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ASTM_D_7797_-_18.pdf

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1、Designation:D779718An American National Standard583/15Standard Test Method forDetermination of the Fatty Acid Methyl Esters Content ofAviation Turbine Fuel Using Flow Analysis by FourierTransform Infrared SpectroscopyRapid ScreeningMethod1,2This standard is issued under the fixed designation D7797;t

2、he number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope*

3、1.1 This test method specifies a rapid screening methodusing flow analysis by Fourier transform infrared(FA-FTIR)spectroscopy with partial least squares(PLS-1)processing forthe determination of the fatty acid methyl ester(FAME)content of aviation turbine fuel(AVTUR),in the range of10 mgkg to 150 mg

4、kg.NOTE1Specifications falling within the scope of this test method are:Specification D1655 and Defence Standard 91-91.NOTE2This test method detects all FAME components,with peak IRabsorbance at approximately 1749 cm-1and C8to C22molecules,asspecified in standards such as Specification D6751 and EN

5、14214.Theaccuracy of the method is based on the molecular weight of C16to C18FAME species;the presence of other FAME species with differentmolecular weights could affect the accuracy.NOTE3Additives such as antistatic agents,antioxidants and corrosioninhibitors are measured with the FAME by the FTIR

6、spectrometer.However the effects of these additives are removed by the flow analysisprocessing.NOTE4FAME concentrations from 150 mg/kg to 500 mg/kg,andbelow 10 mg/kg can be measured but the precision could be affected.1.2 The values stated in SI units are to be regarded asstandard.No other units of

7、measurement are included in thisstandard.1.3 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this standard to establish appro-priate safety,health,and environmental practices and deter-mine the applicability of

8、 regulatory limitations prior to use.1.4 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recom-mendations issued by the World Tra

9、de Organization TechnicalBarriers to Trade(TBT)Committee.2.Referenced Documents2.1 ASTM Standards:3D1298 Test Method for Density,Relative Density,or APIGravity of Crude Petroleum and Liquid Petroleum Prod-ucts by Hydrometer MethodD1655 Specification for Aviation Turbine FuelsD4052 Test Method for De

10、nsity,Relative Density,and APIGravity of Liquids by Digital Density MeterD4057 Practice for Manual Sampling of Petroleum andPetroleum ProductsD4177 Practice for Automatic Sampling of Petroleum andPetroleum ProductsD6300 Practice for Determination of Precision and BiasData for Use in Test Methods for

11、 Petroleum Products andLubricantsD6751 Specification for Biodiesel Fuel Blend Stock(B100)for Middle Distillate FuelsE1655 Practices for Infrared Multivariate QuantitativeAnalysis2.2 CEN Standards:4EN 14214 Specification Automotive FuelsFatty AcidMethyl Esters(FAME)for Diesel EnginesRequirementsand T

12、est Methods1This test method is under the jurisdiction of ASTM Committee D02 onPetroleum Products,Liquid Fuels,and Lubricants and is the direct responsibility ofSubcommittee D02.J0.05 on Fuel Cleanliness.Current edition approved Dec.1,2018.Published January 2019.Originallyapproved in 2012.Last previ

13、ous edition approved in 2017 as D7797 17.DOI:10.1520/D7797-18.2This standard has been developed through the cooperative effort betweenASTM International and the Energy Institute,London.The IP and ASTM logosimply that the ASTM and IP standards are technically equivalent,but their use doesnot imply th

14、at both standards are editorially identical.3For referenced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe ASTM website.4Available from Americ

15、an National Standards Institute(ANSI),25 W.43rd St.,4th Floor,New York,NY 10036,http:/www.ansi.org.*A Summary of Changes section appears at the end of this standardCopyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United StatesThis international standard

16、was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade(TBT)Committee.1 2.3 Energy Institute Standards:5IP 583 Test Method for Determination of the Fatty AcidMethyl Esters Content of Aviation Turbine Fuel UsingFlowAnalysisbyFourierTransformInfraredSpectroscopyRapid Screening Method2.

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