1、:D4239-181 STANDARD TEST METHOD FOR SULFUR IN THE ANALYSIS SAMPLE OF COAL AND COKE USING HIGH-TEMPERATURE TUBE FURNACE COMBUSTION 2018 ():28.11.2018:3589-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West C
2、onshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,
3、West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party
4、,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D4239-181 1 :D4239-181 -1 D4239;,.().1 2018.1.*1.1 .1.1.1 .1.2 1 ASTM D05 ,D05.21 .1 2018.2018.1983.2017.D4239-17.DOI:10.1520/D4239-18E01.ASTM D4239-181 2
5、.1.3,.,.1.4 ,.1.5 ,.,.1.6 -,(TBT).2.:2.1 ASTM:2 D346/D346M D2013/D2013M D3173/D3173M D3176 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D4239-181 3 D3180 D7448 ASTM D7582 E691 (ILS)2.2 ISO:3 ISO 5725-6 ().6.ISO 11722 3.3.1 A(1350 C)1350 C.1350 C (),SO2.,().,:.3 (),1,
6、ch.de la Voie-Creuse,Case postale 56,CH-1211,20,http:/www.iso.ch.ASTM D4239-181 4.,.,.3.1.1 A .,BBOT,.3.2 B(1150 C)(WO3).WO3.1150 C (Sn).,().,:.,.,.ASTM D4239-181 5 4.4.1 .4.2 ,.4.3 D7448.5.5.1 ,250 (60),D2013/D2013M D346/D346M.5.2 D3173/D3173M D7582,ISO 11722 ,.5.3 ,D3176 D3180.6.A(1350 C)6.1 ,3.1(
7、.1).6.2 ,(6.3),ASTM D4239-181 6 1350 C.,.6.3 ,.,1350 C,.6.4 ,.1 ,6.5 ,./-ASTM D4239-181 7 6.6 ,0,3%.(1150 C)6.7 ,3.2(.2).6.8 ,(6.8)1150 C.2 ,B 6.9 ,.6.10 ,.7.7.1 1150 -ASTM D4239-181 8 .,(),.4 ,.7.2 (.).7.3 99,5%,.(.,.)7.4 (RM),.,.,.,SR,.7.4.1 4 ,DC.,.,BDH Ltd.,Inc.(USPC),MD.ASTM D4239-181 9 ,.,2.7.
8、5 BBOT(2,5-(5-2-),C26H26N2O2S)(7,47%).7.6 (WO3).(.)8.8.1 .8.1.1 .8.2 -,.8.2.1 (7.4).,.,.ASTM D4239-181 10 8.2.1.1 ,.8.2.1.2 ,D3173/D3173M,D7582 ISO 11722.,.6.6 (6.4).,.,.8.2.2 BBOT .,.ASTM D4239-181 11 8.2.2.1 :(1).(1)MC-,MT-,SAD-(),SC-.1 (ILS),BBOT 15 80.8.2.3 (.8.2.1.1).,.(7.4),(8.2.1).,.8.2.3.1 ,
9、.8.2.3.2 ,0,707,(0,707R).2 .4.2.3“”ASTM D4239-181 12 ISO 5725-6.8.2.3.3 -,.(8.1)(8.2.1.1).8.2.,.8.3 A(1350 C)(.8.1)(.8.2.3).8.3.1 1350 C.6.6 (),().,(8.2.1).8.3.2 .8.4 B(1150 C)(.8.1)(.8.2.3).8.4.1 1150 C.8.4.2 1 (6.10),100 .8.4.3 ,6.6 ,(10).ASTM D4239-181 13 8.4.4 (),10 (5).8.4.5 ()BTU/(BTU ,0,252),
10、(10).8.4.6 (),.,.8.4.7 ,.8.4.8 .9.9.1 ,.9.2 D3176 D3180.10.10.1 :10.1.1 ,.ASTM D4239-181 14 10.1.2 ;D4239,(A B).11.11.1 250 (60)60 1(A )5,6,2(A BBOT)7 3(B)8.(Sr,r)(SR,R)A1.1-A1.5 A1.1.()250 (60),%(r)(R)0,28 5,61 0,02+0,03A 0,02+0,09A 0,52 0,84 0,02 0,05 .5 (ILS),E691,1999.-ASTM International RR:D05-
11、1020.ASTM serviceastm.org.6 E691,48 24 2011.,.RR:D05-1039.ASTM serviceastm.org.7 (ILS),E691,2013.-ASTM International RR:D05-1042.ASTM serviceastm.org.8 (ILS),E691,2012.-ASTM International RR:D05-1041.ASTM serviceastm.org.ASTM D4239-181 15 2.(BBOT)250 (60),%(r)(R)0,37 5,48 0,053+0,019A 0,125+0,053A 0
12、,6 6,71 0,051+0,01A 0,089+0,017A .3.B 250 (60),%(r)(R)0,38 5,6 0,04+0,05B 0,07+0,07B A ,.B .11.1.1 A A ,(1),.,BBOT(2),.1 2.,BBOT.A,.,.2 ASTM D4239-181 16 ,.11.1.2 (r),(D3180),95%.11.1.3 (R),(D3180),95%.11.2 ,.ASTM D4239-181 17 A1.A1.1 ,(Sr,r)(SR,R),A1.1 1.5.A1.1.()(Sr,r)(SR,R),250 (60),%Sr SR r R 91
13、-2 lvb 0,38775 0,011373 0,0248 0,031822 0,06939 91-1 hvAb 1,24325 0,014004 0,030572 0,039183 0,08554 91-5 hvAb 3,083 0,028888 0,060704 0,080829 0,16985 89-4 hvCb 5,6125 0,080452 0,209299 0,225106 0,58562 91-4 hvCb 0,27725 0,018384 0,025722 0,051439 0,07197 90-1 subB 1,442 0,015066 0,044989 0,042155
14、0,12588 89-7 subA 0,75475 0,019184 0,028152 0,053677 0,07877 91-6 subA 0,46825 0,023578 0,021137 0,06597 0,05914 89-6 subC 0,5235 0,016595 0,023399 0,046433 0,06547 0,666 0,021000 0,0415 0,058622 0,11605 ASTM D4239-181 18 A1.2.(BBOT)(Sr,r)(SR,R),250 (60),%Sr SR r R 89-2 subB 0,3728 0,0193 0,0534 0,0
15、541 0,1496 89-4 hvCb 5,4838 0,0598 0,1600 0,1675 0,4481 89-6 ligA 0,4670 0,0242 0,0657 0,0677 0,1839 89-7 subA 0,7204 0,0297 0,0723 0,0831 0,2023 89-8 hvBb 1,3698 0,0286 0,0453 0,0800 0,1270 89-9 hvAb 4,1013 0,0402 0,1035 0,1125 0,2899 90-1 subB 1,3696 0,0295 0,1176 0,0827 0,3292 91-2 lvb 0,3930 0,0
16、192 0,0331 0,0536 0,0926 91-5 hvAb 3,0251 0,0385 0,1035 0,1079 0,2899 2692c lvb 1,0828 0,0226 0,0410 0,0631 0,1148 -ASTM International RR:D05-1042.ASTM Customer Service serviceastm.org.A1.3.(BBOT)(Sr,r)(SR,R),250 (60),%Sr SR r R 0,6039 0,0194 0,0360 0,0544 0,1009.0,7969 0,0245 0,0437 0,0687 0,1224 DOF 0,6320 0,0148 0,0280 0,0415 0,0785 2017 3,5154 0,0310 0,0568 0,0867 0,1590 3050 4,9786 0,0350 0,0739 0,0979 0,2070 4070 6,7059 0,0437 0,0630 0,1223 0,1764 5018 6,0884 0,0356 0,0705 0,0998 0,1975 70