1、 D 602112 STANDARD TEST METHOD FOR MEASUREMENT OF TOTAL HYDROGEN SULFIDE IN RESIDUAL FUELS BY MULTIPLE HEADSPACE EXTRACTION AND SULFUR SPECIFIC DETECTION 2013 ():2119-13/ASTM :23.09.2013 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM Internat
2、ional)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM In
3、ternational)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the spe
4、cified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 6021-12 1 D 602112 1 D 6021;,.()1.1.1 (H2S),D 396(4,5(),5()6),H2S 0,01 100/().1.2,1 ASTM D02 ,D02.E0 ,.15 2012.2012.1996.
5、2006.D 6021-06.DOI:10.1520/D6021-12.ASTM D 6021-12 2.1.3 ,.,.7.5,8.2,9.2,10.1.4 11.1.2.2.1 ASTM:2 D 396 D 1193 D 2420 (LP)()D 3609 D 4057 D 4084 ()D 4323 D 5504 D 5705 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 6021-12 3 D 7621 3.3.1:3.1.1 ,40 5,5 24,0 2/,.3.1.2
6、,40 C 5,5 24,0 2/,.3.1.3 ,.3.1.4 ,100 C 5,0 50,0 2/,.4.4.1 ,(1 4,24),.,-.4.2 ()0,05 5,0 ASTM D 6021-12 4 ()5 15 60.,.3 ,H2S(.D 4084 D 4323),(.D 5504).4.3 5,.,(-).4.4 ()().,(),H2S /().5.5.1 H2S ,H2S 3 H2S :,Silva.,Carvajal N.Gonzalez A.,1620 1992,N.J.ASTM D 6021-12 5 .,.H2S H2S;.,H2S.5.1.1 H2S ,H2S .
7、5.2 ,H2S .1 D 6021 H2S ,.:1)D 5705 ,H2S .2)D 7621 -,H2S .5.3 H2S ,.H2S 1/(/)()ASTM D 6021-12 6 50 100/(),.2 -,H2S H2S .6.6.1 ,1.:6.1.1 ,3,2 (1).6.1.2 ,316,3,2 (2).6.1.3 (PTFE),0,5,2,5 10 H2S 1 100,0,1 50 0,01 10 ,.6.1.4/,6,3,100 200,5 0 200.6.1.5 ,3,2 (3).6.1.6-H2S,H2S 1 10000 2%ASTM D 6021-12 7.3 .
8、6.1.7 ,0,6 3,2,.6.2-,3,2,0,2 100/.6.3 ,60 0,5 C 30 30 30.6.4 ,0,01 250.6.5 ,.6.6 H2S ,H2S (.D 5504).6.7 ,20.7.7.1 .,ASTM D 6021-12 8.4 ,.7.2 50 (CH3COOH)1 II D 1193 1 5%-.1 7.3 ,20,()().4 ,DC.,.,BDH Ltd.,Poole,Dorset,Pharmacopeial Convention,Inc.(USPC),MD.-(2)/(3)-(1)(1,6)(2)-60 ASTM D 6021-12 9 7.4
9、 (),30,60 120 ,20.7.5 ,1,10 100/H2S ().(!).7.6,(H2S),-.7.7 D 2420 ,.,.4 .7.2 7.7 H2S .7.8 ,(PTFE)(3,2).7.9 (-),20,PTFE-/,.7.10 ,-(3,2 1,6).7.11 ,().8.8.1 H2S 250 500 D 4057.60,ASTM D 6021-12 10 .8.2 ,(!).8.3 (-1 4,24),().2 9.9.1 1.9.2-H2S (!,H2S ASTM D 6021-12 11 ).10.10.1 :10.1.1 ,1/(0,1/),10/(1/)1
10、00/(10/)-120,60 30,.5 (/),/,-,.10.1.2 /(PTFE-,),.10.1.3 ,(.2),.10.1.4 H2S 105 :30 3 100/.60 6 100/.100 10 120/.ASTM D 6021-12 12(!-H2S ):10.1.5 ,.10.1.6 1,0,.10.1.7 (C),().10.1.8 .10.2.1 10.2.7.6 ,H2S,D 3609(D 4084).10.2 :10.2.1 60 C 5 (15).0,5 (H2S 100/),2,5 (H2S 10/),10 (H2S 1/).2 (.1)1 ,3.70 3.10
11、.2.2 (.1),.10.2.3 1 ASTM D 6021-12 13 ,/0.1.10.2.4 2 (.1)10,-H2S.2 .A1.10.2.5 ,().10.2.6 .10.2.1 10.2.5 ,A2.10.2.7 .10.2.1 10.2.5 ,A3.,.10.2.8 A1,A2 A3 ,.(R2 0,95).R .10.3 :10.3.1 ()(1):5 5 ,.(Ioffe B.V.)(Vitenberg A.G),Wiley-Interscience,John Wiley&Sons.-,1984,.131-142.ASTM D 6021-12 14 (1):AT-(),A
12、1-(),A2-(),.10.3.2 ,H2S (2):CPVWSSHvSSH/7162.8313/10/10/0759.346622(2):W(H2S)s-H2S ,P-,Vv-,C(H2S)s-H2S ,/,34.0759-H2S,/,8313.7162-()/(K)=R=,T-,K.P=101325,Vv=120,C(H2S)s=10/T=298.15 K,:SSHW2 (101325)()(120)()(10)(/)67.115.298/7162.8313/10/10/0759.3466(3)10.3.3 (3),H2S ,:ASTM D 6021-12 15 (4):SHFR2-H2
13、S,STA-()H2S.11.11.1 ,-,.1,-.(!).11.2 H2S ().0,1,()0,05 5,0 H2S PTFE-.0,1,.11.3 ,60,5 (15).11.4 0,5,ASTM D 6021-12 16 H2S 1 100 ,2,5 H2S 0,1 50 ,10 H2S 0,01 10 .2 (.1)1 ,3.70 3.11.5 (.1),.11.6 1 ,/0.1.11.7 2 (.1),10 -H2S.2 ,A1.11.8 ,.11.9 .11.3 11.9 ,A2.11.10 .11.3 11.9 ,A3.,.ASTM D 6021-12 17 12.12.
14、1 A1,A2 A3 ,.(R2 0,95).R .12.2 H2S .12.3 ()(1).12.4 H2S (/)()H2S,(),.(4):S2H2SHFTFWARCFF(5):SHFR2-,(3),F2SHC-H2S ,/,FTA-()H2S,WF-,.12.5 .XI.13.13.1 ,95%-ASTM D 6021-12 18 ():F2SHC,/0,022 0,004 0,24 0,07 37,3 1,9 7 .(Beatriz A.Silva),Intevep,SA,Apdo 76343,1070A,.13.2 ,.13.1,.13.3 -.14.14.1 ;ASTM D 60
15、21-12 19 ()X1.X1.1 Wt A1 A2 A3 ,R2 H2S 10/()1,67 1,6508 108 1,431 108 1,2166 108 0,999 0,0792 1,7327 107 1,4242 107 1,2539 107 0,985 X1.1 H2S X1.1.:10240.110431.1106508.1106508.198828STA(1.1)/103468.110240.1 1.6799S2HFR(1.2)107318.91074242.1107327.1107327.17727FTA(1.3)/66.10792.0107318.9103468.1792F
16、SHC(1.4)ASTM D 6021-12 20 D02.0 ,(D 6021-06),.(1).5.1,5.2 5.3.(2)1.(3)D 5705 D 7621 .(4).ASTM D 6021-12 21 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).ASTM(www.astm.org/COPYRIGHT/).
