1、:D 5291-16 ,STANDARD TEST METHODS FOR INSTRUMENTAL DETERMINATION OF CARBON,HYDROGEN,AND NITROGEN IN PETROLEUM PRODUCTS AND LUBRICANTS 2017 ():25.05.2017:3167-17/ASTM -,.9,-49,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru (ASTM International)100 rr Harbor Driv
2、e,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbo
3、r Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by a
4、ny Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 5291-16 1 :D 5291-16 ,1 D 5291;,.().1.*1.1 ,.,.1.2 ,.75%87%,9%16%0,1%2%1 ASTM D02 ,D02.03 .1 2016.2016.1992.2015.D 5291-10(2015).DOI:10.1520/D529
5、1-16.ASTM D 5291-16 2.1.3 /0,75%,.1.3.1,D 0,1%.1.4 ,.1.5 ,.1.6,.1.7 ,.,.2.2.1 ASTM:2 D 4057 D 4177 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 5291-16 3 D 6299 3.3.1 ,.,.3.2 ,.:3.2.1 (),3.2.2 .3.3 .,:3.3.1 ,3.3.2 (,),3.3.3 (),ASTM D 5291-16 4 3.3.4 ,3.3.5 .3.4 .:3
6、.4.1 A3,4 .NOx N2,NaOH CO2 H2O.,CO2 H2O.3.4.2 4,5 (,.3.4.1)CO2,N2 ,.,.,.3.4.3 4,6 3 Leco CHN-600,Leco Corporation,3000 Lakeview Ave.,St.Joseph,MI 49085.4 ,-ASTM International.1,.5 Perkin Elmer 240C 2400,CEC 240XA 440,Perkin Elmer Corporation,Main Ave.,Norwalk,CT 06856.6 Carlo Erba 1106,1108 1500,Car
7、lo Erba Strumentazione,Strada Rivoltana,20090 Rodano,Milan,Italy.ASTM D 5291-16 5 NOx N2.N2,CO2 H2O .3.4.4 D4,7 ,1050C,.,.640C(840C);,120C(50C Flash EA 1112).:,Poropak(Flash EA 1112 ).K .4,8.1 ,7 Flash EA,Thermo Fisher Scientific,Strada Rivoltana,20090 Milano,Italy.ASTM D 5291-16 6 ;,.3.5 ,:3.5.1 ,3
8、.5.2 (),3.5.3 .3.6 ,.4.4.1 ASTM ,.4.2 ,.,.4.3 ,.ASTM D 5291-16 7 5.5.1 ,.5.2 ,:5.2.1 ,(),(,).,.5.2.2 ,:5.2.2.1 (),5.2.2.2 ,.5.2.3 ,.5.2.4 (),(.2).2 ,5.2.2.5.2.5 ().,:5.2.5.1 ASTM D 5291-16 8 ,5.2.5.2 ,.5.2.6 ,().5.2.7 ,.5.3 :5.3.1 ,5.3.2 ,5.3.3 ,5.3.4 ,5.3.5 ,5.3.6 ,5.3.7 ,5.3.8 ,5.3.9 ,5.3.10 ,5.3.
9、11 .5.4 ,0,00001.5.5 .ASTM D 5291-16 9 6.6.1 .,.8 ,.1.,A,%,%,%C8H9NO 71,09 6,71 10,36 C17H23NO3 70,56 8,01 4,84 C7H6O2 68,84 4,95 -2,4-C12H14N4O4 51,79 5,07 20,14 C6H12N2O4S2 29,99 5,03 11,66 C12H10 93,46 6,54 (-)C10H16N2O8 41,10 5,52 9,59 C3H4N2 52,92 5,92 41,15 C6H5NO2 58,53 4,09 11,38 C18H36O2 75
10、,99 12,76 C4H8N2O2 41,37 6,94 24,13 C12H22O11 42,10 6,48 C6H8N2O2S 41,84 4,68 16,27 C6H15NO3 48,30 10,13 9,39 A ,10-,Inc.,Rahway,New Jersey,1983.6.1.8 ,.,.,BDH Ltd.,Poole,Dorset,U.K.,Inc.(USPC),Rockville,MD.ASTM D 5291-16 10 6.2 .1 ,3.4.1 3.4.3;.6.3-:6.3.1,(99,998%),6.3.2,(99,995%),6.3.3 ,6.3.4 .6.4
11、 (),5.2.2 5.2.3.,.,:6.4.1 A3,4:6.4.1.1,6.4.1.2 ,6.4.1.3 ,6.4.1.4 ,6.4.1.5 (),6.4.1.6-,6.4.1.7 ,4,9 .6.4.2 4,5:6.4.2.1 EA 1000,4,10 9 Com-aid,Leco,Leco Corporation,3000 Lakeview Ave.,St Joseph,MI 49085.10 EA 1000,Perkin Elmer,Perkin Elmer Corporation,Main Ave.,Norwalk,CT 06856.ASTM D 5291-16 11 6.4.2
12、.2 MgO,6.4.2.3 ,6.4.2.4 ,6.4.2.5 ,6.4.2.6 ,11 6.4.2.7 ,6.4.2.8 ,6.4.2.9 ,6.4.2.10,6.4.2.11 ,6.4.2.12 ,6.4.2.13 .6.4.3 D 4,6,7:6.4.3.1 ,6.4.3.2 (),6.4.3.3 ,6.4.3.4 (),6.4.3.5 ,6.4.3.6 ,3 1/16 (1,6),6.4.3.7,6.4.3.8 (12 ;),6.4.3.9 .6.5 (QC),.11 Cuprox,Perkin Elmer,Perkin Elmer Corporation,Main Ave.,Nor
13、walk,CT 06856.12 Chromosorb,Carlo Erba Strumentazione,Carlo Erba Strumentazion,Strada Rivoltana,20090 Rodano,Milan,Italy.ASTM D 5291-16 12 ,12.7.,7.1 D 4057 D 4177.7.2 :7.2.1 5.7.2.2 9.8.8.1 ().8.2 ,.1,.,.8.3 /(.3),.,.,.3 ASTM D 5291-16 13 50 300 .8.3.1 A3,4:8.3.1.1 ()5 .()3,1 .6,3 .11,9 .8.3.1.2 .8
14、,8 N-.N-13,8 .8.3.2 4,5:8.3.2.1 EA 10004,10 900C 10 30.,.,.2,5 ,.5 EA 10004,10.5 .2,5 .,1,2 .1,2 ,-,.ASTM D 5291-16 14 8.3.2.2 .,23,8.,1,2 .8.3.3 D4,6,7:8.3.3.1 2.50 .10.120 .10.-.8.3.3.2 5.10.-.8.3.3.3 10.3 1/16 (1,6).4,10 10.8.3.3.4 10.50 .130 ,.4,9 50 .ASTM D 5291-16 15 10.8.3.3.5 1 (),1/4 o .CO2
15、 .4 ,9.4.3,.9.9.1 A3,4:9.1.1 50 200 ,D 4057 D 4177,1 .9.1.1.1 .9.1.1.2 (11).9.1.2 .9.1.2.1:;950C ;950C 750C 53C 9.1.2.2 -,ASTM D 5291-16 16 40 .9.1.2.3 :400 3/()70 3/()7 3/6 3/9.1.3 2-4 ,.10%1%.9.1.4 .,.9.1.5 ,.1%,.9.1.6 ,.,.9.2 4,5:9.2.1 2 4 ,D 4057 D 4177,0,02 .9.2.2 .975C 640C 80C 84C ASTM D 5291
16、-16 17 137,9 110,3 ,413,7 9.2.3 2 4 .,.9.2.4 ,(K),/,.9.2.5 ,.9.3 4,6:9.3.1 5 ,D 4057 D 4177,0,02 .9.3.2 30 12 .9.3.3 .1020C 650C 60C 100C 190C 420 20 70 70 2 9.3.4 :100 20 3/ASTM D 5291-16 18 200 40 3/80 3/60 3/500 3,5/2 9.3.5 ,1 2 ,2 3 3 6 ,.9.3.6 ,.,(.5).5 1992.,.13 ,1992.9.4 D4,7:9.4.1 5 12 ,2 3 ,D 4057 D 4177,0,02 .9.4.2 (10 50 100C)10 30 .12 .,ASTM D 5291-16 19 .9.4.3 :EA ,C 950 1050 ,C 500 980,C 60 75 ,C 60 ,/120 140 ,/40 100 ,10 ,240 500 ,10 13 ,40 ,60 99,995%-,.9.4.4 ,-3-6 ,.9.4.5 ,.9.4.
