1、 D 312008(2014.)C STANDART TEST METHOD FOR TRACE QUANTITIES OF SULFUR IN LIGHT LIQUID PETROLEUM HYDROCARBONS BY OXIDATIVE MICROCOULOMETRY 2014 ():2442-14/ASTM :01.09.2014 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Har
2、bor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100
3、rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translati
4、ons by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 3120-08(2014)1 D 312008(2014.)1 D 3120;,.().1.1.1 3,0 1000/,26 274 C(80 525 F).1 ,(D 4806),(D 4814),Ed75Ed85(D 5798)-1 ASTM D02 ,D02.03 .
5、1 2014.2014.1972.2008.D 3120-08.DOI:10.1520/D3120-08R14.ASTM D 3120-08(2014)2 10%.,.D02.03 ,.1.2 ,1.1,1000/,.,.1.3,.(/).1.4 ,.,.7 9 .2.2.1 ASTM:2 D 1193 D 1298 ,API D 4052 ,API()2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM ASTM D 3120-08(2014)3 D 4057 D 4177 D 4806 D 4814
6、 D 5798 D 6299 2.2 OSHA:OSHA,29 CFR,1910.1000 1910.12003 3.3.1 ,900 1200 ,50 80%20 50%(,.).,-,.-,(I t),.3.2 3 ,732 N,Capitol St.,NW,Mail Stop:SDE,Washington,DC 20401.ASTM D 3120-08(2014)4 :HISOOHSOI233223 (1)-,:eII233 (2)3.3 -()SO2-,.4 4.1 ,.,.5.5.1 ,10 ,1000 .5.1.1 ,.5.2 (,Ni,V,Pb .),ASTM D 3120-08
7、(2014)5 500/().6.6.1 ,.1 ,.1.6.2 .2.2.6.3 ,900 1200,SO2.ASTM D 3120-08(2014)6 6.4 ,-,.,.-.6.5 /-,-,.Ag/AgCl ,.,.-,.2 ,.6.6 /.ASTM D 3120-08(2014)7 /().,.6.7 ().6.8 ,-.6.9 ,SO2,.,.6.10 ,5 80 .80%.6.11 .6.11.1 .-.,ASTM D 3120-08(2014)8 .(.3).6.11.1.1 (),.().,.6.11.1.2 ,.6.11.2 .,-,.,0,5 1,0/(.3).3 ,.,
8、().6.10 0,01.ASTM D 3120-08(2014)9 7.7.1 .,.4 ,.7.2 ,D1193,II III.7.3 .7.4 (3),=1,05.(.).7.5 (85%)(34).(.)7.6 ,()5,.(,.,).7.7 ()5,-.().4 Reagent chemicals,American Chemical Society Specifications,Americal Chemical Society,Washington,DC,.Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset
9、,U.K.,United States Pharmacopeia and National Formulary,U.S.Pharmaceutical Convention,Inc.(USPC),Rockville,MD.5 99,995%.ASTM D 3120-08(2014)10 7.8 -.7.9 0,5 (KI)0,6 (NaN3)500 ,6 (3)1000 .4 .7.10 (NaN3),.(.).7.11 (KI),.7.12 (KCl),.1 Ag/AgCl.7.13 (KNO3),.1 Ag/AgCl.7.14 (I),20 ,.7.15,(,).,()().(.).5 .7
10、.16 FW 184.26,17,399%(/)S(.5).7.17-FW 146.29,21,92%(/)S(c.5).ASTM D 3120-08(2014)11 7.18 ()FW 134.20,23,90%(/)S(.5).6 ,.7.19,(1000 S/),0,5748 0,4652 -0,4184 100-.1-3(.7-9).S/=CBA100106(3):-.-(S).-.1.S/S/500 50 10 1000 1000 500 25 5 2 50 100 100 2.S/1 S/2 S/3 S/-2,5 0,5-50 1,0-250 2,5-500 5,0-1000 0,
11、2 0,2 0,5 1,0 2,5 1,0 5 10 25 50 2,5 50 250 500 1000 ASTM D 3120-08(2014)12 3.S/S/10 10 50 50 50 500 500 1000 500 1000 2 5 2 5 10 5 10 25 100 100 100 100 100 100 100 100 0,2 0,5 1,0 2,5 5,0 25 50 250 500 1000 7.20,.1.7 ,.3.8 /,.9 ,.7.21 (QA),.(QA),11.(QA),.ASTM D 3120-08(2014)13 8.8.1 .8.2 ,OSHA,(MS
12、DS).9.9.1 D 4057 D 4177.,.,.9.1.1(,.;).9.2 ,.10.10.1 -.10.2 .ASTM D 3120-08(2014)14 10.3 .10.4 ,.10.5 .10.6 .10.7 ,.11.11.1 .,.11.2 .2.3.:-S/=BA100 (4):-S/.-.10 ASTM D 3120-08(2014)15.,.,.,.11 ,.11.3 .4 ,.11.4 .,.11.5 .80%.4.S/S 5,0 0,5-50 1,0 250 2,5-500 5,0-1000 80 60 30 20 10-0,25 0,03-1,5 0,03-5
13、,0 0,05-5,0 0,05-10 11.5.1 ,ASTM D 3120-08(2014)16 10%,.,10%,.12 .11.5.2 ,.,0,01.11.5.3 ,.11.5.4 ,.,(.13).(),(.14).2 ,(.15).13 ,.14 ,.ASTM D 3120-08(2014)17 120.,.15 .,.11.5.4.1 ,.,.11.5.5 .().,.,.16 ,0,5 1,0/.11.5.5.1 ,.11.6 ,:11.6.1 ,11.3 11.5.5.ASTM D 3120-08(2014)18 (.12).11.6.2 ,11.3 11.5.5.,()
14、.(.12).17 (SO2).SO3,.,.75%.75%,.,75 90%.11.7 ,SO2(),75%,.,.11.8 ,.ASTM D 3120-08(2014)19 12.(QA)12.1 (QC).2.2 QC/QA ,.3.()ASTM D 3120-08(2014)20 12.3 QC/QA ,1 QC/QA.13.13.1 ,9.,.,.13.1.1 (/).13.1.2 (/).13.2 .,11.3 11.5.5.13.3 .13.3.1 ,.,.13.3.2 ,.13.3.3 ,.ASTM D 3120-08(2014)21 .13.4 ,.13.5 ,(D1298,
15、D4052 ).,.14.14.1 /():,/()=1000 (5),/()=DV 1000 (6):-,(,),-,/,/.M-,V D,.V-,/D,.D-,/.1000-/().ASTM D 3120-08(2014)22 15.15.1 ,.(I)6,RR:D02-1036.(II)7,8 16 ,.3/S 5/S .15.1.1:15.1.1.1 I ,1 20,=.r=0,2802X(0,7901)(7)15.1.1.2 II 3 100/5 40/.:0,03194(+7,4502)1,3226 :0,08520(+0,65758):/15.1.2:6 -ASTM Intern
16、ational RR:D02-1036 7 -ASTM International RR:D02-1546 8 -ASTM International RR:D02-1547.ASTM D 3120-08(2014)23 15.1.2.1 I ,1 20,=.R=0,5973X(0,7901)(8)15.1.2.2 II 3 100/5 40/.:0,1470(+7,4502)1,3226 :0,5152(+0,65758):/15.2 (SRM)(NIST).SRM 2298(4,6/S)2299(13,6/S)SRM 2723(10/S).SRM 2299 2723.,-1,25 SRM 2298.8 16.16.1 ;.ASTM D 3120-08(2014)24 ()1.(QC)1.1 .1.2 QC(.D 6299 MNL 79).1.3 QC .(.D 6299 MNL 79).().,.1.4 QC ,.QC .QC ,.,QC .QC ASTM.1.5,QC,9 ASTM MNL 7,Manual on Presentation of Data Control Char
