1、 D4809-18 ()STANDARD TEST METHOD FOR HEAT OF COMBUSTION OF LIQUID HYDROCARBON FUELS BY BOMB CALORIMETER(PRECISION METHOD)2019 ():14.05.2019:3665-19/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohock
2、en,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Cons
3、hohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except f
4、or ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D4809-18 1 D4809-18 ()1 D4809;,.()1.1.1 .-,0,2%.,.1 ASTM D02 ,D02.05 ,.1 2018.2018.1988.2013.D4809-13.DOI:10.1520/D4809-18.ASTM D4809-18 2 1.2 ,0,04%,.1.3 ,1 2,1-D
5、2-D 0-GT,1-GT,2-GT.1.4 D240,.1.5,.1.6 ,.,.7,10.6,A1.7.1,A3.1.7 -,(TBT).ASTM D4809-18 3 2.2.1 ASTM:2 D129 ()D240 D1018 D1193 D1266 ()D2622 D3120 D3701 -D4294 D5453 ,-D7171 E1 C ASTM 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D4809-18 4 E144 E200 ,3.3.1:3.1.1 ,Qg(/3)
6、,.3.1.1.1 :,.,.25 C .3.1.2 ,Qn(/)4,5 ,.3 Prosen,E.J.,.F.D.Rossini,1956.,.129-148.,C-461,(,.,1947.),F.D.Rossini,.,Carnegie Press,.,.,1953.F.D.Rossini .,-44 .4 ()ASTM International RR:D02-1346.ASTM serviceastm.org.5 Jessup,R.S.,7 NBS(),.ASTM D4809-18 5 3.1.2.1 :,.:,.101,325 (1.),25 C .3.1.3 (),/C.1 ,.
7、3.2 :3.2.1 .3.2.2 .().3.2.3 .,.3.2.4 ,(2).1/=1000/(1)2 /,./.3.2.5 :1 ()=4,1868 JA 1 ()=1055,06 ASTM D4809-18 6 1 ()/=0,0041868/A 1/=0,002326/A 1.=0,101325 _ A .4.4.1 .,.,.5.5.1 ,.5.2 ,.,.5.3 ,().,ASTM D4809-18 7 ,.6 6.1 ,A1.6.2 ,0,01 10.5.1.6.3 ,0,05 10.7.2.7.7.1 .,.6 ,.7.2 ,D1193,IV,.7.3 7 .6 ,.,.,
8、.,BDH Ltd.,.,.,Inc.(USPC),.,.7 ,Clopper and Quince Orchard Roads,.,.20899,39i.,ASTM International.,1 .ASTM D4809-18 8 7.4 0,127 (36),34 B&S(-),100.7.5 .7.6 ,.(.A3.1.),.500 C.7.7 38,.8 7.8,.7.8.1 (0,0866)3,5 (NaOH)1.(.A3.2.)0,0866,E200,.7.8.2 (0,0725)3,84 Na2CO3 1.7.9 2,2,4-(),.9(.A3.3.)8 610,3M,.,AS
9、TM International.,1 .ASTM D4809-18 9 8.8.1 ,.,.,.,.,.,.,.8.2 ,.,.9.9.1 .(.A3.1.),9 ,Clopper and Quince Roads,.,.20899,217b.,ASTM International.,1 .ASTM D4809-18 10 30000.,.9.1.1 ()0,1%.,0,1%.,.(-),0,1%.9.1.2 -.10.(HNO3),11.3,:W=(Qb m+e1)/t(2):W-,/C;m-,;t-,11.1 11.2,C;e1-,;Qb-,/,NBS()39i.1000(4).ASTM
10、 D4809-18 11 3 2,2,4-.4 ,.10 1+10-6 197(P 3,04)+42(m/V)3)+30(Mw/V)3)45(t 25)(3):P-,t,m-,;Mw-,;V-,L;t-,C().9.2 10,1,2 .:Qpst=(t W e1)/a(4):Qpst-,/;t-,11.1 11.2,C;W-,/C;e1-HNO3,;a-,.9.2.1 .10.7 NBS,.12.ASTM D4809-18 12 10.10.1 .10.2 ,.10.3 100 ,U-.10.4 1,0 3 .10.5 :10.5.1 0,01 .(5),.312,.,30000,:V=(W
11、0,0032)/(Q D)(5):V-,3;W-,/C;Q-,/;D-,/3.5 ,(,180 C).ASTM D4809-18 13 10.5.2 ,.,.,.10.6 .3,0.(.),.,4,0,.,.6 2,5 3,55 ,.10.7 :10.7.1 .,.,ASTM D4809-18 14 .:3,0-3,5 C :1,5-1,8 C 10.7.1.1 ,.10.7.1.2 ,.0,5 C,0,3 C.10.7.2 0,05 .,.(2000-2100)0,05 (5).,.7 .,.10.7.3 ,.8 ,.,ASTM D4809-18 15 .1,6.,.10.8 :10.8.1
12、 ,28 C.25-.:10.8.1.1 6-9 -.10.8.1.2 12 -,-.10.8.1.3 9 11 -.10.8.2 ,.,1-.,.10.8.3 ,.ASTM D4809-18 16 15.,.,30-.3 ,.,10.,.9 ,.-,.,.10.9 :10.9.1 .,.15 .,(0,005 C).1-,.,.15.(,ASTM D4809-18 17 ).,0,00005 C.10.9.2 6 .,.0,0005 C.10.10 :10.10.1 .,1.-.,500 3.,300 3.,.10.10.2 0,02%D129,D1266-IP 107,D2622,D312
13、0,D4294 D5453,.10.10.3 C,.11.11.1 ,10,t,C,:ASTM D4809-18 18 t=tf ti r1(b a)r2(c b)(6):t-,C;a-;b-(0,1),63%();-,;ti-,C;tf-c,C;r1-,C;r2-,C.11.2 ,10,t,C,:t=tf ti(7):t-,C;tf-,C;ti-,C.11.3 (A2):e1-HNO3,=3 (0,0866)NaOH,5;e2-(H2SO4),=58,6 ,.e3-,=,/;e4-,1,13 ASTM D4809-18 19 ,0,96 C.11.4 ,:Qg(,t C)=(t W e1 e
14、2 e3 e4)/1000 M(8)Qg(,25 C)=Qg(,t C)+A(t 25)(9):Qg(,t C)-,/;Qg(,25 C)-,/;t-,C;W-,/C;M-,;t-,C;e1,e2,e3,e4-,11.3;A-,/C,25C11(A 1).10 :Qgp=Qg+0,006145H(10):Qgp-,/;H-,%,D1018,D3701 D7171.11.7 NBS,.16.ASTM D4809-18 20 11.5 11 :Qn(,25 C)=Qg(Qg,25 C)0,2122 H(11):Qn(,25 C)-,/;Qg(,25 C)-,/;H-,%,D1018,D3701 D
15、7171.1.A Qg(,t C)A Qg(,t C)A/C/C 43,00 0,00157 45,75 0,00271 43,25 0,00167 46,00 0,00282 43,50 0,00178 46,25 0,00292 43,75 0,00188 46,50 0,00302 44,00 0,00199 46,75 0,00313 44,25 0,00209 47,00 0,00323 44,50 0,00219 47,25 0,00333 44,75 0,00230 47,50 0,00344 45,00 0,00240 47,75 0,00354 45,25 0,00250 4
16、8,00 0,00365 45,50 0,00261 12.12.1 ,.,0,002/.13.12 13.1 ,12 ASTM RR:D02-1229.,RR:D02-1007.ASTM serviceastm.org.ASTM D4809-18 21 ,.13.1.1 ,20.,/1.0,097 0,096 2.0,096 0,099 3.0,100 0,091 13.1.2 ,20.,/1.0,228 0,324 2.0,239 0,234 3.0,207 0,450 13.2 ,:,/0,001 0,089 14.14.1 ;ASTM D4809-18 22 ()A1.A1.1 A1.1.1,.,23 26 C .,.,.,.A1.2 A1.2.1 ,E144,350 50.,.,.,.20,7 -ASTM D4809-18 23 .13 ,12 .A1.3 A1.3.1 (),.,.,.10 0,01 C,.,.A1.4 A1.4.1 ,1 .,.,13 Parr 1108 ,Parr Instrument Co.,211 Fifty-third St.,.,.61265.,