1、 D441990(2015.)()STANDARD TEST METHOD FOR MEASUREMENT OF TRANSITION TEMPERATURES OF PETROLEUM WAXES BY DIFFERENTIAL SCANNING CALORIMETRY(DSC)2017 ():28.09.2017:3282-17/ASTM -,.9,-49,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harb
2、or Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 r
3、r Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translatio
4、ns by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D4419-90(2015)1 D441990(2015.)()1 D4419;,.()1.1.1 ,().-.1.2 15 C 150 C(1).1.3,.1.4 1 ASTM D02 ,D02.10.0A -.1 2015.2015.1984.2010.D4419-90(20
5、10).DOI:10.1520/D4419-90R15.ASTM D4419-90(2015)2,.,.2.2.1 ASTM:2 D87 ()D1160 D3418 E472 (1995.)3 E473,E474 (1986.)3 3.3.1 :3.1.1 (),2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 www.astm.org.ASTM D4419-90(2015)3 .,:c .472,473 474.4.4.1 ().,.,.,(1).1 D 87 .,-.5.5.1 ,.-,;.
6、ASTM D4419-90(2015)4 -,.2 -.120 F 5%95%D1160(760).-.-,-.5.2 ,.,C.,.6.6.1 .(10).6.2 .6.3 (10C/1C/).ASTM D4419-90(2015)5 7.7.1 ,10C/1C/15 C 150 C.,.(WE WT)0,5 C.,.7.2 ,.7.3 ,.7.4,.8.8.1,.9.9.1 ,ASTM D4419-90(2015)6 .,:99%K (1)4 26,9 300,0-(2)51,5 324,8 (3)80,3 353,6 A 122,4 395,7 (4)153,0 426,3 (1)156
7、,6 429,9 A.D 3418.99,98%SRM 350.9.2 ,10,(11.3).10.10.1 ,10 C ,.,.11.11.1 10 1 .3 4 ,.ASTM D4419-90(2015)7 .,.,.(.10.3).11.2 ;10 50/.11.3 (3).10C/1C/,20C 5C ,(4 5).15C 5C 10C/1C/.15 C 30.4 ,50 95%.5 ,.,.11.4 .10C/1C/,20C 5C (6).,10C/1C/,15C ,20C 5C.6 (),.ASTM D4419-90(2015)8 12.12.1 .(.1).(TA)(7 8).7
8、 (TO)(TE)(.1).A -.1.A()-T2A -T2O -T2E -T1A -T1O -T1E,C ASTM D4419-90(2015)9 8 .(TO)(TE).12.2 ,.13.13.1 0,5C .(T1A),(T1E),(T2A)(T2E),.14.14.1 ,:14.1.1 ,:F -,T2A 0,8(1,4),T2E 1,0(1,8)ASTM D4419-90(2015)10 -,T1A 1,2(2,2),T1E 1,4(2,5)14.1.2 ,:F -,T2A 3,5(6,3),T2E 6,1(11,0)-,T1A 2,3(4,1),T1E 11,2(20,2)9
9、-;,D87.14.1.3 .14.2 ,.ASTM D4419-90(2015)11 15.15.1 ;(1)Rossini,F.D.,Pure Applied Chemistry (),.22,1970.,.557.(2)Timmermans Hennant-Roland,J.Chim.Physics(),.34,1937.,.693.(3)API Project()44,I,23-2-(33.5200)A AE.(4)Morrison,J.D.Robertson,J.M.J.Chem.Soc.(),1949.,.987.(5)Mackenzie,R.,Nomenclature in Th
10、ermal Analysis,Part IV,(,IV)Journal of Thermal Analysis(,13,1978.,.387.ASTM D4419-90(2015)12 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.