1、 D 5056-15 STANDARD TEST METHOD FOR TRACE METALS IN PETROLEUM COKE BY ATOMIC ABSORPTION 2016 ():2972-16/ASTM :29.08.2016 -,.9,-49,-1,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM Inte
2、rnational ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.AST
3、M International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or
4、FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 5056-15 1 D 5056-15 1 D 5056;,.().1.*1.1 (,)-.1.2 ,.1.1.3,.1.4 ,.1 D02 ,D02.03 .1 2015.2015.1990.2010.D5056-04(2010).DOI:10.1520/D5056-15.ASTM D 5056-15 2 ,.8-10.1 (/)(/)15 105 5,0 20 225
5、 1,0 150 500 1,5 5 200 1,5 90 420 20 15 115 0,2 5 500 2,0 2.2.1 ASTM:2 D 346 D 6299 D 1193 3.3.1 525C .(Li2B4O7)(LiBO3).2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 5056-15 3 (HCl)-:,.4.4.1 .4.2 .,.,.4.3 ,.5.5.1 ,.6.6.1,525C 10C.ASTM D 5056-15 4 6.2 .6.3 ,50-58.6.4
6、 ,150-200.6.5 .6.6,950C 10C .6.7-(AAS),:6.7.1 ,(D2),.6.7.2 ,-.6.7.3 ,-,-.6.7.4 ,:,.1 ,(.5.1).7.7.1 .,.3 3 ,American Chemical Society,Washington,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.ASTM D 5056-15 5 ,.7.2 ,II D 1193.7.3 ,1,20%(20 HCl 100 II).7.4,2,100/
7、(175 LaCl3 1).7.5 (LaCl3),().7.6 (Li2B4O7),(),(LiBO3),().7.7 ,3 40,0,0,1,Li2B4O7 150 200,.950C 10C 10 .,Li2B4O7,2-.1000 1(20-%HCl).,.2-.100 ,;.400 2().2000,ASTM D 5056-15 6 Dow.2 3 1 Li2B4O7,25 1,20-%HCl 10 2,.7.8 ,(99,9%).1000 (/)1,0 50 (/).,10 (/),.7.9 ,.,13.3 .8.8.1 .,60(0,250),D 346,10,.8.2 30 ,
8、60,200(0,075).ASTM D 5056-15 7 .110C-115C(8).(,200,60,.)9.9.1 -.(,.)10.10.1 10 (0,1),8.2,.(,HCl(5%HCl 95%),.,.,.)ASTM D 5056-15 8 10.2 525C,7,.10.3 ,1 (5,200C 10C)Li2B4O7 .,Li2B4O7 .,Li2B4O7 30.,.2 3,.950C 10C 10,Li2B4O7 .4 .,.10.4 5 10 .25,4 (1),-,25 1,.30,.5 ,.ASTM D 5056-15 9 10.5 ,100-.10 2,(.5)
9、.10.6 3(7.7),1:1.6 .10.7 -(.9).,.2.7 ,.2 ,.,.2 ()C2H2 N2O 309,3 C2H2 422,7 C2H2 248,3 C2H2 232,0 C2H2 N2O 251,6 C2H2 589,0 C2H2 N2O 318,3 10.8 ,50 3 100.(.6).8 ASTM D 5056-15 10 ,.10.9 -.11.11.1 ():M,(/)=A V C/D(1)W:M-,A-,(/),V-,W-,C/D-(10.6,).11.2 .12.12.1 ()(1000 (/)=0,1%).12.1.1 ,.,.ASTM D 5056-1
10、5 11 13.13.1 (.7.9).13.1.1 /,.13.1.2 ,X1 .14.14.1 ,ASTM RR:D02-1007.4 ,.14.1.1 ,.3.3 x=(),/,15-105 15 40,20-225 21 36,150-500 0,39 x3/4 1,18 x3/4,5-200 1,27 x1/2 1,69 x1/2,90-420 1,94 x1/2 9,41 x1/2,15-115 0,19 x 0,61 x,5-500 1,19 x1/2 2,93 x1/2 4 -ASTM International RR:D02-1007.ASTM D 5056-15 12 14
11、.1.2 ,.3 .14.1.3 ,.3 .14.2 .15.15.1;()X1.X1.1 (QC).X1.2 ,ASTM D 5056-15 13 QC(.D 6299 MNL75).X1.3 QC ,6(.D 6299 MNL75).,.,.X1.4 QC ,.,QC .,.,.QC ASTM,(.D 6299 MNL75).X1.5,QC .QC ,.X1.6.D 6299 MNL75 QC .5 MNL7,.6.,3,ASTM International,W.Conshohocken,PA.6 ,.ASTM D 5056-15 14 D02.03 (D 5056-04(2010),.(1 2015.)(1)4.2;.ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,USA.()ASTM 610-832-9585,610-832-9555 serviceastm.org (www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.
