1、 D5774-95(2019.)STANDARD TEST METHODS FOR RUBBER CHEMICAL ANALYSIS OF EXTRACTABLES 2019 ():10.07.2019:3713-19/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,AS
2、TM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM Internation
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4、standard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 5774-95(2019)1 D5774-95(2019.)1 D5774;,.().1.1.1 -,SBR.,:4-11 12 19 20 26 27-42 1 ,D1418.1 ASTM D11 D11.11 .1 2019.2019.1995.2014.D5774-95(2014).DOI:10.1520/D5774-95R19.ASTM D 5774-95(2019)2 1.2 ,.,.1
5、.3 -,().2.2.1 ASTM:2 D297 D1418 D4483 ,3.3.1 .,(ACS),2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 5774-95(2019)3 .3 ,.4 4.1 100 3 10,20 40 .5 100 3 ,.5.5.1 .,-,.,()100.3“Reagent Chemicals,American Chemical Society Specifications”,Am.Chemical Soc.,Washington,DC.,.”A
6、nnual Standards for Laboratory Chemicals,”BDH Ltd.,Poole,Dorset,U.K.,and the United States Pharmacopeia,and National Formulary,U.S.Pharmacopeial Convention,Inc.,(USPC),Rockville,MD.ASTM D 5774-95(2019)4 6 6.1 ,400 500 3.6.2 .2 D297 .6.3 .6.4 .6.5 ,105 3,0 (23 .).7.7.1:7.1.1 (-)70 30 ;4 .,1.,3.7.1.2
7、H-ITM()75 25 92 8 .7.1.3.8.8.1 ,8.1.1 8.1.2.8.1.1 (450)0,1.,ASTM D 5774-95(2019)5,100 5(212 9F),0,25 0,05 (0,010 0,002),-.,.4 0,1.2 .4 6 0,1,;,2-,0,1.8.1.2 (250),0,25 0,05 (0,010 0,002),-,32(90F).0,1.,100 5(212 9F),.0,1.1,1,0%.8.2 0,5 (0,020).6 10 50.3 ,.,(.,),:(),1,5-1,7 89 94 (3,5 3,7),0,177 (80,A
8、STM D 5774-95(2019)6 5,2)4,.,.,.(b)5 6 38 38 (1,5 1,5)5 50 (2),.9.9.1 6 .9.2 100 3 (H-ITM),.,.,.3()(b),.9.3 10 (.1).,20 3 100 3 .4 ,Custom Filter Supply,8581 Mosley,Houston,TX,77075,PES212HC,74/120.-,-ASTM International.1,.5 0,84 0,25,Southern Press and Media Co.,P.O.Box 24,Augusta,GA 30903-0024 24
9、24,1/30 10 -,-ASTM International.1,.ASTM D 5774-95(2019)7 9.4 20 (.1).,20 3 100 3 .9.5 40 (.1).100 3 .9.6 5,.9.7 .1 105 3 3,0 (23 .).10.10.1 :,%=100(A B)/A(1):-,-,.11.6 11.1 (ITP),D4483 6 -ASTM International RR:D11-1002.ASTM D 5774-95(2019)8 D11,D4483.,ITP D4483 .D4483 .11.2 ,ITP,11.3.,.11.3 1 ,().1
10、.1.1 Sr r(r)SR R(R)A 6 30,05 0,112 0,317 1,05 0,137 0,39 1,29 5 32,45 0,082 0,232 0,72 0,458 1,30 4,01 3 39,73 0,132 0,374 0,94 0,289 0,82 2,06 34,08 0,111 0,314 0,92 0,322 0,91 2,29 Sr-,.R -,.(r)-(),.SR-,.R -,.(R)-(),.11.4 ().;.ASTM D 5774-95(2019)9 12.12.1 ,8.1 8.2,6.250-3 .100-3 0,1-NaOH,.13.13.1
11、 ,.:,.SBR,.14.14.1 .15.15.1:15.1.1 (-).7.1.1.,.ASTM D 5774-95(2019)10 15.1.2 H-ITM().7.1.2.H-ITM ,.15.2 :15.2.1 (0,1%).0,1 26,2 3 0,01 NaOH,.,.15.2.2 (0,2%)0,06 6,45 3 0,02 NaOH,50 3 .(H-ITM.)15.3 ()(0,1)0,10 (NaOH).16.16.1 8.1 8.2.17.17.1 ,:17.1.1 6 1.17.1.2 100 3 (15.1),.,ASTM D 5774-95(2019)11 .,
12、.4(b),.17.1.3 10 (.1).250-3 ,20 3 .100 3 .17.1.4 20 (.1).,20 3 .,250 3.17.1.5 100-3 250 3 .100 3 (20 26).17.1.6 100-3 6 .0,1 NaOH .(),100 3 ,.NaOH,.17.2 ,:17.2.1 6 .17.2.2 100 3 H-ITM(9.2)(H-ITM ,).,ASTM D 5774-95(2019)12 .,.17.2.3 10 (.1).250-3 ,20 3 .100 3 .17.2.4 20 (.1).,20 3 .,250 3.17.2.5 100
13、3 .15 (.1).250-3 ,20 3 .1.17.2.6 100 3 .15 (.1).250-3 ,20 3 .2.17.2.7 100-3 17.2.4 250-3 .17.2.8 100-3 (),6 .0,1 NaOH .(),ASTM D 5774-95(2019)13 100 3 ,.NaOH,.4 2 0,1%,17.2.6.18.18.1 :,%=(J K L 0,25)/A(2):J-NaOH,(),3,-NaOH,L-;,:284 ,346 ,315 50:50 ,-,.18.2 :,%=J+/2,5+Y/2,5 K L 0,25/A(3):J-NaOH,100-3
14、 250-3 (),3,-NaOH,ASTM D 5774-95(2019)14 L-;,:284 ,346 ,315 50:50 ,-,-NaOH,1(),3,Y -NaOH,2(),3.19.6 19.1 D4483.D4483 .19.2 (),19.3.,.19.3 1.;.,.ASTM D 5774-95(2019)15 4 ;.19.4 .2 .2.1 ,%Sr r(r)SR R(R)A 6 3,21 0,0457 0,129 4,0 0,080 0,226 7,1 5 4,65 0,0621 0,176 3,8 0,145 0,410 8,8 4 6,16 0,0804 0,22
15、8 3,7 0,191 0,541 8,8 3 4,99 0,0701 0,198 4,0 0,182 0,515 10,3 Sr-,.r-,.(r)-(),.SR-,.R-,.(R)-(),.19.5 ,r,R,(r),(R),.r R,.2,.19.6.26.6 26.9 .2.ASTM D 5774-95(2019)16 20.20.1 100-3 ,17.1.5,0,05 HCl,.21.21.1 .;.SBR,.22.22.1 ,(0,05).22.2 :22.2.1 (0,1%).15.2.1.22.2.2 (0,1%),.22.2.3 (0,1%),.22.2.4 (0,2%).
16、15.2.2(H-ITM).ASTM D 5774-95(2019)17 23.23.1 8.1 8.2 ,(17.1.5).24.24.1 6 100 3 ,(17.1.5).0,05 HCl .(),100 3 ,(17.1.2 17.1.5),(.5).HCl,.5 .,.H-ITM.25.25.1%:,%=(M N P 0,25)/A(4):M-HCl,(),3,N-HCl,ASTM D 5774-95(2019)18 P-;,:306 ,322 ,368 ,384 50:50 ,353 50:50 ,345 50:50 ,-,.26.6 26.1 D4483.D4483 .26.2 (),26.3.,.26.3 1().;.,.4 ();.ASTM D 5774-95(2019)19 26.4 .3 .26.5 ,r,R,(r),(R),.r R,.3,.3.1 ,%Sr r(r)SR R(R)A 6 0,044 0,0085 0,0241 54,7 0,0448 0,127 290,0 5 0,013 0,0056 0,0158 122,0 0,0315 0,0891 69
