1、 D 5580-15 ,/-,-,C9 -STANDARD TEST METHOD FOR DETERMINATION OF BENZENE,TOLUENE,ETHYLBENZENE,p/m-XYLENE,o-XYLENE,C9 AND HEAVIER AROMATICS,AND TOTALAROMATICS IN FINISHED GASOLINE BY GASCHROMATOGRAPHY ():3059-16/ASTM :29.12.2016 2016 (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,US
2、A.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19
3、428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM Intern
4、ational or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.-,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/ASTM D 5580-15 D 5580-15 ,/-,o-,C9 ,1 D 5580;,.().1.*1.1 ,C9 ,.1.2 .,1 ASTM D02 ,D02
5、.04.0L .1 2015.2015.1994.2013.D5580-13.DOI:10.1520/D5580-15.1ASTM D 5580-15 ,-,C9 .C8,-,o-.C9 .1.3 ,:0,1 5%;1 15%;C8 0,5 10%;C9 5 30%10 80%.1.4 0,01%,.1.5 ,(D 6708)D 5580 D 3606 ,D 5580 D 3606,().,D 6708,0,0%2,31%,D 5580.,D 3606,0,0%2,38%,D 3606.1.6 ,2ASTM D 5580-15 (D 6708)D 5580 D 5769 ,D 5580 D 5
6、769,().()(),D 6708,5,4%31,6%,D 5580,T95,95%,D86 149,1C 196,6C(300,4F 385,9F).1.6.1 ,D 5769,3,7%-29,4%,T95,95%,D 86,149,1C 196,6C(300,4F 385,9F).1.7 ,.,-(MTBE),-(TBE),-()(DIPE),.,.1-,.1.8,.1.8.1 3ASTM D 5580-15.1.9 ,.,.2.2.1 ASTM:2 D 86 D 1298 ,API D 3606 D 4052 ,API()D 4057 D 4307 D 5769 ,/-2 ASTM,A
7、STM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.4ASTM D 5580-15 D 6708 ,E 355 3.3.1 ,:3.1.1 ,.3.1.2 ,1,6 (0,06);.3.1.3 ,;0,5 (0,02).3.1.4 -,-,:=(S+C)/C (1):S-,-.3.1.5 1,2,3-2-(TCEP).3.1.6 (WCOT),5ASTM D 5580-15 ().4.4.1 ,-.,2-,(TCEP).C9 ,.TCEP-,(WCOT).,-.WCOT-(C8 C10,)-.4.2 ,C12 ,TC
8、EP-.TCEP-,WCOT-.6ASTM D 5580-15 C8 -.o-WCOT-C9 -.4.3 ,(2-).,/-o-,C9 ,.,WCOT-,C9 .4.4 -,.5.5.1 ,1995.,.5.2 ,().,7ASTM D 5580-15 .6.6.1 .E 355,.1 -.()().1.6.1.1 (GC),.1 ,.1.-.6.1.2 ,.-.6.1.3 ,()(FID)(FID)(TCD)(TCD)8ASTM D 5580-15 (),.1.130 ()200-(FID)(A)250 (B)200 WCOT 60C(6)2C/115C()TCEP-(BACKFLUSH T
9、1 T2.).60C WCOT-,TCEP/WCOT-.115C WCOT-,WCOT-.-TCEP-()10/WCOT-()10/100/11:1 1 6.1.3.1 ,.,.6.1.4 -(),9ASTM D 5580-15 WCOT-.-,0,01 .6.1.4.1 -(),(BACKFLUSH)(RESET)(10.5)-.6.1.5 ,10 .1.6.1.5.1 10 1,6 (0,06).,0,32 0,8 (0,03).6.1.5.2 ,.,.,.6.1.5.3 ,.6.2 :10ASTM D 5580-15 6.2.1 ,.6.2.1.1,(r2),11.4.6.3 ():6.
10、3.1 ,.6.3.1.1.6.3.1.1 -560 (22)1,6 (1/16),0,76 (0,030)0,14-0,15 (20%)80/100 Chromosorb P(AW).,15.6.3.2 ()6.3.2.1.6.3.2.1 WCOT-,30,WCOT-0,53,5,0.11ASTM D 5580-15 7.7.1-,.-99,95%.().7.2 .,.().7.3 2,2,4-().().7.4 ,.,.,.().8.8.1 -:8.1.1 ,.12ASTM D 5580-15 .8.1.2 10 100 ,40 80/100 Chromosorb P(AW).,.,.-.
11、8.2 -:8.2.1 560 (22)1,6 (1/16)0,76 (0,030),.8.2.2 6 12 ,.0,14 0,15 .,.6,0 (0,25).8.3 WCOT-,(.6.3.2.1).9.9.1 ,.D 4057 13ASTM D 5580-15 .9.2 ,.0 5(32 40F).9.3 0 5(32 40F).10.10.1 -WCOT-(.1).,.10.2 ,.1,.10.2.1 ,WCOT-,.10.2.2,.1,6.3.WCOT-,()().14ASTM D 5580-15 10.3 (-):10.3.1 ()RESET(),(.1)10/(17 20 .).
12、1 ,.10.3.2 ,100/.,10.3.1 .11:1.(.1).10.3.3 BACKFLUSH(),10.3.1,.10.3.4 RESET()10/.(.1)10.4 ,-.()RESET,15ASTM D 5580-15 .10.5 :10.5.1 (BACKFLUSH)(RESET)10.5.1.1,10.5.1.2 10.5.1.3.,(.6.1.4.1).,(BACKFLUSH),1 2,.1 2 (),.10.5.1.1 (RESET)()1,0 ,5%,-2-.,.,.6 1 2,.1 2 -.2 .2 ,16ASTM D 5580-15 10.5.1.1.,1 2,.
13、(TCD)82-.2.1 2 10.5.1.2 BACKFLUSH 1.(2-),RESET().3.10.5.1.3 BACKFLUSH 2.-,RESET().4.10.6 :10.6.1 9 .,2 17ASTM D 5580-15 12 ,.:10.6.1.1 ,1,7%-2,2,4-().-.1,0 ,10.2 10.5 2()4().(),().,-2.-2.-WCOT-RESET 4.-,-,-.-RESET 4.10.6.1.2 -,-,(10.5).,18ASTM D 5580-15 -.11.11.1 ,-1,2,4-,()D 4307.-,1,2,4-9 .,.,0,1,
14、0,5,1,0,2,0 5,0 ,1,0,2,5,5,0,10,0 15,0 ,-1,2,4-0,5,1,0,2,0,5,0 10,0 .,.2,.11.2 .,99,9%.19ASTM D 5580-15 2.-(15,56/15,56C)0,8845 0,8719 0,8717/-0,8679 o-0,8848 1,2,4-0,8806 C9+0,8764 2-0,8162 A 1-10 STP 109A,ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.(/-)1:3
15、-.C9+30 C9-C10.11.3 ,100 :0,1,(1,2,4-).(Wi),0,1.50 .10 ,2-,(Ws)0,1.2,2,4-().0-5(32-40F),.11.4 ,20ASTM D 5580-15 RESET,(11.1),10.5.1(BACKFLUSH)3(RESET),2(BACKFLUSH)4(RESET).3 ,(-),9 (1,2,4-).=1,41()+0,00181.3.11.4.1 ,11.4.21ASTM D 5580-15 ,.,-1,2,4-.(rspi)(amti),2 3.rspi=(Ai/As)(2):Ai-,As-.amti=(Wi/W
16、s)(3):Wi-,Ws-.11.4.1.1 (rspi)(amti).3 .11.4.1.2 r2 4.r2 0,990.,.2222yxxyr(4):xXxi(5)yYyi(6):Xi-amti ,22ASTM D 5580-15 x-amti,Yi-rspi,y-rspi.11.4.1.3 .3 r2 .3.i2 A X,Y,xXxi yYyi xy x2 y2 1.0 0.5-2,0 1,02,04,0 1,02.0 1.0-1,0-0,5 0,5 1,0 0,25 3.0 1.5 0,0 0,0 0,0 0,0 0,0 4.0 2.0 1,0 0,5 0,5 1,0 0,25 5.0 2.5 2,0 1,0 2,0 4,0 1,0 A 3x 5,1y 0,252xy 0,102x 5,22y 2222yxyxr 0,15,20,100,252r 11.4.2 i-,:(rspi)=(mi)(amti)+bi(7):rspi-i-(y-),mi-i-,amti-i-(x-),bi-y.23ASTM D 5580-15 11.4.2.1 mi bi :(8):(9)11.4.2.
