1、 D7876-13(2018.)(/)STANDARD PRACTICE FOR PRACTICE FOR SAMPLE DECOMPOSITION USING MICROWAVE HEATING(WITH OR WITHOUT PRIOR ASHING)FOR ATOMIC SPECTROSCOPIC ELEMENTAL DETERMINATION IN PETROLEUM PRODUCTS AND LUBRICANTS 2018 ():17.09.2018:3543-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:inte
2、rstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license o
3、f American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be consid
4、ered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D7876-13(2018)1 D7876-13(2018.)(/)1 D7876;,.().1.1.1 .1.1.1 ,-(-)-(),-,
5、.1 ASTM D02 ,D02.03 .1 2018.2018.2013.2013.D7876-13.DOI:10.1520/D7876-13R18.ASTM D7876-13(2018)2 1.2 ,.1.3 D02,.1.3.1 .1.1.()A Abu Samra et al(1)Barrett et al(2)West et al(3)Matthes et al(4)-Nadkarni(5)-Nadkarni(5)-Feng et al(6)-Fox(7);Nadkarni(8)-Hwang et al(9)-Xie et al(10)-Wondimu et al(11)-Woodl
6、and et al(12)AAS;ICP-AES Kingston and Jassie(13)AAS;ICP-AES Kingston and Haswell(14)ICP-MS Ivanova et al(15)A .ASTM D7876-13(2018)3 1.3.2 ASTM X1.1.4 .,.,-.1.5 ,.,.1.6 NIST().,.1.7 D7455.1.8,.1.9 ,.ASTM D7876-13(2018)4 ,.6 7.1.10 -,(TBT).2.2.1 ASTM:2 C1234 C1347 C1463 ,D482 D874 D1193 D1506 2 ASTM,A
7、STM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D7876-13(2018)5 D2216 ()D4057 D4177 D4309 -D4628 ,D4643 D4951 -D5185 -(-)D5258 D5513 D5765 D5862 6V92TA(2009.)3 3 www.astm.org.ASTM D7876-13(2018)6 D6010 (2016.)3 D6792 ,D7260 ,-(-)D7303 -D7455 D7740 ,-E1358 E1645 2.2 :CFR()1030.1
8、0 FCC Rule()18 ,ASTM D7876-13(2018)7 3.3.1:3.1.1 -,.D7740 3.1.2 ,.D5862 3.1.3 ,.D7740 3.1.4 ,.D6792 3.1.5 .3.1.5.1 .D7740 3.1.6-,.,.ASTM D7876-13(2018)8 3.1.7 (),.3.1.7.1 ,.D6792 3.1.8 (),.D7740 4.4.1 ,().-.,.4.1.1 -(-);/;ASTM .4.2 ,.ASTM D7876-13(2018)9 5.5.1 -,.,.5.2 ,.,.,.,(9).5.3 ,.5.4 ,.ASTM D7
9、876-13(2018)10 .,.,.,.(/).,.,(5).5.4.1 .,.,.,.,-,ASTM D7876-13(2018)11 ,(16).5.4.2 ,(,).,.,240C 800 .,CO2.,.,.,.,CO2.,ASTM D7876-13(2018)12 ,(17).5.4.3 ,CO2 NOx.,.,1 (18).5.4.3.1 ,200C 260C.,.,.-,(19).5.4.4 ,.,.,(20).ASTM D7876-13(2018)13 6.6.1 ,0,001 0,0001,150.6.2-,.2.,-,393,1;309,27 167,038;308,2
10、2;396,15;309,27 217,58 206,83;217,58;231,15 553,6 223,53;233,527;455,40;493,41 249,77 249,77;208,96 422,67 315,88;317,93;364,4;396,85;422,67 357,87 267,72;357,87 324,75 324,75;327,40 248,3;372,0 238,20;259,94 670,78 670,78;610,36;460,29 285,2 279,08;279,55;280,278;,285,21 279,2 257,61;293,31 313,3 1
11、35,387;202,03;281,62 232,0;341,48 231,60;341,48 -177,51;178,29;213,62;214,91;253,40 766,49 766,49;404,72 251,618 288,16;251,618 589,595 589,595 318,4 292,40;290,88 213,86;398,8 202,55;206,20;213,86;334,58;481,05 6.3-,.2.ASTM D7876-13(2018)14 ,190 -.6.4 ,.1%1.,2,8 3/(100./).,.,100 .6.4.1 (CFR)1030.10
12、,(C)(1),(C)(2),(C)(3),.(FCC)FCC 18.6.5 ,(),100 .100 .200C,0,2 .(,100-0,2 ,100 .).,ASTM D7876-13(2018)15 .6.5.1 ,.1 ,.6.5.2 .(,().6 9).6.6 ,.,(1:1)60C 10.,.6.7 ,(,),.,.45,30.(30 435 .).ASTM D7876-13(2018)16 .6.8 ,.3/.(,.,).6.9 ,250.6.10 ,25,50 100.6.11 ,525C 25C 250-.,.(,).6.12 ,-.6.13 ,.ASTM D7876-1
13、3(2018)17 7.7.1 .-,.,.,.7.2 ,/,.(.).(,.HF ,).7.3 ,.,.7.3.1 .ASTM D7876-13(2018)18 7.4,;,II ,D1193.7.5 (),.8.8.1 ,.D4057 D4177.,.9.9.1 :9.1.1 ,D482 D874,.9.1.2 Meeker .9.1.3 .1 ,2 525C.1.ASTM D7876-13(2018)19 2 ,.9.2 :9.2.1 1 10 .30 .(.,).3 ,.0,1 .9.2.2 50-.9.3 :9.3.1 0,1 1 -.4 (,),.,ASTM D7876-13(20
14、18)20 ,.9.3.2 125 15.190 15.1 .25-.,.(/.).4 ,.5 ,0,10 .,1.6 .9.3.3 .2,5C 2.7 ,.ASTM D7876-13(2018)21 9.3.4 .,()(,(80C,)(1:1),(80C,)(1:1),.,.,.(10%),.8 .9.3.4.1 ,.9.3.5 (,)./,.ASTM D7876-13(2018)22 ,.(,.).,.9.3.5.1 ,1;1.9.3.5.2 ,(,).9.3.6 .,.9.3.7 ,.,.5 .9.3.7.1,.ASTM D7876-13(2018)23 9.3.8 .9.3.8.1
15、,125 15,190 15.9.3.8.2 ,575 635,50 100%.635 700,30 100%.164C 4C.180C .,700,.9 ,.9.3.8.3 .9.3.9 ,.,.ASTM D7876-13(2018)24 9.3.10 360 .,.9.3.11 .,.,.,.(,.).(.,.,.,.(ASTM D7876-13(2018)25 ).(),.).().,.).(,().,).(,).9.3.12 ,.ASTM D7876-13(2018)26 ,15 ,.9.3.13 ,().(,),.().9.3.13.1 ,.9.3.13.2 ,.,.9.3.14 2
16、5-50-.9.3.15 ,.0,5,.10%.,.ASTM D7876-13(2018)27 9.3.16 -,.10 ,.11 ,.,.HF,HF.HF ,.HF ,.HF,.,.12 ,(10%);,.CO2,.9.4 :9.4.1 -.9.4.2 -.2.,.ASTM D7876-13(2018)28 13 ASTM,D4628 ,D4951 D5185 -.-D7740 D7260,.10.10.1 ,.11.11.1-;-;()X1.X1.1 ASTM .X1.1.1 D1506:16 ,2-6 550C 25C.ASTM D7876-13(2018)29 X1.1.2 D4643:().D2216,.X1.1.3 E1358:.,.,600.X1.1.4 D5258:-.100 .X1.1.5 D5765:./,150C.X1.1.6 D6010:,ASTM D7876-13(2018)30 -.1-5 ,115C 30 -(1+1).,.-.X1.1.7 C1347:,.X1.1.8 ,C1463:HF NHO.,-.X1.1.9 D4309:,.X1.1.10 D55
