1、 D 4698 92(2007)STANDARD PRACTICE FOR TOTAL OF SEDIMENT SAMPLES FOR CHEMICAL ANALYSIS OF VARIOUS METALS 2007.:0857-07/ASTM :24.12.2007 NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.-
2、,.9,-49,-1,119991.:(495)236-54-49,236-43-83:(495)230-13-72 E-mail:interstgost.ru Web:www.interstandart.ru ()(ASTM)100 Harbor Drive,West Conshohocken,PA 19428,USA.ASTM ,ASTM,.,ASTM ().This translation has been made by Federal agency on technical regulating and metrology(Interstandard)under license fr
3、om the American Society for Testing and Materials(ASTM),100 Barr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM has neither approved nor endorsed this translation,and in all cases only the English edition as published and copyrighted by ASTM shall be considered as the official version.Reproduction
4、 of this translation by parties other then Federal agency on technical regulating and metrology of Russia(Interstandard)or ASTM is strictly forbidden under U.S.and international copyright laws.NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact AS
5、TM International(www.astm.org)for the latest information.ASTM D 4377-00(2006)1 D 4698 92(2007)1 D 4698;,.()1 1.1 (),-,-,-.1.2 ,.1.3 ,ASTM,1 ASTM D19 D19.07 ,.15 2007.2007.1987.2001 D 4698-92(2001).NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontac
6、t ASTM International(www.astm.org)for the latest information.ASTM D 4377-00(2006)2().,-,(),D 3976,.1.4 ,.,.7.1.5 -.,.2.2.1 ASTM:2 D 1129,D 1192 3 D 1193 D 3976 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM 3 NOTICE:This standard has either been superseded and replaced by a
7、 new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4377-00(2006)33.3.1 -,D 1129.3.2 ,:3.2.1 -,95%.3.2.2 -,95%.4.4.1 ,:,.,.,.,NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM Internatio
8、nal(www.astm.org)for the latest information.ASTM D 4377-00(2006)4,.4,5,6,7.4.2,D 3976.4.3 ,100 (150),.4.4 -/.4.5 -,.5.5.1 ,.5.2 (,)(,).5.3 ,.4 Johnson,W.,and Maxwell,J.,Rock and Mineral Analysis(),2nd Edition,John Wiley&Sons,New York,1981,p.489.5 Pinta,M.,Modern Methods for Trace Element Analysis(),
9、Ann Arbor Science Publishers,Ann Arbor,1982,pp.133-264.6 Dolezal,J.,Povondra,C.,and Sulcek,Z.,Decomposition Techniques in Inorganic Analysis(),Elsevier Publishing Co.,New York,1968,pp.11157.7 Shapiro,L.,Rapid Analysis of Silicate,Carbonate,and Phosphate Rocks,(,)Revised Edition,U.S.Geological Survey
10、 Bulletin,1401,1975,p.76.NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4377-00(2006)5,.A-6.6.1 ,.6.2 .7.7.1 ,.4,5 7.2 (CsCl),(H3BO3),(LiBO2)(Li2B4O7),-.NOTICE:This standard ha
11、s either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4377-00(2006)68.8.1 drill point()7,5,1 (25,4),3/4 (19,05)1 3/8 (34,925).8.2 .8.3 ,1000C.9.9.1 ().,8.,.9.2 -,II D 1193.9.3 -.,8 ,DC.,Analar Standards for
12、 Laboratory Chemicals,BDH Ltd.,Poole,Dorset,U.K.United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the late
13、st information.ASTM D 4377-00(2006)7 .6.1.9.4 ,(4/)-4 CsCl 1.9.5 -6 500 .12,5 (1,41)1.9.6 -1 LiBO2,2 Li2B4O7.1-,.9.7 ,-,:(1,500),(1,249),(1,000),(0,200),(0,040),KCl(0,668),(18,987),NaCl(0,636)(1,227)(.9.5)1000.:(1500/),(500/),(1000/),(200/),(40/),(350/),(3000/),(250/)(200/).-.9.8 ,1,2 3-10,6 2 (.9.7
14、)(.9.5)100 .1.9.9 ,(.1,41).NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4377-00(2006)89.10 (1+1)-250 (.1,41)250 .9.11 (50/)-50 H3BO3 1.,12-18.1 1,2 3 1,/2,/3,/()10 6 2 100 60
15、 20 20 12 4 300 180 60 150 90 30 20 12 4 50 30 10 25 15 5 35 21 7 4 2 1 10.10.1 ,HNO3(1+1),.10.2 ,105C(.D 3976).10.3 100,100,NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4377
16、-00(2006)9 ().10.4 ,100 (150).10.5 1,2 (6 6 (152,4 152,4).0,2000 ,30./,.10.6 ,.10.5.10.7 ,.10.5.10.8 ,1000,30.2-,200C.,.10.9 ;,.3-.10.10 250 3/4 1 (19,05 25,4).50 ,.5 HNO3(1+1)NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4377-00(2006)10 60.,.10.11 60 100 .4-,.,.,.10.12 200 ,.,.10.13 10 CsCl 20 H3BO3.5-CsCl ,H3BO3 ;,-.10.14 (.9.8)100 5 CsCl 10 H3BO3(5).10.15 ASTM .NOTICE:T
