1、 ()“-,”(“”).8527 ()1 Standard Test Methods for Carbon Black in SBR(Styrene-Butadiene Rubber)Recipe and Evaluation Procedures1 ASTM D 3191-14 :6 160:.:6 160-:12 :15.03.2016 2016.“”:8527/ASTM D :31.03.2016 D3191 10(2014)1 ()-1 D3191;,.().1 1.1 ,(SRB).1.2 ,(SI).1.3 ,.,.2 2.1 ASTM2 D412 -D1646 -,()D1799
2、 -,D1900 -,D2084 -D3182 -,D3674 -(1999)3 D4483 D5289 145 _ 1 D24 (ASTM)D24.71 .1 2014.2014.1973.2010 D3191-10.-(DOI):10.1520/D3191-10R14.2 ASTM,Web-ASTM(www.astm.org)(serviceastm.org).ASTM Web-ASTM.3 Web-ASTM:www.astm.org.D3191 10(2014)2 3 3.1 ,.(),.ASTM.3.2 .,;.4 4.1 IRM,.-1500 100,00 ,91 3,00,31 1
3、,75 ,21 1,00 50,00 TBBSC,D 1,00_ 156,75 _ A 91(IRM 91)G.H.Chemicals,Ltd.(1550 Brouillette St.,P.O.Box 456,St.Hyacinthe Quebec Canada,J2S 7B8).IRM 21 IRM 31 Akron Rubber Development Lab(2887,Gilchrist Road,Akron,OH 44305).B (MIM),.,.C 1,0;-0,02;-0,1.0,01.,0,001.DTBBS:-2-.E ,0,5,525,0.0,01.0,01,75%.5
4、5.1 D1799 D1900.5.2 1,145,1 (125 3).,10.D3191 10(2014)3 6 6.1 D3182.6.1.1 (50 5).,.:(1)-.(2)-.(3)-.6.1.1.1 .0,5%,.D1646 D2084(),D3674,.6.2 6.2.1 -,1,1 (0,045),.1/2 3/4 .2,0 2,0 .2,0 4,0 .3/4 .2,0 6,0 .1,4 (0,055),3/4 .1,8 (0,070)3/4 .10,0 16,0 -,.TBBS,1,8 (0,070).3,0 19,0 3/4 .2,0 21,0 0,8 (0,032).6
5、.2,0 23,0 ,6 (0,25)4,.1,0 24,0 _ 24,0 D3191 10(2014)4 6.2.1.1 ,2,2 (0,085).,.6.2.1.2 1 8 (23 3),(35 5)%D3182.6.2.2 -6.2.2.1 :(16)8,06/(77/).,32.6.2.2.2 ,.,-1500 ,.0,75 0,75 ,TBBS,.,.1,25 2,0 3,5,71.1,5 3,5 _ 3,5 6.2.2.3 D3182(6 12 ).,.,32.6.2.2.4 ,.0,5%,.,1,8 (0,070),TBBS 5 3/4 .2,5 2,5 2,5 6.2.2.5
6、1 ,.6.2.2.6 0,5 (0,020).650 ,.9 .,32.6.2.2.7 2,2 (0,085),.6.2.2.8 ,1 24 (23 3)55%.1 24 ,(35 5)%D3182.,7.D3191 10(2014)5 6.2.3 -6.2.3.1 ,(50 5)0,51 (0,020).,(60 3).()6,3 6,6/(60 63/).1,0 1,0 ,TBBS,.1.1,0 2,0 ,.1,0 3,0 .6,0 9,0 _ 9,0 6.2.3.2 ,.,.6.2.3.3 0,80 (0,032).,.6.2.3.4 .0,5%,.6.2.3.5 -,2,2 (0,8
7、5).6.2.3.6 D2084 ,6 (0,25).6.2.3.7 (23 3)1 8,(35 5)%D3182.,7.7 7.1 -D3182.7.1.1 :50 145.7.1.2 16 96 (23 3),.1-1-6 .,7.1.2.7.1.3 D3182.,D412.,IRB 7.,IRB.D3191 10(2014)6 7.2 -D2084 c D5289 .7.2.1 :1,7,1 0,160 0,30,.:1,7,5 0 ,0,05 ,160 0,30,.7.2.2 :(L),(MH),L 1 (ts1),50%(tc(50)90%(tc(90).8 4 8.1 D4483,
8、.8.2 -(,.),8.3 8.4.2.3.8.3 -2 1990.(SRB-4,SRB-4,SRB D-4,SRB F-4)D412.,SRB 6(IRB 6).,.(1).8.3.1 8.3.1.1 300%-300%D3191(D412)0,87 (125/2).(),0,87 (125/2),.,.8.3.1.2 -D3191(D412)2,02 (293/2).(),2,02 (293/2),.,.8.3.1.3 -D3191(D412)47,7%.(),47,7%,.,._ 4,-ASTM International,-RR:D24-1030.D3191 10(2014)7 8.
9、3.2 8.3.2.1 300%-300%D3191(D412)1,85 (268/2).(),1,85 (268/2),.,/.8.3.2.2 -D3191(D412)3,30 (478/2).(),3,30 (478/2),.,/.8.3.2.3 -D3191(D412)65,3%.(),65,3%,.,/.1-D3191-2(-;D412)300%,(/2)Sr r SR R D-4-6,28(-911)0,33(48)0,93(135)0,57(83)1,62(235)A-4-1,36(-197)0,29(41)0,81(117)0,94(137)2,67(388)B-4-0,23(-
10、34)0,15(22)0,43(63)0,54(78)1,52(220)F-4 2,45(355)0,40(58)1,13(164)0,44(64)1,24(180)-1,33(-194)0,31(44)0,87(125)0,65(95)1,85(268),(/2)Sr r SR R D-4-7,22(-1047)0,58(84)1,65(239)1,15(166)3,24(470)F-4-3,02(-437)0,60(87)1,71(248)1,06(154)3,00(435)B-4-0,38(-55)1,05(153)2,98(432)1,18(171)3,34(484)-4 2,41(3
11、49)0,48(69)1,35(195)1,27(184)3,59(520)-2,05(-298)0,71(103)2,02(293)1,17(169)3,30(478),%Sr r SR R F-4-78 17,3 48,9 17,3 48,9 B-4-6 23,5 66,5 23,5 66,5 A-4 12 9,3 26,4 17,6 49,7 D-4 105 14,0 39,7 31,2 88,2 8 16,8 47,7 23,1 65,3 .:Sr-;r-;D3191 10(2014)8 SR -;R .8.4 -2 1990.4 (SRBs A-4,B-4,D-4,F-4).D412
12、.,SRB 6(IRB 6).,.(2).8.4.1 8.4.1.1 300%-300%D3191(D412)0,77 (111/2).(),0,77 (111/2),.,.8.4.1.2 -D3191(D412)1,56 (227/2).(),1,56 (227/2),.,.8.4.1.3 -D3191(D412)78,8%.(),78,8%.,.,.8.4.2 8.4.2.1 300%-300%D3191(D412)1,29 (187/2).(),1,29 (187/2),.,/.8.4.2.2 -D3191(D412)2,87 (416/2).(),2,87 (416/2),.,/.8.
13、4.2.3 -D3191(D412),93,5%.(),93,5%,.,/.D3191 10(2014)9 2-D3191-2(-;D412)300%,(/2)Sr r SR R D-4-5,10(-740)0,05(8)0,15(22)0,53(76)1,49(216)-4-0,68(-99)0,21(31)0,60(87)0,21(31)0,60(87)-4-0,13(-19)0,15(22)0,42(61)0,50(72)1,41(205)F-4 2,36(342)0,47(68)1,34(194)0,51(74)1,45(210)-0,89(-129)0,27(39)0,77(111)
14、0,46(66)1,29(187),(/2)Sr r SR R D-4-6,58(-954)0,57(82)1,61(233)0,57(82)1,61(233)F-4-2,10(-305)0,64(93)1,82(265)1,03(149)2,92(423)-4 0,73(105)0,39(56)1,10(160)1,24(180)3,52(511)-4 2,52(366)0,57(83)1,62(235)1,08(157)3,07(445)-1,36(-197)0,55(80)1,56(227)1,01(147)2,87(416),%Sr r SR R F-4-60 14,3 40,5 26
15、,5 75,0-4 17 15,7 44,4 15,7 44,4-4 19 18,2 51,6 32,9 93,2 D-4 59 48,2 136,3 48,3 136,8 9 27,9 78,8 33,1 93,5 .:Sr-;r-;SR-;R .8.5 -2 2009.12 8(IRB 8).D412.,IRB 8 IRB 7.,.3 .8.5.1 8.5.1.1 300%-(r)300%D3191(D412)1,22 (177/2).(),1,22 (177/2),.D3191 10(2014)10 ,.8.5.1.2 -(r)D3191(D412)2,44 (354/2).(),2,4
16、4 (354/2),.,.8.5.1.3 -(r)D3191(D412)55,8%.(),55,8%,.,.8.5.2 8.5.2.1 300%-(R)300%C D3191(D412)1,57 (228/2).(),1,57 (228/2),.,/.8.5.2.2 -(R)D3191(D412)2,48 (360/2).(),2,48 (360/2),.,/.8.5.2.3 (R)D3191(D412)63,5%.(),63,5%,.,/.8.6 -().,.D3191 10(2014)11 3-D3191-2(-;D412)300%,(/2)IRB 8 Sr r SR R 3-0,82(-119)0,40(58)1,12(162)0,67(97)1,89(274)23-0,79(-115)0,43(62)1,22(177)0,80(116)2,26(328)19-0,74(-107)0,46(67)1,30(189)0,58(84)1,64(238)1-0,65(-94)0,42(61)1,18(171)0,58(84)1,63(236)13-0,58(-84)0,53(77)1,
