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ASTM_D_5709_-_22.pdf

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1、Designation:D570922Standard Test Method forSieve Analysis of Petroleum Coke1This standard is issued under the fixed designation D5709;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses i

2、ndicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope*1.1 This test method details a procedure for performingparticle size distribution analysis by dry sieve testing on greenpetroleum coke with a topsize of no more than

3、 75 mm andcalcined petroleum coke with a topsize of no more than 25 mm.Size fractions go down to and include 4.75 mm for greenpetroleum coke and 75 m for calcined petroleum coke.NOTE1To convert units,see Table 1 on nominal dimensions inSpecification E11.For example,75 mm is approximately equivalent

4、to anominal sieve opening of 3 in.and 25 mm to a nominal sieve opening of1 in.Likewise,4.75 mm can be converted to approximately 0.187 in.and75 microns to 0.0029 in.1.2 The values stated in SI units are to be regarded asstandard.No other units of measurement are included in thisstandard.1.2.1 The si

5、eve size is reported as U.S.A.standard testseries in any units listed in Table 1 on nominal dimensions ofSpecification E11,or their commercial size equivalents.1.3 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user o

6、f this standard to establish appro-priate safety,health,and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the D

7、ecision on Principles for theDevelopment of International Standards,Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade(TBT)Committee.2.Referenced Documents2.1 ASTM Standards:2D2013 Practice for Preparing Coal Samples for AnalysisD4749 Test Method for Perfor

8、ming the Sieve Analysis ofCoal and Designating Coal SizeD6969 Practice for Preparation of Calcined Petroleum CokeSamples for AnalysisD6970 Practice for Collection of Calcined Petroleum CokeSamples for AnalysisD8145 Practice for Sampling of Green Petroleum CokeE11 Specification for Woven Wire Test Si

9、eve Cloth and TestSieves3.Terminology3.1 Definitions of Terms Specific to This Standard:3.1.1 bulk sample,nthe reduced and divided representa-tive portion of the gross sample as prepared for shipment to andreceived by a laboratory,to be prepared for analysis.3.1.2 gross sample,nthe original,uncrushe

10、d,representa-tive portion taken from a shipment or lot of coke.3.1.3 lot,na quantity of coke to be represented by a grosssample.3.1.4 representative sample,na sample collected in such amanner that every particle in the lot to be sampled is equallyrepresented in the gross sample.3.1.5 topsize,nthe si

11、ze of the smallest opening of onesieve of a series upon which is cumulatively retained a total ofless than 5%of the sample.This defined topsize is not to beconfused with the size of the largest particle in a lot.4.Summary of Test Method4.1 A representative coke sample is divided into ranges ofpartic

12、le size by the use of a series of square-holed sieves.5.Significance and Use5.1 The test method concerns the sieving of coke intodesignated size fractions for the purpose of characterizing thematerial as to its particle size distribution.It requires the use ofstandard sieves,standard sampling method

13、s,standard samplepreparation methods,and a minimum initial sample mass basedon lot topsize.Suggestions are given for industry typical sievestacks for both green and calcined petroleum coke.5.2 Particle size distribution is significant in that manyphysical characteristics of a coke are related to suc

14、h a1This test method is under the jurisdiction of ASTM Committee D02 onPetroleum Products,Liquid Fuels,and Lubricants and is the direct responsibility ofSubcommittee D02.05 on Properties of Fuels,Petroleum Coke and Carbon Material.Current edition approved May 1,2022.Published May 2022.Originallyappr

15、oved in 1995.Last previous edition approved in 2015 as D5709 09(2015).DOI:10.1520/D5709-22.2For referenced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary

16、 page onthe ASTM website.*A Summary of Changes section appears at the end of this standardCopyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United StatesThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade(TB

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