1、 4716 D874-13a(2018.)STANDARD TEST METHOD FOR SULFATED ASH FROM LUBRICATING OILS AND ADDITIVES 2018 ():17.09.2018:3547-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM Inter
2、national ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM
3、 International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or F
4、BU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D874-13(2018)1 4716 D874-13a(2018.)1 D874;,.().1.1.1 ,.:,.,.1 ASTM D02 ,D02.03 .1 2018.2018.1946.2013.D874-13.DOI:10.1520/D0874-13AR18.IP .ASTM D874-13(2018)2 1.2 0,02%,.0,005%.1 ,.,D482.2 ,
5、.,.3 ,.1.3,(FAME),EN 14213 EN 14214,.1.4,.1.5 ,.,.1.6 -,ASTM D874-13(2018)3 ,(TBT).2.2.1 ASTM:2 D482 D1193 D4057 D4177 D6299 2.2 CEN:3 EN 14213 (FAME)EN 14214 (FAME)3.3.1:3.1.1 ,.2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 (CEN),Avenue Marnix 17,B-1000,Brussels,Belgium
6、,http:/www.cen.eu.ASTM D874-13(2018)4 4 4.1 ,.775,.,775 .5.5.1 ,.,(.4).,.4 ,.5.2 ,.,.,.4 4 Nadkarni R.A.,Ledesma R.R.Via G.H.,“Sulfated ash TM:Limitations of Realiability and Repeoducibility,”SAE 952548,SAE,400 Commonwealth Drive,Warrendale,PA 15096-0001,U.S.A.ASTM D874-13(2018)5 6.6.1 ;50 100 ,0,02
7、%,120 150 ,0,02%,.(,.)5 ,0,1%,.,13 ,.6.2 775 25 .6.3,0,1.7.7.1 .,.5 ,5“Reagent Chemicals,American Chemical Society Specifications”,Am.Chemical Soc.,Washington,DC.,.”Annua Standards for Laboratory Chemicals,”BDH Ltd.,Poole,Dorset,U.K.,and the United States Pharmacopeia,and National Formulary,U.S.Phar
8、macopeial Convention,Inc.,(USPC),Rockville,MD.ASTM D874-13(2018)6,.7.2 ,II III,D1193.7.3 (),.6 ,9.1 9.11,100 ,0,5 120 150.9.11.7.4 (1,84)(H2SO4).(.-.)7.5 (1+1)1 (1,84)1 .(.,.)7.6-2-,(,.),99%.7.7,(,.),99%.7.8 (QC),.QC 12.ASTM D874-13(2018)7 8.8.1 D4057 D4177.,.9.9.1 (.9.3).9.2 ,775 25 10.0,1.7 ,.9.3
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10、11 ,0,02%,1 ,775 25 30 5.(.7)0,1.,1 ,.,w,.6 -ASTM International RR:D02-1597.ASTM Customer Service serviceastm.org.ASTM D874-13(2018)10 10.10.1 :,%=(w/W)100(2):w-,W-.11.11.1 0,001%,0,02%,0,01%,D874.12.12.1 QC(.7.8).12.1.1 QC/(QA),.12.1.2 QC/QA ,QC/QA 1.13.6 13.1 ,:ASTM D874-13(2018)11 13.1.1 0,005%0,
11、10%:13.1.1.1 ,:r=0,047X0,85(3).13.1.1.2 ,:R=0,189X0,85(4).13.1.1.3 .1.10 0,005%0,10%ASTM-IP,1975.1.0,10%,%0,005 0,0005 0,0021 0,010 0,0009 0,0038 0,05 0,0037 0,0148 0,10 0,0066 0,0267 ASTM D874-13(2018)12 13.1.2 0,11%25%:13.1.2.1 ,:r=0,060X0,75(5).13.1.2.2 ,:R=0,142X0,75(6).13.1.2.3 .2.2.0,10%,%0,5
12、0,036 0,084 1,0 0,060 0,142 5,0 0,201 0,475 10,0 20,0 25,0 0,337 0,567 0,671 0,799 1,343 1,588 11 0,10%25%ASTM-IP,1981.ASTM D874-13(2018)13 13.1.3 ,2006.,API PC 107,:8 :0,8%1,6%:0,08068 X1,40:0,1563 X1,40 13.1.4 .3.3.API PC 10 ,%0,80 0,06 0,11 0,90 0,07 0,13 1,10 0,09 0,18 1,60 0,16 0,30 13.2 ,.14.1
13、4.1;7 (API),(API),1220 L.St.,NW,Washington,DC 20005-4070,http:/www.api.org.8 -ASTM International RR:D02-1625.ASTM Customer Service serviceastm.org.ASTM D874-13(2018)14 ()1.1.1 QC.1.2 ,QC(.D6299 MNL 7).9 1.3 QC ,(.D6299 MNL 7).,().1.4 ,QC ,.QC .QC ,.,QC .QC ASTM,.1.5,QC,.QC 9 MNL 7,Mannual on Present
14、ation of Data Control Chart Analysis,6th ed,ASTM International,W.Conshohocken,PA.ASTM D874-13(2018)15,.D6299 MNL 7 QC .ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.
