1、Designation:D454720Standard Guide forSampling Waste and Soils for Volatile Organic Compounds1This standard is issued under the fixed designation D4547;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number
2、 in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope1.1 This guide describes recommended procedures for thecollection,handling,and preparation of solid waste,soil,andsediment samples for subsequent det
3、ermination of volatileorganic compounds(VOCs).This class of compounds includeslow molecular weight aromatics,hydrocarbons,halogenatedhydrocarbons,ketones,acetates,nitriles,acrylates,ethers,andsulfides with boiling points below 200 Celsius(C)that areinsoluble or slightly soluble in water.1.2 Methods
4、of sample collection,handling,storage,andpreparation for analysis are described.1.3 This guide does not cover the details of sampling design,laboratory preparation of containers,and the analysis of thesamples.1.4 It is recommended that this guide be used in conjunctionwith Guide D4687.1.5 This guide
5、 offers an organized collection of informationor a series of options and does not recommend a specific courseof action.This document cannot replace education or experi-ence and should be used in conjunction with professionaljudgment.Not all aspects of this guide may be applicable in allcircumstances
6、.This ASTM standard is not intended to repre-sent or replace the standard of care by which the adequacy ofa given professional service must be judged,nor should thisdocument be applied without consideration of a projects manyunique aspects.The word“standard”in the title of thisdocument means only th
7、at the document has been approvedthrough the ASTM consensus process.1.6 The values stated in SI units are to be regarded asstandard.No other units of measurement are included in thisstandard.Reporting of test results in units other than SI shallnot be regarded as nonconformance with this standard.1.
8、7 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this standard to establish appro-priate safety,health,and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.8 Th
9、is international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade(
10、TBT)Committee.2.Referenced Documents2.1 ASTM Standards:2D1193 Specification for Reagent WaterD1586/D1586M Test Method for Standard Penetration Test(SPT)and Split-Barrel Sampling of SoilsD3550/D3550M Practice for Thick Wall,Ring-Lined,SplitBarrel,Drive Sampling of SoilsD4687 Guide for General Plannin
11、g of Waste SamplingD4700 Guide for Soil Sampling from the Vadose ZoneD5058 Practices for Compatibility of Screening Analysis ofWasteD5681 Terminology for Waste and Waste ManagementD5792 Practice for Generation of Environmental Data Re-lated to Waste Management Activities:Development ofData Quality O
12、bjectivesD6051 Guide for Composite Sampling and Field Subsam-pling for Environmental Waste Management ActivitiesD6232 Guide for Selection of Sampling Equipment forWaste and Contaminated Media Data CollectionActivitiesD6282/D6282M Guide for Direct Push Soil Sampling forEnvironmental Site Characteriza
13、tionsD6418 Practice for Using the Disposable En Core Samplerfor Sampling and Storing Soil for Volatile Organic Analy-sis(Withdrawn 2018)3D6640 Practice for Collection and Handling of Soils Ob-tained in Core Barrel Samplers for Environmental Inves-tigationsD8170 Guide for Using Disposable Handheld So
14、il CoreSamplers for the Collection and Storage of Soil for1This guide is under the jurisdiction of ASTM Committee D34 on WasteManagement and is the direct responsibility of Subcommittee D34.01.02 onSampling Techniques.Current edition approved Sept.1,2020.Published September 2020.Originallyapproved i
15、n 1991.Last previous edition approved in 2015 as D4547 15.DOI:10.1520/D4547-20.2For referenced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe
16、ASTM website.3The last approved version of this historical standard is referenced onwww.astm.org.Copyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United StatesThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recommendations issued by the World Trade Organization Technical Barriers to T
