1、 D 301213 STANDARD TEST METHOD FOR THERMAL-OXIDATIVE STABILITY OF POLYPROPYLENE USING A SPECIMEN ROTATOR WITHIN AN OVEN 2014 ():2429-14/ASTM :15.08.2014 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Con
2、shohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,We
3、st Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,e
4、xcept for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 3012-13 1 D 301213 1 D 3012;,.()1.1.1 ,.1.2 ,.1 ,.1 ASTM D20 D20.15 .1 2013.2013.1972.2007.D 3012-07.DOI:10.1520/D3012-13.ASTM D 3012-13 2 .1.3,.,.1.4 ,.,.
5、2 ISO 4577-1983 ,.2.2.1 ASTM:2 D 618 D 883,D 3641 D 4101 D 5374 E 77 E 220 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 3012-13 3E 608 E 644 E 691 E 1137/E1137M E 2251 ASTM 2.2 ISO:3 ISO 4577-1983 ISO 1873 :1:2:3.3.1 ,D 883.4.4.1 ,.4.2 3 (ANSI),25 W.43rd St.,4th Fl
6、oor,-,NY 10036.ASTM D 3012-13 4.,.5.5.1 ,.5.2 ,.5.3 .,.,(K).100 150C 10C.5.4 .5.5 ASTM D 3012-13 5 ,.6.6.1,1000 250/(197 49/).4 6.1.1 ,150 1C(302 1,8F),.150C,154C(309F).6.2 ,0 200C(32-372F).6.2.1 .E 77.6.2.2 ASTM S67C-03 E 2251.6.2.3 E 608 E 220.6.2.4 E 644 E 1137/E1137M 4 Precision Scientific Freas
7、,835 B,M POM-206C-1,.ASTM D 3012-13 6 NIST Special Publication 250-22.5,6 6.3 ,200 5C(392 9F).6.4 ,D 3641.6.5-:6.5.1-,:6.5.1.1 -,(3)1,00 0,05 (0,039 0,002).3 152,4 152,4 (6 6).6.5.1.2 ,.3 (0,1).6.5.2-,D 3641.-1,00 0,05 (0,039 0,002),50 10 1,00 (2 0,4 0,039),50 10 1,00.6.6 ,0,05-0,20 (0,002-0,008),.5
8、 Mangum,B.W.,NBS Special Publication 250-22(1987).6 (NIST),100 Bureau Dr.,Stop 3460,MD 20899-3460.ASTM D 3012-13 7.6.7 ,50 10 (2 0,4),.6.8 ,1000/(197/).1 .2.,.6.8.1 (.1)7.1 3 1.6.8.2 (.2).,1/.1 7 CS191 Standard Scientific Supply Company .ASTM D 3012-13 8.2 6.9 ,.6.10,.,.6.11 ,.ASTM D 3012-13 97.7.1
9、-,.:7.2 :7.2.1 200 5C(392 9F).7.2.2 .,.,.-,-.,1,00 0,5 (0,039 0,002),.3-4 200 5C(392 9F).-,.7.3 :7.3.1 D 4101.7.4 .10,50 1,00 0,05.ASTM D 3012-13 10,.7.5 ,.,.4 -,-.7.6 .7.7 ,.7.8 ,.8.8.1 D 4101.,23 2C(73,4 3,6F)50 10%40 A D 618.1C(1,8F)5%.9.9.1 ,-,150C(302F)1C,1,5C .ASTM D 3012-13 119.1.1 80 (3).9.2
10、 ,150C ,150C,140 1C,10C,.5 140C,.,150C.9.3 ,1000 250/(197 49/).6 ,.7 -+23C.-+20 +80C.25%-35C .9.4 1 15%/.9.4.1 ,D 5374.9.4.2 .X1.,15%,.ASTM D 3012-13 12 ,.10.10.1 .10.2 ,.30-40 (1,2-1,6).(,).10.2.1 .,.10.3 ,.10.4 ,-,.5 .8 ,ASTM D 3012-13 13 .,.10.4.9 ,.10.5 .11.11.1 :11.1.1 ,11.1.2 ,150C8,11.1.3 ,15
11、0C9,11.1.4 ,11.1.5 ,11.1.6 ,11.1.7 ,150C,11.1.8 ,11.1.9 (),.12.12.1 1 (round robin),1970.E 691,.,8 7 150C,150C.()140C().ASTM D 3012-13 14,.1,25 (0,50).,.(r R(12.2 12.2.3).1 ,.,E 691,.12.2 12.2.3).1.,SrA SRB rC RD L 14,0 0,765 2,63 2,16 7,44 M 34,9 3,08 6,95 8,72 19,6 H 63,4 5,42 18,7 15,3 52,9 A Sr
12、.B SR .C r=2,8 Sr.D R=2,8 SR.12.2 r R Sr SR ,:12.2.1 (r),ASTM D 3012-13 15 ,Ir .12.2.2 (R),IR .12.2.3 12.2.1 12.2.2 95%-(0,95).12.3 ,.13.13.1;.()X1.X1.1.X1.1.1 ,.ASTM D 3012-13 16X1.2.X1.2.1 ,.,1-.X1.3.X1.3.1,.X1.3.2 ,.X1.4.X1.4.1,.X1.4.2 ,.X1.4.3 ,.,.,.X1.4.4 .ASTM D 3012-13 17X1.4.5 .X1.4.6 ,.X1.4
13、.7 ,.X1.5.X1.5.1 .X1.4.3.X1.5.2 (C+273=K)X1.5.3 ,PV=nRT,:(X1.1):V1-,3,V2-,3,T1-,K,T2-,K.X1.1 V1 ,3 +23C,V1 :(X1.2):V0-,+23C,3,296=296K=23C K().X1.5.4 :(X1.3):ASTM D 3012-13 18-,3/,V3-,/,A-,2,60-.X1.5.5 :(X1.4):AC-.D20 (D 3012-07),.(1 2013.)(1)6.1.(2)8.1(3)8 .10.2.(4).ASTM D 3012-13 19ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).ASTM(www.astm.org/COPYRIGHT/).
