1、:D 492710 ,STANDARD TEST METHODS FOR ELEMENTAL ANALYSIS OF LUBRICANT AND ADDITIVE COMPONENTS BARIUM,CALCIUM,PHOSPHORUS,SULFUR,AND ZINC BY WAVELENGTH-DISPERSIVE X-RAY FLUORESCENCE SPECTROSCOPY 2012 ():1796-12/ASTM :19.10.2012 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru htt
2、p:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Soc
3、iety for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the or
4、iginal version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 4927-10 1 :D 492710 ,1 D 4927;,.().1.*1.1 ,.1.1 ASTM D02 D02.03 .1 2010.2010.1989.2
5、005.D4927-05.DOI:10.1520/D4927-10.ASTM D 4927-10 2 1.2 A(),(.8 13).1.3 B(),(.14 19).1.4%,.1.5 ,.,.2 ASTM:2 D 6299 3.3.1 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 4927-10 3 ,.,.-.(A B).1.,%0,04-8,5 0,01-1,0 0,01-0,5 0,1-4,0 0,01-0,6 3.2 A().3.2.1,(,).().,().3.2.2
6、 ASTM D 4927-10 4 3.2.1.3.3 B(),.,.3.3.1 ,.,.3.3.2 ().3.3.3 ,.().3.4 ,1.1.ASTM D 4927-10 5 4.4.1 ,.:,.,.5.5.1 ,.,.,0,03%()1%().,.,.6.6.1 ,1 10.ASTM D 4927-10 6 :6.1.1 ,().6.1.2,.6.1.3 ,(LiF200),(PET),().6.1.4 ,.6.1.5,.6.2,30 1.6.3 ,.3,0,25 0,35 (6,3 8,8).1 ,(,).7.7.1 .,3 E.I.du Pont de Nemours and C
7、o.ASTM D 4927-10 7 4.,.A()8.8.1,.8.2 P-10,90%10%().8.3 ,(,-).8.4 :8.4.1 ,5,0 0,1%.(2,5 0,1%),9.1,.(,),(2,5 0,1%),9.1,4 ,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.ASTM D 4927-10 8 ,5,0 0,1%.2 ,().8.4.2 2-,8,0 0,1%.(4,0 0,1%),9.1,.-(,),(4,0 0,1%),9.1,8,0 0,1
8、%.8.4.3 ,12,0 0,1%.%,12,0 0,1%.(,),12,0 0,1%.12,0 0,1%,ASTM D 4927-10 9,12,0 0,1%.8.4.4 ,24,0 0,1%.8.5 :3 ,8.5.1-8.5.5,-,(,)%.8.5.1 2-,4%,0,1%(95%-),10.1.1 10.1.2.8.5.2 ,4%,0,1%(95%-),10.1.1 10.1.2.8.5.3(2-),97%(9,62%).(),4,0 0,1%,0,1%(95%-),10.1.1 10.1.2.8.5.4 ,4%,0,1%(95%-),10.1.1 10.1.2.8.5.5-n-,
9、97%,(21,9%).(ASTM D 4927-10 10),2,0%,0,1%(95%-),10.1.2.8.6 (QC),.QC 12.9.9.1,240 0,5 (5,0 0,1%),30 0,1 2-(8,0 0,1%)30 0,1 (8,0 0,1%)450 1 1.10.,8.4.1 8.4.2,:A=240 (5/x)(1)B=30 (8/y)(2)C=720 A+B(3):A-,-,-,ASTM D 4927-10 11 x-,%,-,%.9.2 ,24%,.(,).10.10.1,:10.1.1 0,1%,0,00,0,01,0,025,0,050,0,075 0,10%.
10、10.1.2 0,1%,0,00,0,10,0,25,0,50,0,75 1,00%.10.1.3 1,000 0,001 ,8.4.3,30.10.1.4 1,000 0,001 ,9.1,30.10.1.5 8,00 0,001 ,10 .10.2:10.2.1 ,ASTM D 4927-10 12 0,00 2,00%.10.2.2 1,000 0,001 30 ().10.2.3 9,000 0,001 ,.10 ,6.2.11.,11.1 .,.11.2 (),.2.60.4 ,.2,.11.3 R ,:R=E/I(4):E-,I-.ASTM D 4927-10 13 5 .2.,.
11、LiF200.,2 L1 2,77596 87,17 K1,2 3,35948 113,09 ()L1 3,00115 96,38 ()L1 3,5994 126,77 ()K2 2,75216 86,23 K1,2 2,836 89,56 ()L1 2,7958 87,96 K1,2 1,43644 41,80 ()K1,2 1,65791 48,63 ()K1,2 1,54184 45,03 K1,2 2,4746 75,85 ()1 2,4345 74,41 11.4 (%),.,10.1.1 10.1.2.,.ASTM D 4927-10 14 12.12.1 QC .QC,13.13
12、.13.1 ,:13.1.1 ,1,0%,8,000 0,001 30,1,000 0,01 ,9.1,1,000 0,001 ,9.2.10.13.1.2 ,1,0%,0,5%.8,000 0,001 30,1,000 0,001 ,9.1,1,000 0,001 ,9.2.10.13.1.3 ,13.1.1 13.1.2 ,11.1,11.2.11.3.ASTM D 4927-10 15 6 ,10,-,(,)%.13.1.4%,():,%=SDSM(5):M-,%,S-,D-,.13.2 :13.2.1 ,2%,9,000 0,001 30,1,000 0,001 (9.2).13.2.
13、2 ,2%,1 1,5%.9,000 0,001 30,1,000 0,001 (9.2).13.2.3 13.2.1 13.2.2 ,./.13.1.4 .ASTM D 4927-10 16 B()14.14.1,.14.2 P-10,90%10%().14.3 ,(,-).14.4 4:14.4.1 2-,5%,0,1%,15.1.(,),5,0,0,1%(95%-).14.4.2 ,4%,0,1%,15.1.(,),4,0,0,1%(95%-).14.4.3(2-),97%(9,62%).(ASTM D 4927-10 17 ),2,5%,0,1%(95%-),15.1.14.4.4 ,
14、2,5%,0,1%(95%-),15.1.(,),2,5%,0,1%(95%-)14.4.5-n-,97%,(21,9%).(),7,5%,0,1%(95%-),15.1.7 (.8.5 14.4).14.5 (QC),.QC 18.ASTM D 4927-10 18 15.15.1 ,14.4.1-14.4.5,(.3).15.2 .3 ,.3.(%)1 0 0,80 0,5 0 0,5 2 1,0 0 0 0 0 3 1,0 0 0,5 0 0,5 4 0 0,80 0,5 1,5 0 5 0,5 0,40 0,25 0,75 0,25 6 0 0 0,5 1,5 0,5 7 1,0 0
15、0 1,5 0,5 8 1,0 0 0,5 1,5 0 9 0 0,80 0 1,5 0,5 10 0,5 0,40 0,25 0,75 0,25 11 1,0 0,80 0 1,5 0 12 1,0 0,80 0,5 1,5 0,5 13 0 0 0,5 0 0 14 0 0,80 0 0 0 15 0,5 0,40 0,25 0,75 0,25 16 1,0 0,80 0,5 0 0 17 0 0 0 1,5 0 18 0 0 0 0 0,5 19 1,0 0,80 0 0 0,5 20 0,5 0,40 0,25 0,75 0,25 16.16.1 .,.ASTM D 4927-10 1
16、9 16.2 (),.4.60.8 ,.4,.4.,2,78 3,55 6,15 5,37 1,43-LiF200 LiF200 LiF200 ,2 87,13 113,1 140,92 106,22 41,79 ,2 85,7 114,5 142,90 108,00 43,6 A FS D F F F FS D A F=,S=FS=,D=,.16.3 ,(),:(6):Ci-i,Di-i,Ei-i,Ii-i,ij-j i,ASTM D 4927-10 20 Cj-j.,.16.4 ,(,.)(,).,.17.17.1%(x,xx,0,xxx,0,0 xxx).17.2,.18.18.1 QC .QC,19.ASTM D 4927-10 21 19.19.1 .,.19.2 ,(16.2).19.3 ,(16.3).19.4 19.1-19.3 ,1%,2%.20.20.1 (QC)(.12 18 ).20.1.1 ,QC/QA ,.20.1.2 QC/QA QC/QA 1.21.5 21.1 ,5 ASTM International RR:D02-1259.ASTM D 4927-
