1、:D4929-19a STANDARD TEST METHODS FOR DETERMINATION OF ORGANIC CHLORIDE CONTENT IN CRUDE OIL 2020.():31.01.2020:3820-20/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru www.interstandart.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International
2、,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM Internat
3、ional does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“In
4、terstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D4929-19a 1 :D4929-19a 1 D4929;,.().1.*1.1 (1/-),(XRF).1.2 .,.5 .1 ASTM D02 ,D02.03 .1 2019.2019.1989.2019.D4929-19.DOI:10.1520/D4929-19A.ASTM D4929-19a 2 1.3 .1.4 B .1.5 C (XRF).1.6,.1.6.1 ,C.1.7 ,.
5、,.1.8 ,(TBT).ASTM D4929-19a 3 2.2.1 ASTM:2 D86 D1193 D4057 D4177 D6299 D6300 D6708 D7343 ,3.3.1 ,204C(400F).D86,.,.,2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D4929-19a 4 ,().3.2 .3.2.1 A,.,.,.25 30,.3.2.2 B,80%20%,.,800C.,.,.3.2.3 :Cl+Ag+AgCl(s)(1)ASTM D4929-19a 5
6、 3.2.4 ,:Ag Ag+e(2)3.2.5 ,.3.2.6 C,K (MWDXRF),(MEDXRF)(EDXRF)./.4.4.1 .,-,.4.1.1 ,.4.1.1.1 ,.ASTM D4929-19a 6 4.1.2 1/5/,20%.4.1.2.1 ,1/,20,Pd L,Ag L,Ti K,Sc K Cr K.23.2.2 ,(.24.6).,ASTM D4929-19a 25 2,7 (20).,.23.2.3 ,.23.2.4 ,K.23.2.5,K.23.2.6 ,().23.3 -(MEDXRF),:23.3.1 ,Ag Pd HOPG Bragg().L-Ag Pd
7、.,.23.3.2 ,(.24.6).4,0 (30,4).,.23.3.3 ,175 5,9 (10000).ASTM D4929-19a 26 (SDD).23.3.4 ,/.23.4 (EDXRF),:23.4.1 ,2,9.23.4.2 ,(,FWHM),175 5,9 (10000).(SDD).23.4.3,K .23.4.4 ,(.24.6).4,0 (30,4).23.4.5 ,/.ASTM D4929-19a 27 23.5 :23.5.1 ,/.23.5.2 ,.,(.23.5.3).23.5.3,(.23.5.2),.,.23.5.4 ,0,1 100.24.24.1 .
8、,.7 ,7 ,DC.,.,BDH Ltd.,Inc.(USPC),MD.ASTM D4929-19a 28 ,.24.2 ,.(.27.6).24.3 (CD),.1,2,4-.(.).(1,2,4-.).24.4 ,.24.5()()().,.,.,ASTM D4929-19a 29 ,.,.1%.(.27.4)(.28.1).(.29.1).3 .,.4 .24.5.1 ,.24.6 ,().99,9%.,10%(.).,.24.7 ,ASTM D4929-19a 30,(.31).5 .,.6 ,.24.8 (WMO),1/,1/.,(.27.1).,.C/H(.29.7),.25.2
9、5.1 D4057 D4177 .25.2 ,.,(),.ASTM D4929-19a 31 ,.,.25.3 ,.,.,-.,.25.4-,(.24.2).,.25.5 ,.,.,.,.25.6 ,.,.ASTM D4929-19a 32 25.7 (.23)(-).,-.,25.2 25.3.25.4.D7343 .26.26.1 ,XRF .,.26.1.1 (T),.27.27.1 ,(CD,.24.3)(WMO,.24.8).1,2,4-(.24.3).,.ASTM D4929-19a 33 ,:0 (),5,10,25/,50/100/.7 XRF ,.(.3).,0,5,.27.
10、1.1 (/),.10:(10):Cl-,/,CD-,ClCD-,/,0,8095/0,861/1,2,4-,WMO-,ClWMO-,/.27.1.2 ,27.1.27.1.3 .,.,ASTM D4929-19a 34 -.27.2 ,28 29.27.3 ,.():(11)(12):l-,Cl-/,m-,b-,.27.4 .A .13.29.1.27.5 ,.,.().ASTM D4929-19a 35 27.6 (24.2).,.,.,31.28.28.1 ,.B 29.1.28.2 :28.3 25.28.4 ,.28.5 MWDXRF ,I(.11).ASTM D4929-19a 3
11、6 ,29.28.5.1 0,5.%,.,.28.6 MEDXRF K 2,622.,(.24.8),(.8),.,29.8 ,Ag,2,8 3,3.,Pd 2,7 3,2.,.28.6.1 MEDXRF ,.28.7 EDXRF ,.ASTM D4929-19a 37 28.7.1 EDXRF ,.28.8 ,.,.,28.2 28.7,.29.29.1 ()(F).13.,F 1.(13):F-,A-,(.27.4),B-,.29.2 MWDXRF (Icor):(14)ASTM D4929-19a 38:F-,.13,I-().29.2.1 (Cl)(Icor)I .11.27.3.F
12、.29.3 MEDXRF K .29.3.1 F .29.3.2 (Cl)12 .27.3.29.4 EDXRF .29.5 0,5%,.,.,.ASTM D4929-19a 39 29.6 ,.(Clo):(15):Cld-(.28.8),/,Mo-,Mb-,Clb-,/.29.7 /(C/H),.16:(16):ClC/H-,C/H,(C/H)whiteoil-C/H ,5,7;(C/H)-C/H ,Clwhiteoil-,.29.7.1 C/H .Clwhiteoil C/H.,C/H (C/H)whiteoil.C/H .,ASTM D4929-19a 40,.16.,.29.8 ,C
13、l .11 .12(.27.3),f,.3(.12.1).30.30.1 /(/),17.2 A,22.2 B/29.8 C.30.1.1 /(/).5 A,.7-9 B/29 C.30.1.30.2 ,D4929 A,D4929 B D4929 C.C ,MWDXRF,MEDXRF EDXRF.,X2.31./(QA/QC)31.1 .ASTM D4929-19a 41 31.1.1 QA/QC ,.31.1.2 ,X1 QA/QC.31.2 ,X1.31.3 C QA/QC:31.3.1 (24.7),.31.3.1.1 1/.1/,().-1/,().,.,20/,.31.3.2 ,.,
14、ASTM D4929-19a 42 ,.31.3.3 .,-.31.3.4 ,.31.3.5 ,.31.3.6 .,.,.,.ASTM D4929-19a 43 32.8 32.1 ,.,A,B C.,X2,.32.1.1 ,.32.1.1.1 A -Cl 1/():r=0,32(+0,33)0,644(17)-/.2 .9.32.1.1.2 B -Cl 1/():r=1,01(0,17)0,467(18)8 -ASTM International RR:D02-1293 A B,RR:D02-1875 C.ASTM :serviceastm.org.ASTM D4929-19a 44 -/.
15、2 .9.32.1.1.3 C -Cl 1/()2.3 .8.1 ,C XRF r,/MWDXRF r=0,643*X0,44(19)MEDXRF r=0,591*X0,44(20)EDXRF r=0,934(X+0,4)0,48(21)R,/MWDXRF R=1,235*X0,44(22)MEDXRF R=1,500*X0,44(23)EDXRF R=2,000(X+0,4)0,48(24)X-/,round robin,29.,30(D6300),.32.1.2 ,.ASTM D4929-19a 45 2 r,Cl,/B r,/C r,/A r,/B MWDXRF MEDXRF EDXRF
16、 1 0.4 0.9 0.6 0.6 1.1 2 0.6 1.3 0.9 0.8 1.4 3 0.7 1.6 1.0 1.0 1.7 4 0.8 1.9 1.2 1.1 1.9 5 0.9 2.1 1.3 1.2 2.1 6 1.1 2.3 1.4 1.3 2.3 8 1.3 2.6 1.6 1.5 2.6 10 1.4 2.9 1.8 1.6 2.9 12 1.6 3.2 1.9 1.8 3.1 A .17.B .18 C .19 MWDXRF,.20 MEDXRF .21 EDXRF.32.1.2.1 A -Cl 1/():R=0,7(+0,33)0,644(25)-/.3 .9.32.1.2.2 B -Cl 1/():R=1,32(0,17)0,467(26)-/.3 .9.32.1.2.3 C -Cl 1/(ASTM D4929-19a 46 )2.3 .8.3 R,Cl,/B R,/C R,/A R,/B MWDXRF MEDXRF EDXRF 1 0.8 1.2 1.2 1.5 2.4 2 1.2 1.8 1.7 2.0 3.0 3 1.5 2.1 2.0 2.4 3.6
