1、 D 631798(2009.),STANDARD TEST METHOD FOR LOW LEVEL DETERMINATION OF TOTAL CARBON,INORGANIC CARBON AND ORGANIC CARBON IN WATER BY ULTRAVIOLET,PERSULFATE OXIDATION,AND MEMBRANE CONDUCTIVITY DETECTION 2013 ():2168-13/ASTM :25.10.2013 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost
2、.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of Ameri
3、can Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as
4、 the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 6317-98(2009)1 D 631798(2009.),1 D 6317;,.().1.1.1 (),(),()10 1000/.D 2777.D
5、 5997 .,1 ASTM D19 D19.03 ,.1 2009.2009.DOI:10.1520/D6317-98R09.ASTM D 6317-98(2009)2 CO2 .,.CO2 .CO2,HCO3 H+,.,.CO2 .D 4519.1.2 ,.CO2 .CO2 .1.3 ,.1.4 .D 5997.1.5 ,.ASTM D 6317-98(2009)3 ,.2.2.1 ASTM:2 D 1129,D 1192 (2003.)3 D 1193 D 2777 ,D19 D 3370 D 4210 (2002.)3 D 5997 D 4519 -3.3.1 ,2 ASTM,ASTM
6、 www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 www.astm.org.ASTM D 6317-98(2009)4 ,D 1129.3.2 ,:3.2.1 (),-.3.2.2 ,.3.2.3 ().3.2.4 ().4.4.1 .,.,.,.:(1),;(2)CO2 CO2 .(-,1 ).(3)CO2,CO2 ,;ASTM D 6317-98(2009)5(4)(=/)(/=/).,.1.1-54 .5.5.1 ,.,.6.6.1 CO2 ,.;,.:.6.2-250/4 .ASTM D 6317-98(20
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8、/,/25000/1 3,2 8,2 55 2 3,2 22 61 3 2,4 8,0 105 4 4,2 13 89 5 2,8 13 30 6 3,0 8,0 70 7 4,8 8,9 67 8 4,7 8,3 63 9 4,6 11 62 10 4,7 2,9 72 A (5/).7.1.6 ,(=),(/=).,.8.8.1 .,6 .,.6 ,.,DC.,.,BDH Ltd.,Poole,Inc.(USPC),MD.ASTM D 6317-98(2009)10 8.2 ,I II D 1193.,.,CO2 pH 2 ,CO2 ().CO2 .8.3 (15%/.)15%/.15 1
9、00.,2000/.8.4 (6M)6M ,600/.,ASTM D 6317-98(2009)11 .336 95%-(.1,84)1 .410 85%-(.1,69)1 .8.5 ,(1000/)(KHC8H4O4).,1 ;,KHC8H4O4=0,471 ,1/1/0,471 2,12 .CO2 1-,1 .9.9.1 D 1192 D 3370.9.2 ,.()40-.,.9.3 4C.pH 2.,.,ASTM D 6317-98(2009)12 -.9.4 ,.9.5 ,0,5/,.,.,.,.10.10.1 .,pH (4).,.11.11.1 1000/.11.2 .,.ASTM
10、 D 6317-98(2009)13 11.3 500/.,500/.,.14.1 .12.12.1 .,.12.2 ,.,pH 2 (),.CO2 ,.12.3 .,.ASTM D 6317-98(2009)14 13.13.1 ,.13.2 ,.,.,.14.14.1 .,.2 0,25/C 25000/C ,25000/.11,.14.2 .7 .(10%).7 -ASTM International.ASTM D 6317-98(2009)15 .,:25000/.2 14.2.1 ,.14.2.2 ().(NIST 170)(Baker 0076-001).100/.,.,.()(/
11、)=1,0202 =-0,1234 ASTM D 6317-98(2009)16 .,.2 .14.2.3 D 2777-96 3.1 11 .,.3 .14.2.4 ,:(1):St-So-14.2.5 .3 ,.ASTM D 6317-98(2009)17 2 1 2 3 4 5 6 7 8 9 10 11 12-5 5 3 5 5 5 4 5 5 5 5 5./14,6 26,8 29,8 48,1 14,3 14,9 22,9 22,4 36,3 12,5 19,4 26,5 0,8 7,0 8,8 4,0 2,5 5,4 2,3 3,1 10,2 2,5 2,5 4,7.%5,25
12、26,26 29,58 8,32 17,46 36,40 10,00 13,76 28,15 20,33 12,77 17,79 3 :(/)10 11 25 28 50 55 100 110 495 550-8 8 8 8 8 8 8 8 8 8 10,0 11,0 25,0 28,0 50,0 55,0 100,0 110,0 495,0 550,0 8,53 6,04 20,58 23,14 49,19 51,13 96,70 103,08 482,45 541,33%85,25 54,89 82,30 82,63 98,38 92,95 96,70 93,70 97,46 98,42
13、(St)4,45 3,62 3,92 2,17 4,77 2,57 6,51 4,39 17,40 21,75 ,%52,19 59,92 19,07 9,40 9,69 5,03 6,73 4,26 3,61 4,02-8 8 8 8 8 (So)5,28 1,87 2,00 3,46 3,59 ,%72,47 8,54 4,00 3,47 0,70 .7 0,46 0,40 0,96 0,39 0,55 0,52 0,60 0,48 1,17 1,36.7 ,%1,41 1,39 1,62 0,82 0,58 0,68 0,50 0,37 0,25 0,26 ASTM D 6317-98(
14、2009)18 14.2.6 ,2,.,3.,.15.15.1 ,.15.1.1 ,.,10 550/.,.,ASTM D 6317-98(2009)19 ,14.,.3 15.1.2 .11.1 15.1.3 .12.15.1.4 ,().10 550/.,/,/(St)ASTM D 6317-98(2009)20 .15.1.5 ,.,20.,.,x 3ST,ST x 14.15.1.6 .(P):A-,-,-,Vs-,V-,.,ASTM D 6317-98(2009)21,.15.1.7 ,.,.,F-.16.16.1;ASTM D 6317-98(2009)22 (1)Godec,R.
15、D.,Kosenka,P.K.,Hutte,R.S.,5,132,094(21 1992.).(2)Godec,R.,ONeill,K.,Hutte,R.,1992.,17-22.(3)Deak-Phillips,A.,Rathgraber,K.,Hutte,R.,1993.-,.(4)Barley,R.,Hutte,R.,ONeill,K.,/1994.,20-25.(5)Bollinger,M.J.,Craig,A.,Godec,R.,Kosenka,P.,ONiell,K,16-,1997.ASTM D 6317-98(2009)23 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).ASTM(www.astm.org/COPYRIGHT/).
