1、:D 481515 ,TAME,DIPE,1 4 STANDART TEST METHOD FOR DETERMINATION OF MTBE,ETBE,TAME,DIPE,TERTIARY-AMYL ALCOHOL AND C1 TO C4 ALCOHOLS IN GASOLINE BY GAS CHROMATOGRAPHY 2015.():2733-15/ASTM :08.10.2015 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(AS
2、TM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materi
3、als(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction
4、 of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 4815-15 1 :D 481515 ,TAME,DIPE,1 4 1 D 4815;,.().1.*1.1 .-(),-(),-(),(DIPE),-,-,-,-(-).1 ASTM D02 ,D02.04.0L .
5、1 2015.2015.1989.2015.D 4815-15.DOI:10.1520/D4815-15.*ASTM D 4815-15 2 1.2 0,20%20,0%.0,20%12,0%.%.10%,0,20%.A1 ,10%.1.3 ,-85 -85,.-85 .1.4 ,(.D3606).1.5,.1.6 ,.,.ASTM D 4815-15 3 2.2.1 ASTM:2 D 1298 ,API D 1744 3 D 3606 D 4052 ,API()D 4057 D 4307 D 4420 (2004.)3 3.3.1 ,:3.1.1 1,6 .3.1.2 ,2 ASTM,AST
6、M www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 .www.astm.org.ASTM D 4815-15 4,.3.1.3 -,-,:=(S+C)/C(1):S-,-.3.1.4-3.2:3.2.1 DIPE .3.2.2 ETBE -.3.2.3 -.3.2.4 -.3.2.5 1,2,3-2-.3.2.6 WCOT ,.4 4.1 ,1,2-(),.,.ASTM D 4815-15 5 4.2 ,DIPE ,WCOT.4.3 .4.4 -.,;.5.5.1 ,.,.,.5.2 .6 6.1 ,.1,ASTM
7、D 4815-15 6 ,.2,.1,.-,(.2).1./WCOT,.2 ,15,56/15,56 C(=1,00)(DME=1,00)-DIPE -1,2-(DME)-E 2,90 3,15 3,48 3,83 4,15 4,56 5,04 5,36 5,76 6,00 6,20 6,43 6,80 7,04 8,17 0,58 0,63 0,69 0,76 0,82 0,90 1,00 1,06 1,14 1,19 1,23 1,28 1,35 1,40 1,62 0,43 0,46 0,51 0,56 0,61 0,67 0,74 0,79 0,85 0,88 0,91 0,95 1,
8、00 1,04 1,20 18,0 32,0 46,1 60,1 74,1 60,1 88,2 74,1 102,2 74,1 102,2 88,1 90,1 74,1 102,2 1,000 0,7963 0,7939 0,7899 0,7922 0,8080 0,7460 0,8114 0,7282 0,8058 0,7452 0,8170 0,8720 0,8137 0,7758 6.1.1 -.,2 -5 1 0,005%.ASTM D 4815-15 7 2.,/-:60 75 ,1,0 3,0 200 5 15:1 ,-.,200 250 3 0,2 0,3,60 18 8-10
9、18-20 ,0,1%12,0%0,1%12,0%.1,0 .1 B .1.6.1.2 ,11 .1.6.1.2.1 Valco No.A 4C10WP,1,6 (1/16).ASTM D 4815-15 8 ,15.6.1.2.2 Valco No.C10W,0,8 (1/32).0,32 .6.1.2.3 ,.,.6.1.3 .6.1.4 (),-.,.6.1.4.1 ,.,.6.1.4.2 ,-.6.2 ,:ASTM D 4815-15 9 6.2.1 5 .1 6.1.1.6.2.2 .,.6.3,:6.3.1 ,.6.3.2.,6.3.1.1.,6.3.2,6.1.2.3.6.3.1
10、.1 -,560 (22),1,6 (1/16)0,76 (0,030),0,14 0,15 20%P(AW)80/100.,15.6.3.2 ()6.3.2.1 .2.ASTM D 4815-15 10 6.3.2.1 WCOT,WCOT 30 (1181)0,53 (0,021)2,6 .,15.2.,7.7.1-,.-99,95 .7.2 ,.(.)ASTM D 4815-15 11 7.3,.(.)8.8.1 :8.1.1 ,1 4 ,DIPE .8.1.2 10 100 .40 P(AW)80/100 .,.,.9.9.1 ,.D 4057 .9.2 ,0 5 (32 F 40 F)
11、,.9.3 ,ASTM D 4815-15 12 0 5 (32 F 40 F),.10.10.1 560 1,6 (0,76).10.2 6 12 ,.0,14 0,15 ,.,6,0 (0,25).10.3 WCOT .(.11.1).-11.3 RESET.120 5 10.60,.11.11.1 WCOT ,.,;.11.2 .2,ASTM D 4815-15 13 .11.2.1 ,.11.3 :11.3.1 ,RESET,5,0/(14 .).11.3.2 ,70/.11.3.1 .11.3.3 BACKFLUSH 11.3.1.,.11.3.4 RESET ,3,0 3,2/.,
12、TCD,21/.11.4 ,.-,.ASTM D 4815-15 14 11.5 .,.11.5.1 BACKFLUSH 0,23.RESET 1 3 ,0,5%(.7.3),.0,23 BACKFLUSH ,.,RESET,RESET.,.2.11.5.1.1,BACKFLUSH ,.11.5.2 BACKFLUSH ,.BACKFLUSH ,0,20 0,35.,5 4.BACKFLUSH ,(,),.ASTM D 4815-15 15 11.5.2.1 DIPE BACKFLUSH ,.,DIPE.11.5.3 BACKFLUSH,.1 (TCD FID),D 4420,BACKFLUS
13、H TIME ,.12.12.1 ,.1.12.1.1 ,.12.2 ,D 4307.12.2.1 5 ,.,0,1;0,5;2;5;10,15 20%.12.2.2 .,99,9%.,D 1744.ASTM D 4815-15 16 12.2.3 ,.12.2.4 (1%)100 ,.:0,1.,.(Wi)0,1 .5 (DME)(WS)c 0,1.12.2.5 100,0 ,/(63,35%).30%,.5 (40 F),.12.3:12.3.1 .(rspi):rspi=(Ai/As)(2):Ai-,As-,(amti):amti=(Wi/Ws)(3):ASTM D 4815-15 17
14、 Wi-,Ws-,.r2 .r2 0,99 .r2 :2222yxxyr(4):=i x(5)y=Yi y(6):Xi-,amti,x-(amti)Yi-,rspi,y-(rspi).12.3.2 .3 r2 Xi Yi.12.3.3 i-:(rspi)=(mi)(amti)+bi(7):(rspi)-i-(),mi-i-,amti-i-(),bi-,.12.3.4 mi bi :mi=2/xxy(8)ASTM D 4815-15 18 bi=y mix(9)12.3.5 .3:mi=5/10=0,5(10)bi=y mix=1,5 (0,5)(3)=0(11)(.7).3:(rspi)=0,
15、5(amti)+0(12)1 bi 0 ,.3 7.3.12.3.6 bi ,.Ai 0,wi 0,1%.%i-,wi,13.,13:wi=(bi/mi)(Ws/Wg)100%(13):wi-i-,wi 0,1%,Ws-,Wg-,.ASTM D 4815-15 19 2 Ws Wg ,.3 ,12.3.7 -(bi),.3 i-(),bi=0,015 mi=1,83.13.1,Ws=0,4 (0,5)Wg=7 (9,5).13,:wi=(0,015/1,83)(0,4/7)100%=0,05%(14)12.3.8 wi 0,1%,bi,.wi .wi 0,1%.-wi 0,1%,i-.ASTM
16、 D 4815-15 20 13.13.1 0,5 (Ws)10-.0,1.10-,(Wg)0,1 .().,-.,5 (40 F).13.2 ,.1,0-3,0 15:1.,.13.3 ,.14.14.1 ,.ASTM D 4815-15 21,.3,(Wi),(rspi):(rspi)=(mi)(amti)+bi(15):(rspi)-i-(),mi-,bi-,amti-3,amti=siWW(rspi bi)/mi(16)Wi=(rspi bi)/miWs(17)=(Ai/As bi)/miWs(18)%(wi):giiWWw%)100(19):Wg-.14.2 0,01%.0,20%,.14.3 ,20:ifiiDDwV(20):wi-%,19,Vi-%,ASTM D 4815-15 22 Di-15,56 (60 F).1,Df-D 1298 D 4052.14.4%0,01%.14.5%,:iiitotMNwW0,16(21).0,160,16222111MNwMNwWtot(22):wi-%13,Wtot-%,Mi-.1 16,0-,Ni-.14.6%0,01%.15.4
