%).8.4 (),10.1,.().ASTM D 7582-15 8 D 3173,D 3174 D 3175.,(),.9.9.1 ,.9.2 ,.10.10.1 ,250 (60)D 2013 D 346.11.11.1 ,.,.11.2 ,ASTM D 7582-15 9
8、,.11.3 MacroTGA-,.,.,0,05%10 ,.0,05%0,0005 1,0000.,D 3173 D 3174.,.12.12.1 .,.().(),D 3173,D 3174 D 3175.ASTM D 7582-15 10 13.13.1 ,.,.13.2 ,:13.2.1 11,.1 0,1 ,.13.2.2 107 3.,0,4 1,4 (.8.1).,(.11.3).,1.13.2.3 MacroTGA-(,).ASTM D 7582-15 11 13.2.3.1 0,7 1,4 .,26 30 107 950 20(.2).7.MacroTGA-.2 ,.-.(2
9、6 30)(TGA-30 45/),.GA-950 .13.2.3.2 ,.,.ASTM D 7582-15 12 .13.2.4 950 600.(,).,750 15 1,950 20 1.,0,4 0,5 ,1,3 1,4 .,(.11.3).,2 ,3 .13.3 :13.3.1 13.2.1.13.3.2 13.2.2.13.3.3 13.2.3 13.2.3.1.13.4 :13.4.1 13.2.1.13.4.2 13.2.2.ASTM D 7582-15 13 13.4.3 ,500 10C 1.,500 750 15C 1,500 950 20C 1.,0,4 0,5 ,1,
10、3 1,4 .,(.11.3).,2 (),3 ().(.13.4.3.1).13.4.3.1 ().,.,;D 5016,(SO3).,.13.5 :ASTM D 7582-15 14 13.5.1 ,13.2.1 .13.5.2 ,13.2.2.13.5.3 ,13.4.3.3 MacroTGA-,(.),.3 14.14.1 -,.14.2 ,:M=(W B)/W 100(1):W-,-,.14.3 ,V,:V=(B C)/W 100(2)ASTM D 7582-15 15:-,.14.3.1 ,:D=(W C)/W 100(3):D-,%.V=D M(4)14.4 ,A,:A=(F G
11、)/W 100(5):F-,G-,.14.5 ,H,:H=100 (M+A+V)(6),.15.15.1 :15.1.1 (,),.15.1.2 ,:()ASTM D 7582-15 16 ;()(),.15.1.3 ,/,.15.1.4 ,.D 3180.16.16.1 ,.1 2.,(Sr,)(SR,R),.A1.1 A1.2.1 (r)(R),%r R (-)1,29-21,66 0,21 0,69 ()1,28-21,62 0,25 0,79 ()2,93-16,73 0,19 0,31 (),22,38-36,41 0,36 1,32 (),/39,5-46,42 0,84 1,83
12、 16.1.1 (r),250 (60),ASTM D 7582-15 17 ,95%.4 MacroGA-,.2 (r)(R),%r R 0,15-0,97 0,11 0,27 ()0,31-9,69 0,09 0,12 ()1,02-11,47 0,36 1,12 16.1.2 (R),250 (60),95%.3 ,1 (1 ).1 2%()-0,047 (),0,217 ()40C/30C/0,127 ()0,45 ASTM D 7582-15 18 16.2 :16.2.1 ,.-,.16.2.2 ,(.A1.1 A1.2),.,MacroTGA-,(),D 3180.MacroTG
13、A-.16.2.3,.,95%,.3.,.A1.1 1.2,.X1.1 X1.2.16.2.4 ,ASTM D 7582-15 19 ,.,.4.4 ,()1 2 ,(),()(),16.3 ,E 691,2008.RR:D05-1038.4 17.17.1;,MacroTGA-;.4 -ASTM International RR:D05-1038.ASTM D 7582-15 20 ()A1.A1.1 ,(Sr,r)(SR,R),.A1.1 A1.2.A1.2:,5,68 5,84%.I(r)0,21%.0,16%I(r)=0,21%.,95%,.A1.3:,5,76%,6,58%.I(R)
14、0,69%,0,82%.I(R)=0,69%,95%;,.5 5 ISO 5725-6:1994 -6:ASTM D 7582-15 21 A1.1 (Sr,r)(SR,R),40-45C =1,.,ASTM D 7582-15 22 A1.2 (Sr,r)(SR,R),()X1.X1.1 ,A 4 (2 ).,()ASTM D 7582-15 23 X1.2 ,3 .X1.3 40/30/40/-30/ASTM D 7582-15 24 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.