1、:D 5443-14 -,200C STANDARD TEST METHOD FOR PARAFFIN,NAPHTHENE,AND AROMATIC HYDROCARBON TYPE ANALYSIS IN PETROLEUM DISTILLATES THROUGH 200C BY MULTI-DIMENSIONAL GAS CHROMATOGRAPHY 2017 ():30.01.2017:3075-17/ASTM -,.9,-49,-1,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interst
2、andart.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testi
3、ng and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version
4、.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 5443-14 1 :D 5443-14 -,200C 1 D 5443;,.().1.*1.1 ,200C.200C 270C .,.,1 ASTM D02 ,D02.04.0L .15 20
5、14.2014.1993.2009.D 5443-04(2009)1.DOI:10.1520/D5443-14.ASTM D 5443-14 2 ,C9 ,.1.2 ,C6 C7,C5.0,05%.1.3 ,/,.1.4,.1.4.1 C.1.5 ,.,.7 .1.2.2.1 ASTM:2 D 4057 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 5443-14 3 D 4307 ,D 5134 -D6839 ,3.3.1 ,-.,200C.,.,.-.3.2 -100%.3.3
6、 .D 5134.,ASTM D 5443-14 4 D6839 (PIONA).1.(.)(.)(.)2,3-(.)(.)1-(.)(.)(.)1,-2-(.)2,2,4-()(.)(.)1,-2,-4-(.)(.)(.)(.)(.)(.)()(.)-()(.)()(.)1,2-(-)(.)(.)1,2,4-(.)1,2,3-(.)1,2,4,5-(.)()4.4.1 ASTM D 5443-14 5 .4.2 ,.5.5.1 ,.(,-)(,).6.6.1 ,130 0,1C :6.1.1 ,.6.1.2 ,.6.1.3 -,:150C 170C 0,015/5 10-12 /107 5,
7、5%,ASTM D 5443-14 6 15%.,.,C13,-C15,.,;.6.2 ,.,.,0,1 0,5.,(120C 180C).6.3 :6.3.1 75 ,6.3.2 (%),6.3.3 ,6.3.4 ,(2),6.3.5 ,6.3.6 ,.6.4 ASTM D 5443-14 7 ,-.,Tenax3,.2.,-,.,:2.Tenax3 Molsieve ,3 4 0,16-0,18 1,8 0,002-0,06 ,2,0-2,1 1,8-2,0 2,5 1,6-2,0 1,6 OV-275A OV-101A.%30 4-5.ChromasorbB ChromasorbB.PA
8、W WAW.Tenax3-13XC,D.60/80 80/100 80/100.A OV-101 OV-275 Ohio Valley Specialty Chemical Co.,115 Industry Rd.,Marietta,OH 45750.B Chromasorb World Minerals,Corp.,Santa Barbara,CA.13X.D 13X 5A -.6.4.1 Tenax 60C 280C,5C,.3 Tenax AKZO,Velperiveg 76,P.O.Box 9300,6800 SB Arnhem,.ASTM D 5443-14 8,1,5.6.4.2
9、100C 490C,10C,.,10,450C 100C 15.6.4.3 170C 350C.170C 220C.1 /.,ASTM.,.7.7.1-,.7.1.1,99,995%,0,1/H2O.().7.1.2,99,995%,0,1/H2O.().7.2 :7.2.1,99,99%.().ASTM D 5443-14 9 7.2.1,10/().7.3 .,-.,-.,.7.4 ,.2 .,8.2 ,9.7.5 .,:7.5.1 .7.5.2 .ASTM D 5443-14 10 ,(PFA).7.5.3 ,-,.7.5.4 ,.7.6 ,.1.,.1,.,.1,0%6,0%.,.,.
10、,C9.99%.D 4307.7.7 :7.7.1-:7.7.1.1 -ASTM D 5443-14 11 ,.16 23/,620 (90 .).-A.7.7.1.2,.7.7.1.3 -Tenax .12 17/,517 (75 .).-.7.7.1.4 -.10 15/.7.7.2 ,-,.7.7.3 ,.3 -.,-.ASTM.ASTM D 5443-14 12 .1.-8.8.1 ,.,.8.1.1 .1 2 -.()()TENAX .13 0 1 -ASTM D 5443-14 13 .8.1.2 .3 13 .2.8.1.3 .3 4 ,.1.3.A 8.1.4 .5 6 ,.2
11、.-TENAX .13 ASTM D 5443-14 14 1 .4.A 1 .5.B 1 .6.B -.13.13.13 TENAX TENAX TENAX -ASTM D 5443-14 15 .7.1 .8.C 8.2 ,.A,B C,-.-.13.13 TENAX TENAX -ASTM D 5443-14 16 9.9.1 .,.3 4,.5 6 .,.9.2 -,A,B C,7.6.,11 12,:0,3%(,C5),0,3%(,).1 .9.C -TENAX.13 ASTM D 5443-14 17 .10.11.12.-TENAX TENAX TENAX.13.13.13 -A
12、STM D 5443-14 18 .13.3.(.1),(C),(C),130 130 130 130 column 220 220 150 150 13X 100 430 ,30 5 Tenax3 60 280 1 9.3 :9.3.1 ,.3,.3 4 ,.5 6 .9.3.2 0,2 .-TENAX.13 -ASTM D 5443-14 19 200C ,200C.,.4.(.1)()(),/23 16-23 ,/15 10-15 ,/14 12-17 A,3,6 2,7-4,6 ,3,4 2,7-4,6 ,3,6 2,7-4,6 9.3.3 80%.,-,.9.3.4 .4.100C
13、430C,/.3 5.ASTM D 5443-14 20 ,.13 ,:,.5.(.2),(C),(C),130 130 130 130 column 170 170 170 170 13X 100 430 10C Tenax 60 280 1 9.3.5 .5.100C,Tenax .,.9.3.6 ,C8,200C Tenax.,-,-C9.9.3.7 .6.Tenax 280C .ASTM D 5443-14 21 .200C .6.(.2)()(),/25 20-35 ,/7 5-10 ,/20 15-30 A,2 1,7 2,5 ,2 1,7 3,0 ,2 1,7 3,0 9.3.8
14、 4,5 Tenax .7 .Tenax 60C.5,5.200C .9.3.9 .8,.Tenax,C8,C9 C10.,.200C,ASTM D 5443-14 22 .9.3.10 ,-,90%-.9.3.11 .9.Tenax 280C .9.3.12 4,5 Tenax .10 .Tenax 60C.5,5.200C .9.3.13 .11 Tenax.10 ,Tenax.9.3.14 .12.Tenax 280C .200C .9.3.15 6,5 Tenax .13 ASTM D 5443-14 23 200C .Tenax 60C,.14.9.4 ,11 12,.,:0,3%(
15、,C5),0,3%(,).9.5 ,9.3.10.10.1 .D 4057.ASTM D 5443-14 24 .10.2 .3.10.3 ,9.3 .10.4 0,2 .,.10.5 .11.11.1 ,.14 .7.-.,.,.15.11.2 ,.ASTM D 5443-14 25 11.3 ,100%.-,.8,:(1):Fi-,Caw-,12,011,4 Cn-,Haw-,1,008,4 Hn-,0,7487-.,1.11.3.1 0,88 200C,0,85 200C 0,835 C9 .11.4 ,.:Aic=Ai Fi(2):Aic-,4 ASTM DS 4B,C1 C10,AS
16、TM International,W.Conshohocken.ASTM D 5443-14 26 Ai-.11.5 ,11.4:(3):T-.7.1 2-3 4 2,3-5-6 1-7 8 4-1-9-10 1,-2-11 2,2,4-12-13 1,-2,-4-14-15-16-17-18 19 ()20-()21-22 23 1,2-(o-)24-25 1,2,4-26 1,2,3-27 1,2,4,5-28 ASTM D 5443-14 27 .15.8.-,3 0,916.4 0,906.5 0,899 0,874.6 0,895 0,874 0,811 7 0,892 0,874 0,820 8 0,890 0,874 0,827 9 0,888 0,874 0,835 10 0,887 0,874.11 0,886 0,874.11.6 ,.:ASTM D 5443-14 28 (4):Mi-.12.12.1 :12.1.1 C11,0,01%,12.1.2 ,200C,0,01%,12.1.3 ,200C(,-),0,01%,12.1.4 C9 (,C9+),0,01%
