1、 4457:D664-182:177/96 STANDARD TEST METHOD FOR ACID NUMBER OF PETROLEUM PRODUCTS BY POTENTIOMETRIC TITRATION 2019 ():15.02.2019:3612-19/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,
2、USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA
3、19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM Inte
4、rnational or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D664-182 1 4457 :D664-182 :177/96 1 D664;,.().1 13.3.1 2018.2 16.1.1.1 16.1.2.1 2019.1.*1.1 ,1 ASTM D02 ,D02.06 .1 2018.2018.1942.2017.D664-17.DOI:10.1520/D0664-1802.ASTM-IP 19
5、64.ASTM D4739 D664 .ASTM D664-182 2 .1.1.1 A ,-2-.,10-9;,10-9,.,10-9.,0,1/KOH 150/KOH.1.1.2 B .,.1 ,.1.2 ,.,.2 ,D974 D3339.ASTM D664-182 3 ,.3 D664 .1.3,.1.4 ,.,.1.5 -,(TBT).2.2.1 ASTM:2 D974 D1193 D3339 -D4057 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D664-182 4
6、D4177 E177 ASTM.3.3.1:3.1.1 ,.3.1.1.1 ,-2-,.3.1.1.2 .,.3.1.1.3 .,.ASTM D664-182 5 4.4.1 ,.,-.,.5.5.1 ,.5.2 ,ASTM D664-182 6 .6.6.1 :6.1.1 ,0,005 0,002 0,5,6.1.2 6.1.3,0,2 20.,.4 ,5 1012,1000,.6.1.2 ,.6.1.3 ,/-(Ag/AgCl),1-3 LiCl .6.1.3.1 Ag/AgCl,ASTM D664-182 7,.,1-3 LiCl .,.5 ,.6.1.4 ,.6,30 45.6.1.4
7、.1 ,.6.1.5,10,0,05 0,02.,100 130 .,2.6.1.6 ,250,125 ,.ASTM D664-182 8 6.1.7 ,.6 ,.6.2 :6.2.1 ,.,6.1,.6.2.2 .0,5,0,05.6.2.3 50,50 0,5.6.2.4 2,0,A.6.2.5 250,125 ,.7.7.1 .,ASTM D664-182 9 3,.,.7.1.1 ,.7.1.2 ,.7.2 ,I,II III D1193.7.3 ,.7.4.(,).7.5 ,LiCl.7.6 ,1-3 (LiCl).7.7 ,(.)7.8-2-,(0,1%2).(.),5%,95%.
8、3 ,American Chemical Society,Washington,DC.,.Annual Standards for Laboratory Chemicals,BDH Ltd,Poole,Dorset,U.K.,and United States Pharmacopeia and National Formulary,U.S.Pharmaceutical Convention,Inc.(USPC),Rockville,MD.ASTM D664-182 10 ,Linde Type 4,10 .7 ,-2-,.,.7.9 4,7 10 ,.8.8.1 Ag/AgCl,1-3 LiC
9、l ,.,().LiCl.,LiCl .8.2 -,.,4.ASTM D664-182 11 1.7.1.162 (20 25).162,.162,().8.2.1 ,.,.8.3 ,.,.8 .1 .8.3.1 ,(1 ),.,.1 LiCl .,ASTM D664-182 12 ,.8.3.2 (4,5 5,5)5.-2-.8.3.3 ,LiCl.,HCl 4,5 5,5.,.8.3.3.1 3 6,.(.8.2).9.9.1 ,.9 .,.9.2 4 10,5,ASTM D664-182 13 2 ,.,.10.10.1 D4057()D4177().10.1.1 ,.10.1.2 ,.
10、10 ,.A 11.11.1.7.11.2 (HCl)1,19.(,.)11.3.(.)11.4 ,(0,1/).(.11.2 7.8.)9 (HCl,ASTM D664-182 14 1,19)1 -2-.,0,0005,8 ()0,1/KOH,125 ,CO2.11.5 ,(0,1/).(.7.7 7.8.).6 (KOH)1 -2-.10.,.,(CO2),.,0,0005/,CO2.11.6 5 0,2 495 5 -2-.500 5 .(.),.11.7.(.)12.12.1 250-.1()(.ASTM D664-182 15.11)125 (.12).,125-.1(b)60 .
11、8.1.,.,.11 ,.,.,.12 ,(.),.,.1.()125 (b)60 ,0,05-1,0 20,0 2,0 0,10 0,05-1,0 10,0 1,0 0,10 1,0-5,0 5,0 0,5 0,02 1,0-5,0 2,5 0,25 0,02 5-20 1,0 0,1 0,005 5-20 0,5 0,05 0,005 20-100 0,25 0,02 0,001 20-100 0,25 0,02 0,001 100-260 0,1 0,01 0,0005 100-260 0,1 0,01 0,0005 12.2 ,0,1-/ASTM D664-182 16 ,25 .()
12、.12.3 :12.3.1 0,1/,.12.3.2 (),0,1 0,1/30,0,05.12.3.3 (),0,1 0,1/30,30.12.3.4 ,5/0,1 ,.12.3.5 ,-2-,.5,.5-2-,.,8.1.8.3.3.12.4 :12.4.1 ASTM D664-182 17,.12.4.2 ,.,4.,.12.4.3 0,1/.,.,5 15 .0,05 0,5.,10 10.60.12.4.4 ,10 200.,.13.1.1.12.4.5 .2-.pH 4,5 5,5 3 5 .2-ASTM D664-182 18 ,.,.,.,45,2-,3-5 pH 4,5 5,
13、5 .2-,.,2-.,.,.,8.1.8.3.3.13 0,1 ,0,01 0,05;20;(0,05),.12.5 :12.5.1 125 60,.0,1/0,01 0,05,ASTM D664-182 19 .,.,0,01 0,05.,.12.5.2 ,125 60,.0,1/HCl 0,01 0,05 ,12.5.1.13.13.1 0,1/(.1).(.14),.(.1 ),.14 ,0,05-15,30%,.,ASTM D664-182 20 .13.1.1 .,.:125 .10,00 125 .,.10,00 ,125 .,.D 10,00 ,125 .,.1 ,0,1 AS
14、TM D664-182 21 13.1.2 ,(10)(4),.15 ,.13.2 ,12.4,.13.3 ,13.3.1,.13.3.1 :,/=()56,1/W(1),/=(CM+Dm)56,1/W(2):-,10,10,.,.-,-,/,-HCl,/,ASTM D664-182 22 W-,-,4,D-HCl,.14.14.1 ,.16 ,.14.2 ,.4 14.3 ,.4 .,.14.4 ,.4 ASTM MNL 7,6-,ASTM International,W.Conshohocken,PA.ASTM D664-182 23 ,.,.,.14.5,.,.15.15.1 ,:.,.
15、,.:(D664,)=()(3)(D664,)=()(4)15.2 ,.ASTM D664-182 24 16.5,6 16.1 :16.1.1 (r),20.16.1.1.1 ,.,60:,KOH/60 (5)=0,1938 X0,8199 (pH 10),KOH/60 (6)=0,3456 X0,9758 :X=.16.1.2 (R),5 -ASTM International RR:D02-1551.ASTM Customer Service serviceastm.org.6 -ASTM International RR:D02-1869.ASTM Customer Service s
16、erviceastm.org.ASTM D664-182 25 ,20.16.1.2.1 ,.,60:,KOH/60 (7)=0,4022 X0,8199 (pH 10),KOH/60 (8)=0,5542 X0,9758 :X=.2.60 125 ,60 60 125 125 r,r,(pH 10)r,r,(pH 10)0,1938 X0,8199 0,3456 X0,9758 0,1275 X1,0431 0,2028 X1,0513 5 KOH/0,73 1,71 0,68 1,10 1 KOH/0,19 0,35 0,13 0,20 R,R,(pH 10)R,R,(pH 10)0,4022 X0,8199 0,5542 X0,9758 0,2188 X1,0431 0,3160 X1,0513 5 KOH/1,50 2,67 1,17 1,72 1 KOH/0,40 0,55 0,22 0,32 16.2 :16.2.1 ,.ASTM D664-182 26 16.3 ,.B 17.17.1.7.17.2 ,(0,1/)(.7.7 7.8.).0,56 (KOH)1 -2-,1
