1、:D 513-16 STANDARD TEST METHODS FOR TOTAL AND DISSOLVED CARBON DIOXIDE IN WATER ():3033-16/ASTM :21.11.2016 2016 -,.9,-49,-1,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM Internationa
2、l ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM Intern
3、ational does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“
4、Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 513-16 1 :D 513-16 1 D 513;,.().1.*1.1 ,(CO2),:A()2 800/8 15 (CO2,)5 8 0/16 24 1.2 ,.1.3 A .1 ASTM D19 D19.05 .15 2016.2016.1938.2011.D 513-111.DOI:10.1520/D0513-16.ASTM D 513-16 2 1.4 ,16.4.1.5
5、.1.6 1988.X1 .1.7 ,.,.2.2.1 ASTM:2 D 1066 D 1129,D 1193 D 1293 pH D 2777 ,D19 D 3370 D 5847 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 513-16 3 E 200 ,3.3.1:3.1.1 ,.D 1129.4.4.1 ,.0,04%CO2 .10/,;,/.4.2 CO2 .CO2 .-CO2 .,.ASTM D 513-16 4 5.5.1 .,.3 ,.5.2 ,I D 1193.
6、,.,CO2,.8.2 E 200.6.6.1 .,CO2 .7.7.1 ,D1066 D 3370.3 ,.,.,BDH Ltd.,Poole,Dorset,U.K.,Inc.(USPC),Rockville,MD.ASTM D 513-16 5 7.2 ,.,.,pH .,.,CO2 -.,.7.3 .7.4 ,.A 8.8.1 (14.3),CO2,.8.2 ,2 800/CO2.8.3 .,(pH 8 9)ASTM D 513-16 6 NaOH,.CO2 .8.4 ,.9.9.1 pH 5,0.CO2 CO2 .CO2 CO2.CO2 :9.2 pH-,.CO2,.9.3 ,pH 4
7、,8-5,2.pH ,CO2(.10).ASTM D 513-16 7 10.10.1 .,10%CO2 44/100/(CaCO3)pH 4 5,:,/pH 5 pH 4 H2S 10 7 NO2(NO2)161 24 HSO3(SO2)320(SO2)48(SO2)HOAc()372 216 HCOOH()1841 345 10.2 (),.,CO2,.10.3 .,.,:(1)(.1);(2).1 .,0,1 M ,0,1 M 0,1 M :0,1 M 0,1 M .-,0,1 M.,ASTM D 513-16 8 0,1 M.,0,4 .10.4 (12.1).1 M ,.2,5/.1
8、 M,.,0,425 NaNO3 10 .11.11.1 pH-,.11.2,CO2.4 11.3 -,.12.12.1 294 700 1.pH 4,5 HCl(90).12.2 (0,1 M)8,40 1.4 ,.ASTM D 513-16 9 12.3 (0,01 M)10,0 (0,1 M)100.12.4 .0,45-.:,.,.13.13.1 .13.2 10 100.150-.13.3 0,5 0,01 M NaHCO3 .(10)(2,2/CO2 5,0/(CaCO3).13.4 0,5 0,01 M NaHCO3 .(5)(4,4/CO2 10,0/(CaCO3).13.5
9、0,9 0,1 M NaHCO3 .(2)ASTM D 513-16 10(43,2/CO2 98,1/(CaCO3).13.6 10 0,1 M NaHCO3 .(2)(433/CO2 983/(CaCO3).13.7 .pH-,()(),.2/800/CO2.14.14.1 .14.2 150-,Vs,(100).14.3 1 ,Vb,10 .,Cm,.14.4 ,s,:ASTM D 513-16 11 15.5 15.1 ,.1().2().1.CO2,A 15.2 CO2,.1.15.3,15.1 15.2,.,D 2777,.,5 -ASTM International D19-10
10、69.ASTM Customer Service serviceastm.org.,/,/ASTM D 513-16 12 .2.CO2,A 1 A ,/,/%(91%)2,1 2,7+28,6 5,1 6,9+35,3 101 100 1,0 803 730 9,1 2,1 3,0+42,8 5,1 7,1+39,2 101 114+12,9 803 754 6,1 15.4 D 2777-77,.1.4 D 2777-13,D19.,/,/ASTM D 513-16 13 CO2,16.16.1 ,.16.2 ,.16.3 ,5 800/CO2.16.4 ,:,.,.17.17.1 .CO
11、2 ,ASTM D 513-16 14 .pH CO2.18.18.1 ,.,:(H2S),(Cl2),(Br2),(HCl),(HBr),(HI),(HF),(SO2)(SO3).18.2 ,.18.3 ,19.3.,.18.4 ,;.19.19.1 .6 6 ,Coulometrics,UIC,:P.O.Box 863,Joliet,IL 60434.,-ASTM.,1 .ASTM D 513-16 15 19.2 ,.3.A K L M D N E O F P G Q H R I S J T .3.(CO2)19.3 ,.4.,.,.19.4 ,ASTM D 513-16 16 D 12
12、93.A ,D 14/20,125,12 E .4.20.20.1 CO2 100%.20.2 (.1+5)500 170 HClO4(.1,67),1.20.3 100 2 HClO4(.1,67)5 (AgClO4).ASTM D 513-16 17 0,1 30%(H2O2),.2 (H2SO4)100 ,(Ag2SO4),30%H2O2,AgClO4.21.21.1 ;.,.-,.22.22.1 :22.1.1 .22.1.2 HClO4(.20.2)100 pH 2 3 15,CO2.22.1.3 5,00 (.22.2).0,2 HClO4(.20.2).5 B.22.1.4 CO
13、2 .ASTM D 513-16 18 22.1.5 ,.12.,.,.,.22.2 :22.2.1 CO2 800/,22.1.3,5,00.A.22.2.2 CO2 800/,.,.,CO2.CO2 100/,.22.2.3 .,.,.22.2.4 ,ASTM D 513-16 19 ,.(60)CO2,.2 CO2 .,CO2,.22.2.5 2 HClO4(.20.2)pH 3 ,HClO4.HClO4.,.22.3 pH D 1293.3 ,CO2HCO3CO3 pH.,CO2 pH.pH CO2.23.23.1 CO2 23.1.1 23.1.2 23.1.3 .23.1.1 :C
14、O2,/=0,7329(A ):ASTM D 513-16 20 A-,;-,.23.1.2 CO2 :CO2/=0,200(A ):A-,;-,.23.1.3 5,00,23.1.1 23.1.2,5.24.5 24.1 ,.5.5.CO2,ST SO SO ,CO2/ASTM D 513-16 21 24.2 CO2 ,.2.2 ,/,/%7,8 8,09+3,72 22,1 22,29+0,86 372,1 369,83 0,64 736,0 730,87 0,70 24.3 ,NaHCO3.,.,5,00.24.4 D 2777-77,.1.4 D 2777-13,D19.25.(QC
15、)25.1 ASTM D 513-16 22 .25.2 13 21.,.25.3 10%.80 120%.25.4 10%.,LCS.25.5 ,/(.D 5847).25.6 .26.26.1 (CO2);ASTM D 513-16 23 ()X1.X1.1 ,X1.1.1 X1.1.5,1988.ASTM 1987.,11.01.X1.1.1 CO2 ,CO2,.CO2 ,.pH CO2.X1.1.2 CO2 -.,CO2 ,CO2 .X1.1.3 pH .X1.1.4 8,5 5,0 pH .,CO2,pH CO2.X1.1.5 CO2 CO2 ASTM D 513-16 24 .,p
16、H.X1.2 ,X1.1.1 X1.1.5,-,D 2777.D19 (D 513-111),.(15 2016.)(1)3.1.(2)12,.(3)13.7 .(4)25.4.ASTM D 513-16 25 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.