1、Designation:D585496(Reapproved 2015)Manual of Petroleum Measurement Standards(MPMS),Chapter 8.3Standard Practice forMixing and Handling of Liquid Samples of Petroleum andPetroleum Products1This standard is issued under the fixed designation D5854;the number immediately following the designation indi
2、cates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope1.1 This practice covers the handling,mixing,and cond
3、i-tioning procedures that are required to ensure that a represen-tative sample of the liquid petroleum or petroleum product isdelivered from the primary sample container/receiver into theanalytical test apparatus or into intermediate containers.1.2 Annex A2 covers acceptance test criteria for powerm
4、ixer and sample container combinations,while Annex A3and Annex A4 detail acceptance tests for mixing systems.Appendix X1 is a guide for selecting sample containers.1.3 For sampling procedures,refer to Practices D4057(APIMPMS Chapter 8.1)and D4177(API MPMS Chapter 8.2).Practice D5842(API MPMS Chapter
5、 8.4)covers sampling andhandling of light fuels for volatility measurement.1.4 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine t
6、he applica-bility of regulatory limitations prior to use.2.Referenced Documents2.1 ASTM Standards:2D4057 Practice for Manual Sampling of Petroleum andPetroleum ProductsD4177 Practice for Automatic Sampling of Petroleum andPetroleum ProductsD4306 Practice for Aviation Fuel Sample Containers forTests
7、Affected by Trace ContaminationD4928 Test Method for Water in Crude Oils by CoulometricKarl Fischer TitrationD5842 Practice for Sampling and Handling of Fuels forVolatility Measurement2.2 API Documents:3MPMS Chapter 8.1 Practice for Manual Sampling of Petro-leum and Petroleum Products(ASTM Practice
8、D4057)MPMS Chapter 8.2 Practice for Automatic Sampling ofPetroleum and Petroleum Products(ASTM PracticeD4177)MPMS Chapter 8.4 Practice for Sampling and Handling ofFuels for Volatility Measurement(ASTM Practice D5842)MPMS Chapter 10.9 Test Method for Water in Crude Oils byCoulometric Karl Fischer Tit
9、ration(ASTM Test MethodsD4928)Recommended Practice 2003,Protection Against IgnitionsArising Out of Static,Lighting,and Stray CurrentsPublication 2026,Safe Access/Egress Involving FloatingRoofs of Storage Tanks in Petroleum ServicePublication 2217,Guideline for Confined Space Work in thePetroleum Ind
10、ustry2.3 Department of Transportation:4Code of Federal Regulations,Title 49,Section 1732.4 Occupational Safety and Health Standards:429 Code of Federal Regulations,Subpart Z,“Toxic andHazardous Substances,”Part 1910.1000 and following3.Terminology3.1 Definitions of Terms Specific to This Standard:3.
11、1.1 intermediate containerthe vessel into which all orpart of the sample from a primary container/receiver istransferred for transport,storage,or ease of handling.3.1.2 petroleumdenotes petroleum crudes,as well as pe-troleum products,normally associated with the petroleumindustry.1This practice is u
12、nder the jurisdiction of ASTM Committee D02 on PetroleumProducts,Liquid Fuels,and Lubricants and the API Committee on PetroleumMeasurement,and is the direct responsibility of Subcommittee D02.02.08 the jointASTM-API committee on Sampling(API MPMS Chapter 8.0).Current edition approved April 1,2015.Pu
13、blished June 2015.Originallyapproved in 1996.Last previous edition approved in 2010 as D5854 96(2010).DOI:10.1520/D5854-96R15.2For referenced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refe
14、r to the standards Document Summary page onthe ASTM website.3Available from American Petroleum Institute(API),1220 L.St.,NW,Washington,DC 20005-4070,http:/www.api.org.4Available from the Superintendent of Documents,U.S.Government PrintingOffice,Washington,DC 20402.Copyright ASTM International,100 Ba
15、rr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United States1 3.1.3 primary container/receiverthe vessel in which asample is initially collected.3.1.3.1 DiscussionExamples of primary sample contain-ers include glass and plastic bottles,cans,and fixed andportable sample receivers.3.1.4 s
16、amplingall the steps required to obtain a samplethat is representative of the contents of any pipe,tank,or othervessel,and to place that sample in a container from which arepresentative test specimen can be taken for analysis.3.1.5 test specimenthe representative sample taken fromthe primary or intermediate sample container for analysis.4.Significance and Use4.1 Representative samples of petroleum and petroleumproducts are required for the determination of chemical andphysical properties used to
