1、 D 5863-00a(2016.),-STANDART TEST METHODS FOR DETERMINATION OF NICKEL,VANADIUM,IRON AND SODIUM IN CRUDE OILS AND RESIDUAL FUELS BY FLAME ATOMIC ABSORPTION SPECTROMETRY ():2933-16/ASTM :06.07.2016 2016 -,.9,-49,-1,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/
2、(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Mat
3、erials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduct
4、ion of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 5863-00(2016)1 D 5863-00a(2016.),-1.D 5863;,.().1.1.1 ,-(AAS).1.2 ,7 13 AAS ,Ni,V Fe.1.3 ,14 19 AAS ,Ni,V N
5、a.,1 ASTM D02 ,D02.03 .1 2016.2016.1995.2011.D5863-00(2011).DOI:10.1520/D5863-00AR16.ASTM D 5863-00(2016)2 ,.,.1.4 ,.1.1.5 .1.6,.1.7 ,.,.7.1,8.2,8.5,10.2,10.4 15.1.2.2.1 ASTM:2 D 1193 D 4057 D 4177 D 6299 2 ASTM ASTM,www.astm.org serviceastm.org.ASTM ASTM Document Summary.ASTM D 5863-00(2016)3 3.3.1
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7、United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.ASTM D 5863-00(2016)5.6.2 .,.7.7.1-,-/(.).1.7.2 ().1.,400 ASTM D 5863-00(2016)6 ,(.2),250,2,5.1 16(1,5,0,060).1 1 2 3 1/16 25,4 38,1 50,8 77,8 3 7/8 5 6 98,4 127 165,1.2.7.3 400,.1/ASTM D 5863-00(2
8、016)7 ()5%HNO3 .7.4 ,525 25 ,400-.,.7.5 .7.6 ,().7.7 ,(),.8.8.1 ,100/,.8.2 ,HNO3,(,.).8.3 ,50%().8.4 ,5%()19 .8.5 ,H2SO4,(,.).8.6 ,Al(NO3)3 9HOH.ASTM D 5863-00(2016)8 8.7 ,KNO3.9.9.1 ,100/:,.9.2 ,.1.5%.1.-,/318,4 232,0 248,3 0,5 20 0,5 20 3,0-10 250/Al,Al(NO3)3 5%HNO3 N2O C2H2 /C2H2/C2H2 9.3 5%,.1,.
9、9.4 ,.ASTM D 5863-00(2016)9 10.10.1 ,0,0025 0,12 .10.0,5 H2SO4 .1 ,10,100 .,.10.2 (),.,.(1/.,.,20 ,10 .)10.3 (.2).,.(.1).(),.,.,.ASTM D 5863-00(2016)10 10.4 ,.10.3 .(.).10.5 525 25.,.10.6 10 1+1 HNO3.15 30.10.7 10 (5%).10.8 .(.1)(5%).().11.11.1 -.ASTM D 5863-00(2016)11 11.2 .12.12.1 :12.2 .12.3 ,.12
10、.4 ,.,5%,.12.5 .,().12.6 ,.,12.2 12.5.12.7 ,.13./(QA/QC)13.1 ASTM D 5863-00(2016)12 QC.13.1.1 QA/QC,.13.1.2 ,1 QA/QC.13.2 ,1.14.14.1.7.1.14.2 50 100.100.15.15.1 :,-,-(.).,(/).15.2 ,U.S.P.15.3 ASTM D 5863-00(2016)13 ,100/.4 16.16.1 ,5%20%.V,Ni Na 20/,5%.20/,20%.16.2 5%,5%.,20%,20%.,.16.2.1 ()(),.2.4
11、,Conoco Inc.,Conostan Division,P.O.Box 1269,Ponca City,OK 74602.,-ASTM International.1,.ASTM D 5863-00(2016)14 2.-,/318,4 232,0 589,0 0,5 15 0,5 20 0,1-5 15/Al,N2O C2H2/C2H2/C2H2 ,16.2.2 ,.17.17.1.11.18.18.1.12.19./(QA/QC)19.1.13.20.20.1 ,:,/=(V F)/W(1):-(ASTM D 5863-00(2016)15 ,),/,V-,F-,/,W-,.20.2
12、 ,:,/=F(2):-,/,F-,/.21.21.1 :21.1.1 /.22.5 22.1 .().NIST SRM 1618.6 NIST SRM 8505.6 22.1.1 ,5 -ASTM International RR:D02-1351.ASTM D 5863-00(2016)16 ,.3 .4,.3.,/,/50 500 10 100 3 10 1-20 1,10,50 0,130,92 0,20 0,65 0,0051,4 0,98 0,12 =,/4.(/)(/)1 10 50 100 500 0,12 0,89 0,13 0,98 1,2 7,8 4,8 2,5 1,2
13、11,0 9,0 4,0 3,2 25,0 40,0 22.1.2 ,.5 .6,.22.2 ,NIST.V Ni 6 ,Gaithersburg,MD 20899.ASTM D 5863-00(2016)17 ,.V ,Ni ,.Fe Na ,.5.,/,/50 500 10 100 3 10 1-20 0,330,90 1,20,80 1,3 0,53 0,061,2 1,450,45 0,69 =,/6.(/)(/)1 10 50 100 500 0,69 4,4 0,95 4,1 6,9 11,0 27,0 10,0 6,6 21,0 48,0 15,0 15,0 89,0 170,0
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