1、:D 459013 -STANDARD TEST METHOD FOR COLORIMETRIC DETERMINATION OF p-tert-BUTYLCATECHOL IN STYRENE MONOMER OR AMS(-METHYLSTYRENE)BY SPECTROPHOTOMETRY ():2310-14/ASTM :01.04.2014 2014 (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM I
2、nternational ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and d
3、oes not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly for
4、bidden according to the USA legislation and international copyright.-,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/ASTM D 4590-13 :D 459013 -1 D 4590;,.().1.*1.1 4-()-1 100/.,490 ,.,.1.2 ,1 ASTM D16 ,D16.07 ,C9 C10.1 2013.2013.1986.2009.D4590-09.DO
5、I:10.1520/D4590-13.*1ASTM D 4590-13 ,29.1.3,.1.4 ,.,.8.2.2.1 ASTM:2 D 1193 D 3437 D 4790,D 6809 29 E 691 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.2ASTM D 4590-13 2.2 :OSHA,29 CFR 1910.1000 1910.12003 3.3.1.D 4790 ,.4.4.1 -.5.5.1 ,.6.6.1 ,1 5 490.6.2 ,.15 3 ,732 N.Capi
6、tol St.,NW,Mail Stop:SDE,DC 20401,http:/www.access.gpo.gov.3ASTM D 4590-13.,5.0,15 NaOH 15 300 600 5 100 200 7.7.1 .,.4 ,.7.2 4-,Mp 52-55C.7.3,ACS.7.4,.7.5 n-,.7.6 ,10-(10N),.7.7 ,0,15 N.0,75 10N 25 .,25 n-0,75 .,.,4 Reagent chemicals,American Chemical Society Specifications,American Chemical Societ
7、y,Washington,DC,.Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,U.K.,United States Pharmacopeia and National Formulary,U.S.Pharmaceutical Convention,Inc.(USPC),Rockville,MD.4ASTM D 4590-13 .7.8 ().,0,500 0,001 0,0001 500 1 (0,1).1000/,1.,./=()()(106)/(1)7.9 ,D 1193,I.8.8.1 (OSHA),.8
8、.2 -,.,.8.3 ,.5ASTM D 4590-13 9.9.1 D 3437.10.10.1 5,10,20,30,40,50,70 100/0,5,1,2,3,4,5,7 10 100 .0,5/.1 ,.-.10.2 11.10.3 .2 .,.11.11.1 .11.2 15 .11.3 ,NaOH .3 ,.11.4 300 NaOH 6ASTM D 4590-13 30.4 ,30.NaOH .11.5 600 15,.11.6 5 490.11.7 /.,2 :,/=()()/()(2)12.12.1 /()-.13.13.1 ,(95%).ILS,BC .,.E 691;
9、ASTM RR:D16-1009.5 5 -ASTM International RR:D16-1009.7ASTM D 4590-13 13.2 (),.1.,“r”a 95%-.13.3 ,.1.,“R”a 95%-.1 4,7 0,23 0,94 15,2 0,47 5,08 24,5 1,55 4,91 94,6 3,98 9,94 13.4 ,95%-.0,6/,.99%-.14.14.1 .14.1.1 ,.8ASTM D 4590-13 14.1.2 ,.14.1.3 /(QA/QC),.14.1.4 /(QA/QC),D6809 .15.15.1-;AMS;-;PTBC;,BC
10、;BC D16 (D 4590-09),.(01 2013.).(1)D16.9ASTM D 4590-13 10ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).ASTM(www.astm.org/COPYRIGHT/).