1、 D550112(2016.),20%,STANDARD TEST METHOD FOR DETERMINATION OF ETHANOL AND METHANOL CONTENT IN FUELS CONTAINING GREATER THAN 20%ETHANOL BY GAS CHROMATOGRAPHY 2019 ():26.06.2019:3703-19/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International
2、)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM Interna
3、tional)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specifie
4、d translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D5501-12(2016)1 D550112(2016.),20%,1 D5501;,.().1.1.1 ,20%.,.1.1.1 20%100%,0,01%0,6%.1 ,20%,D5599,12%,D4815.1 ASTM D02 ,D02.04.0
5、L .1 2016.2016.1994.2012.D5501-121.DOI:10.1520/D5501-12R16.ASTM D5501-12(2016)2 1.2 ,.1.3 ,D1364,.1.4 ,225 C,-,.1.5,.1.6 ,.,.2.2.1 ASTM:2 D1298 ,API D1364 ()2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D5501-12(2016)3 D4052 ,API()D4057 D4175 ,D4307 D4626 D4806 ,D4815
6、 ,TAM,1 4 D5599 -D5798 D6299 D6792 E203 E355 ASTM D5501-12(2016)4 E594 -,E1064 E1510 3.3.1 ,.D4175 E355 E594.3.2:3.2.1 ().3.2.2 (),.3.2.2.1 -.3.2.3 ,.3.2.3.1 ,ASTM D5501-12(2016)5 ,.3.3:3.3.1 3.3.2 4.4.1 ,.-,.-.,.,.,.5.5.1 -20%100%,.5.2 D4806.ASTM D5501-12(2016)6 5.3 D5798.1 100 150 15 C 60 C 12 15
7、30 C/30 C/250 C 250 C 19 23 300 C 200:1 0,1 0,5 -300 C (30/)(300/)(30/)20 -21/24/()-.6.6.1 ,1.,(,200:1).-ASTM D5501-12(2016)7 ,.,.-.6.2 .,0,1 0,5.2 ,.,.6.3 ,().,.6.3.1.6.3.1 ,(),150 0,25 1,0,100 0,25 0,5,.150-,.E1510.6.4 ,:6.4.1 80/,ASTM D5501-12(2016)8 6.4.2 ,6.4.3 ,6.4.4 ,6.4.5 (1),6.4.6 ,6.4.7 ,6
8、.4.8 ,.7.7.1 .,.3 7.2-,99,95%.().-.3 ,.,.,.,BDH Ltd.,.,.,Inc.(USPC),.,.ASTM D5501-12(2016)9 7.3 ,.99,95%.(-).(-).7.4 ,.7.4.1 ,.7.4.2 ,.,D1364 ,.-,.7.4.3 ,99,5 .0,01 .().7.4.4 ().99 ,.ASTM D5501-12(2016)10 7.4.5 ().7.4.6 -,.95%),(51%83%)(20%51%).ASTM D5501-12(2016)19 11.1.2 30 .,.D6299.12.12.1 .1.12.
9、2 ,0,002.%.12.3 0,1 0,5 .(.9.5).13.6 .7.13.13.1 ,.10.4,.13.1.1 ,(ARi),4.,.ASTM D5501-12(2016)20 ARi=areai RF(F)i(4):ARi-,(i),areai-(i),RF(F)i-()()(i)-C7.13.1.2 ,.10.4.1.2.i,ARi.,.4 150-,-ASTM D5501-12(2016)21 1 0,995 3%.5 EtOH y EtOH x x=0:y=0:.%EtOH ASTM D5501-12(2016)22 13.1.3 (),.5.,95%105%./,.%=
10、ARt(5):ARt-ARi .3 A 20 C,/15,56 C 3,20 0,791 0,796 2,06 0,789 0,794 A -=1.13.2 :(6):RMi-,ARi-,i,ARt-ARi .13.3 .D1364,E203,E1064 .ASTM D5501-12(2016)23 13.4 :Mi=RMi (100 .%)(7)100 :Mi-,RMi-6.13.5 :(8):Vi-%i,Mi-%i 7,Di-i t 3,Ds-t,D1298 D4052.6 20%(E20)150-,ASTM D5501-12(2016)24 .7 ()20%100-14.14.1 0,0
11、1%7 0,01%8 .15.4 15.1 ,:15.1.1 ,4 (2011.)ASTM International RR:D02-1749.ASTM serviceastm.org.,0.11%ASTM D5501-12(2016)25 ,.A,%,%20 99,8 2,1856 X-0,6 0,01 0,6 0,02705(X+0,1037)A X .4 ,%20 0,36 2,60 40 0,24 1,72 51 0,21 1,48 68 0,17 1,25 83 0,15 1,11 97 0,14 1,01 0,1 0,01 0,02 0,2 0,01 0,04 0,3 0,01 0
12、,05 0,4 0,01 0,06 0,5 0,02 0,07 0,6 0,02 0,09 15.1.2 ,:A%,%20 99,8 15,708 X-0,6 0,01 0,6 0,1209(X+0,1037)A X .4 4 ,.15.1.1 15.1.2.ASTM D5501-12(2016)26 15.1.3 ,.16.16.1 E85;()X1.X1.1 ,.(X1).X2.=/100(X1.1)=(1 )/1(X1.2)X1.2 .X1.3 ,.,.ASTM D5501-12(2016)27 X1.4 .0,1.,.X1.5 ,.X1.1 E75.X1.6 X1.3.%(i)=(i)
13、/100(X1.3)(i)-,-.C,B.X1.7 .(,).X1.8 10-13.ASTM D5501-12(2016)28 X1.1 75-%A B C D E 1 ,C ()2 0,251 0,250=B2 C13 0,42 3 44,887 44,67=B3 B13 74,83 4 5,998 5,97=B4 D13 10,00 5 8,565 8,57=B5 E13 14,35 6 0,14=B2 C14+B3 B14+B4 D14+B5 E14 0,23 7 0,11=B3 B12+B2 C12+B4 D12+B5 E12 0,18 8 59,701 59,701 100,00 9
14、 10 EtOH MeOH -C7 11-0,9976 0,9999 0,9950 1,0000 12 .0,0024 0,0039 0,0001 0,0000 13 0,9952 0,9960 0,9949 1,0000 14 (=1 .)0,0024 0,0001 0,0050 0,0000 X2.X2.1 ,X1,.E50 X2.1.X2.2,.,X2.1.=.%(i)/(100%)100(X2.1)ASTM D5501-12(2016)29 X2.1 E50 A B C D E F 1 ,-C (-)2 0,200 0,200=B2 C12 0,31 0,31 3 32,812 32,
15、68=B3 B12 50,65 50,70 4 31,507 31,49=B4 D12 48,81 48,86 5 0,08=B2 C13+B3 B13+B4 D13 0,12 0,12 6 0,07=B3 B11+B2 C11+B4 D11 0,11 7 64,519 64,519 100,00 100,00 8 9 EtOH purity MeOH Purity 10-0,9976 0,9999 1,0000 11 .0,0017 0,0002 0,0005 12-0,9959 0,9997 0,9995 13 0,0024 0,0001 0,0000 (=1 .)X3.,X3.1 .,.
16、X3.2 ,.ASTM D5501-12(2016)30 X3.2.1 .(0,1 0,2).(,).X3.2.2 ,.X3.2.3 (,).,(,).X3.2.4 .,.X3.3 /,-.,.,.ASTM D5501-12(2016)31 .-,.X3.4 :X3.4.1 .X3.4.2 ./.X3.5 D5501 ,.,.,.X3.6 .,.,13.X3.7 .ASTM D5501-12(2016)32 ,.X3.8 .X4.X4.1 ,().X4.2 (.D6299 75).X4.3 ,(.D6299 7).,.X4.4 ,.,(.D6792).X4.5 ASTM,5 MNL7,:8-,ASTM International,2010.ASTM D5501-12(2016)33 (.D6792).X4.6 ,(.D6299).,.X4.7,.,.X4.8 ,D6299.X4.9 .(D6299,D6792 7).ASTM D5501-12(2016)34 ASTM International -,.,.,.-ASTM International.,.,.ASTM Internati
