1、 D 3712-05(2011.)STANDARD TEST METHOD FOR ANALYSIS OF OIL-SOLUBLE PETROLEUM SULFONATES BY LIQUID CHROMATOGRAPHY ():1411-11/ASTM :11.04.2011 2011 -,.9,-49,-1,119991.:(499)236-54-49,236-43-83:(499)230-13-72 E-mail:interstgost.ru Web:www.interstandart.ru (ASTM International,)100 rr Harbor Drive,West Co
2、nshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FGU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,W
3、est Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,
4、except for ASTM International or FGU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 3712-05(2011)1 D 3712-05(2011.)369/(95)1 D 3712;,.().1.1.1 .,.1.2 ,.1.3 ,1 ASTM D02 D02.04.0 .1 2011.2011.1978.2005.D371205.DOI:10.1520/D3712-05R11.ASTM-I
5、P.ASTM D 3712-05(2011)2 ,.1.4,.1.5 ,.,.2.2.1 ASTM:2 D 95 D 2896 3.3.1:3.1.1 ,17 ,.=,(8.1.1)=,(10.1)=(10.1.1).D=(10.4)=(10.5)F=(10.6)G=(10.6)=(11.1)2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 3712-05(2011)3 I=(11.2)J=T/KS K=S=(17.1.4)=,(17.1.5)U=(17.1.2)V=,(17.1.3)
6、Wc=,25 (6.9)Ws=,25 (15.1)=(12.1)Y=H2SO4 NaOH,(12.1)Z=H2SO4 NaOH,(12.1)=(13.1)=(13.1)=H2SO4(17.1.6)=NaOH(17.1.6)DD=(17.1.7)4.4.1,.,.,.,.,.4.2 D 95.D 2896.ASTM D 3712-05(2011)4 5.5.1 .,.6.6.1 ,-2,.1.,.6.2 .6.3 ,.6.4 ,100 (212 F)559 635 (22-29).6.5 ,800-1000 (1500-1800 F).6.6,100.6.7 ,D 95.ASTM D 3712-
7、05(2011)5 .1.6.8 ,25 0,2 (77 0,3 F).2.ASTM D 3712-05(2011)6 6.9,.2.1 ;15-20 (60-68 F)25 0,2 (77 0,3 F).30.,.,().1.,Wc.7.7.1 .,.3 ,.7.2 (.).7.3 (95%),3 (.).3“Reagent Chemicals,American Chemical Society Specifications”,Am.Chemical Soc.,Washington,DC.,.”Annual Standards for Laboratory Chemicals,”BDH Lt
8、d.,Poole,Dorset,U.K.,and the United States Pharmacopeia,and National Formulary,U.S.Pharmacopeial Convention,Inc.,(USPC),Rockville,MD.ASTM D 3712-05(2011)7 7.4 (.).7.5 ,.7.6 ()(.-.).7.6.1 (1+1)(.7.6.)(HCl).7.6.2 (1+3)(.7.6.)(HCl).7.7 (99%)0,9%.(.).7.7.1 ,(1+1)99%1 .7.8 1,0 1.7.9 1,0 100 50%.7.10.250
9、74 (60 200).4 4 ,62,W.R.Grace and Co.,Davison Chemical Corp.,Baltimore,MD 21203.,-ASTM International.1,.ASTM D 3712-05(2011)8 7.11 ,(0,1/)(-.)0,1/NaOH,.7.12 ,.7.13 240 (Na2SO4)1.7.14 (1,84)(H2SO4),36/.(.-.).7.14.1 ,(0,1/)0,1/(H2SO4).8.,8.1 ,:8.1.1 10 ,0,001 250-,.50 ,.100 HCl(1+1),.,.ASTM D 3712-05(
10、2011)9 8.1.2 500-.,250-.250-50-,.500-50 HCl(1+3).50 .8.2 :8.2.1 500-50-Na2SO4,2-3 ,.8.2.2 .10 Na2SO4.,Na2SO4 3 4,.250-,50 .50-,.,10 .50 99%,0,1/NaOH .;100-,ASTM D 3712-05(2011)10 10.,0,1 NaOH ,.9.9.1 80-100 (.1).,.1 .9.2 15 1 .,.13 (),.10.10.1 ,1,25 Na2SO4(8.8.2),.:20%75 30%50 40%25 ASTM D 3712-05(2
11、011)11 10.1.1 2 ,0,001 100-,.10-25 ,.,.10.2 250-0,0001 .1 5 .10.2.1 13 (),10-.13 (1/2),200 .10.2.2 ,.10.2.3 ,250-.,.13 (1/2),10-.13 (1/2),.,.ASTM D 3712-05(2011)12 10.3 250-0,0001 .230 ,10.2.1(.2).,250-.,.13 (),.2 ,.10.4 10.2.2,.559-635 (22-25).,.550-635 (22-25).30,.,0,001.D.10.4.1 .,.10.5 10.3.30 1
12、00 ASTM D 3712-05(2011)13(212 F)550-635 (22-25).,.,0,001.10.6 (),.,7,.10.4 10.5.F G.(),.11.11.1 (10.5)25 ,100-.,25-,.100 (212 F)550-635 (22-25).11.2 ,(.3).3-4 H2SO4(.1,84),.ASTM D 3712-05(2011)14,-,.,3-4 H2SO4 ,.800-1000 (1500-1800 F).I.3 H2SO4 .H2SO4 .12.()12.1 10 (.4)0,01 250-,.100 (50%),;,.,0,1/H
13、2SO4 .,0,1/NaOH (.5).,Y,Z.4 ,5 .5 ,NaOH Na2CO3 NaHCO3.NaOH Na2CO3,ASTM D 3712-05(2011)15 NaOH,Treadwell and Hall5.13.()13.1 3 0,5 ,.,.3-4 H2SO4 ,(.3).,-,.,3-4 H2SO4 ,.800-1000 (1500-1800 F).14.14.1 D 95.15.15.1 ,70-80 (160-180 F).70-80 (160-180 F),.25 0,2 (77 0,3 F)2,5 Treadwell,F.P.,and Hall,W.T.,A
14、nalytical Chemistry,II,John Wiley and Sons,Inc.,New York,NY,p.512.ASTM D 3712-05(2011)16,.,.,;1.Ws.16.16.1 D 2896.17.17.1 ,3.1.17.1.1 :,%=(D F)100/(B/100)A (1),(D F)100/C .17.1.2 ,U,:,%=(E G)100/C (2)17.1.3 ,V,:V=(E G)J100/(B/100)A (3)17.1.4 ,S,:S=71H/I (4)ASTM D 3712-05(2011)17 17.1.5 ,:T=2S 6()(5)
15、T=2S+91()(6)T=2S 22()(7)T=S 5()(8)17.1.6 ()NaOH()H2SO4(CCA):CCB=40 YZ/10X (9)CCA=49 YZ/10X (10)17.1.7 (),DD,:DD=100(BB/AA)(71 U/S)(71 CCB/40)(11)17.1.8 :,25/25 =Ws/Wc (12)18.18.1 ,:18.1.1 ,:ASTM D 3712-05(2011)18 ,%0,63 ,%0,92,%0,1 0,000032S2 0,0000322 0,001 18.1.2 ,:,%0,92 ,%1,74,%0,34 0,000067S2 0,0000672 0,0075 18.2 ,.19.19.1 ;ASTM D 3712-05(2011)19 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).ASTM(www.astm.org/COPYRIGHT/).
