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ASTM_D_5612_-_94_2013.pdf

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1、Designation:D561294(Reapproved 2013)Standard Guide forQuality Planning and Field Implementation of a WaterQuality Measurement Program1This standard is issued under the fixed designation D5612;the number immediately following the designation indicates the year oforiginal adoption or,in the case of re

2、vision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope1.1 This guide covers planning and implementation of thesampling aspects of environmental data generation ac

3、tivities.Environmental data generation efforts are comprised of fourparts:(1)establishment of data quality objectives(DQOs);(2)design of field sampling and measurement strategies andspecification of laboratory analyses and data acceptance crite-ria;(3)implementation of sampling and analysis strategi

4、es;and(4)data quality assessment.1.2 This guide defines the criteria that must be considered toensure the quality of the field aspects of environmental dataand sample generation activities.1.3 DQOs should be adopted prior to the application of thisguide.The data generated in accordance with this gui

5、de aresubject to a final assessment to determine whether the DQOswere met.For example,many screening activities do notrequire all of the quality assurance(QA)and quality control(QC)steps found in this guide to generate data adequate tomeet the project needs.The extent to which all of therequirements

6、 must be met remains a matter of technicaljudgement as it relates to the established DQOs.1.4 This guide presents extensive management requirementsdesigned to ensure high-quality samples and data.The words“must,”“shall,”“may,”and“should”have been selectedcarefully to reflect the importance placed on

7、 many of thestatements made in this guide.1.5 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory l

8、imitations prior to use.2.Referenced Documents2.1 ASTM Standards:2D596 Guide for Reporting Results of Analysis of WaterD1129 Terminology Relating to WaterD2777 Practice for Determination of Precision and Bias ofApplicable Test Methods of Committee D19 on WaterD3370 Practices for Sampling Water from

9、Closed ConduitsD3856 Guide for Management Systems in LaboratoriesEngaged in Analysis of WaterD4210 Practice for Intralaboratory Quality Control Proce-dures and a Discussion on Reporting Low-Level Data(Withdrawn 2002)3D4447 Guide for Disposal of Laboratory Chemicals andSamplesD4448 Guide for Sampling

10、 Ground-Water Monitoring WellsD4840 Guide for Sample Chain-of-Custody ProceduresD4841 Practice for Estimation of Holding Time for WaterSamples Containing Organic and Inorganic ConstituentsD5172 Guide for Documenting the Standard Operating Pro-cedures Used for the Analysis of WaterD5283 Practice for

11、Generation of Environmental Data Re-lated to Waste Management Activities:Quality Assuranceand Quality Control Planning and ImplementationE29 Practice for Using Significant Digits in Test Data toDetermine Conformance with SpecificationsE178 Practice for Dealing With Outlying ObservationsE1187 Termino

12、logy Relating to Conformity Assessment(Withdrawn 2006)32.2 U.S.Environmental Protection Agency Documents:4QAMS-005/80(NTIS No.PB83170514/LL),Interm Guide-lines and Specifications for Preparing Quality Assurance1This guide is under the jurisdiction of ASTM Committee D19 on Water and isthe direct resp

13、onsibility of Subcommittee D19.02 on Quality Systems,Specification,and Statistics.Technical Resources,and Statistical Methods.Current edition approved Jan.1,2013.Published January 2013.Originallyapproved in 1994.Last previous edition approved in 2008 as D5612 94(2008).DOI:10.1520/D5612-94R13.2For re

14、ferenced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe ASTM website.3The last approved version of this historical standard is referenced onww

15、w.astm.org.4Available from Standardization Documents Order Desk,DODSSP,Bldg.4,SectionD,700RobbinsAve.,Philadelphia,PA19111-5098,http:/www.dodssp.daps.mil.Copyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United States1 Project Plans,Office of Monitoring S

16、ystems and QualityAssurance,Dec.29,1980QAMS-500/80.Development of Data Quality Objectives,Description of Stages I and II,July 16,1986QAMS-004/80(NTIS No.PB83219667/LL),Guidelines andSpecifications for Preparing Quality Assurance ProgramPlans,Office of Monitoring Systems and QualityAssurance,Sept.20,19803.Terminology3.1 DefinitionsThe terms that are most applicable to thisguide have been defined in Terminologies D1129 and E1187.3.2 Definitions of Terms Specific to This Standard:3.2.1 background s

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